This publication presents the first Quality Manual for the Laboratories at the Nuclear Materials Characterization Division. The Manual describes the laboratories, its organization structure, fields of activities, personnel records, equipments, maintenance and calibration. The main aspects concerning quality assurance in the analysis were discussed. The whole system of receiving, identifying and processing analysis of the samples is shown. Since there are many information to be contained in several subjects of the Quality Manual, there were produced separate documents that are cross referenced in the manual. (author).