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{sup 232} Th - {sup 233} Pa separation by extraction chromatography

Abstract

Thorium and protactinium behavior in extraction chromatography systems is presented, aiming its separation by selective retention of the micro constituent on the column. TBP/alumina, TBP/voltalef UF 300, TOA/alumina and TOA/voltalef UF 300 systems were verified. Column preparation as well the {sup 233} Pa removal conditions were settled. The best {sup 232} Th separation from its irradiation product, {sup 233} Pa, has been achieved by using TBP/voltalef UF 300 system. {sup 233} Pa was selectively retained on column from 10 M HCl solutions and eluted with 3 M HCl. (author).
Publication Date:
Dec 31, 1991
Product Type:
Miscellaneous
Report Number:
INIS-BR-3076; CONF-9110453-
Reference Number:
SCA: 400105; PA: AIX-24:000078; SN: 93000912531
Resource Relation:
Conference: 31. Brazilian Congress on Chemistry,Recife (Brazil),21-25 Oct 1991; Other Information: PBD: 1991
Subject:
37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; PROTACTINIUM 233; EXTRACTION CHROMATOGRAPHY; THORIUM 232; EXPERIMENTAL DATA; GAMMA SPECTROSCOPY; HYDROCHLORIC ACID; TBP; TDA; 400105; SEPARATION PROCEDURES
OSTI ID:
10108383
Research Organizations:
Instituto de Pesquisas Energeticas e Nucleares (IPEN), Sao Paulo, SP (Brazil)
Country of Origin:
Brazil
Language:
English
Other Identifying Numbers:
Other: ON: DE93608791; TRN: BR9230503000078
Availability:
OSTI; NTIS (US Sales Only); INIS
Submitting Site:
INIS
Size:
[10] p.
Announcement Date:
Jun 30, 2005

Citation Formats

Matsuda, H T, and Araujo, B.F. de. {sup 232} Th - {sup 233} Pa separation by extraction chromatography. Brazil: N. p., 1991. Web.
Matsuda, H T, & Araujo, B.F. de. {sup 232} Th - {sup 233} Pa separation by extraction chromatography. Brazil.
Matsuda, H T, and Araujo, B.F. de. 1991. "{sup 232} Th - {sup 233} Pa separation by extraction chromatography." Brazil.
@misc{etde_10108383,
title = {{sup 232} Th - {sup 233} Pa separation by extraction chromatography}
author = {Matsuda, H T, and Araujo, B.F. de}
abstractNote = {Thorium and protactinium behavior in extraction chromatography systems is presented, aiming its separation by selective retention of the micro constituent on the column. TBP/alumina, TBP/voltalef UF 300, TOA/alumina and TOA/voltalef UF 300 systems were verified. Column preparation as well the {sup 233} Pa removal conditions were settled. The best {sup 232} Th separation from its irradiation product, {sup 233} Pa, has been achieved by using TBP/voltalef UF 300 system. {sup 233} Pa was selectively retained on column from 10 M HCl solutions and eluted with 3 M HCl. (author).}
place = {Brazil}
year = {1991}
month = {Dec}
}