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Title: Apparatus and method for the determination of grain size in thin films

Abstract

A method for the determination of grain size in a thin film sample comprising the steps of measuring first and second changes in the optical response of the thin film, comparing the first and second changes to find the attenuation of a propagating disturbance in the film and associating the attenuation of the disturbance to the grain size of the film. The second change in optical response is time delayed from the first change in optical response.

Inventors:
 [1]
  1. Barrington, RI
Issue Date:
Research Org.:
Brown Univ., Providence, RI (United States)
OSTI Identifier:
873571
Patent Number(s):
6191855
Assignee:
Brown University Research Foundation (Providence, RI)
Patent Classifications (CPCs):
G - PHYSICS G01 - MEASURING G01B - MEASURING LENGTH, THICKNESS OR SIMILAR LINEAR DIMENSIONS
G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
DOE Contract Number:  
FG02-86ER45267
Resource Type:
Patent
Country of Publication:
United States
Language:
English
Subject:
apparatus; method; determination; grain; size; films; film; sample; comprising; steps; measuring; changes; optical; response; comparing; attenuation; propagating; disturbance; associating; change; time; delayed; time delay; optical response; grain size; sample comprising; film sample; /356/

Citation Formats

Maris, Humphrey J. Apparatus and method for the determination of grain size in thin films. United States: N. p., 2001. Web.
Maris, Humphrey J. Apparatus and method for the determination of grain size in thin films. United States.
Maris, Humphrey J. Mon . "Apparatus and method for the determination of grain size in thin films". United States. https://www.osti.gov/servlets/purl/873571.
@article{osti_873571,
title = {Apparatus and method for the determination of grain size in thin films},
author = {Maris, Humphrey J},
abstractNote = {A method for the determination of grain size in a thin film sample comprising the steps of measuring first and second changes in the optical response of the thin film, comparing the first and second changes to find the attenuation of a propagating disturbance in the film and associating the attenuation of the disturbance to the grain size of the film. The second change in optical response is time delayed from the first change in optical response.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Mon Jan 01 00:00:00 EST 2001},
month = {Mon Jan 01 00:00:00 EST 2001}
}

Works referenced in this record:

Nondestructive detection of titanium disilicide phase transformation by picosecond ultrasonics
journal, November 1992


Study of vibrational modes of gold nanostructures by picosecond ultrasonics
journal, January 1993


Ion implant monitoring with thermal wave technology
journal, September 1985


Picosecond Ellipsometry of Transient Electron-Hole Plasmas in Germanium
journal, May 1974


Picosecond acoustic pulse reflection from a metal‐metal interface
journal, September 1990


Picosecond acoustics as a non-destructive tool for the characterization of very thin films
journal, November 1987


Sound velocity and index of refraction of AlAs measured by picosecond ultrasonics
journal, November 1988


Carrier lifetime versus ion‐implantation dose in silicon on sapphire
journal, February 1987


Generation and detection of picosecond acoustic pulses in thin metal films
journal, March 1987


Laser Picosecond Acoustics in Various Types of Thin Film
journal, January 1992


Analysis of lattice defects induced by ion implantation with photo‐acoustic displacement measurements
journal, November 1994


Transient thermoreflectance from thin metal films
journal, July 1986


Measurements of the Kapitza conductance between diamond and several metals
journal, March 1992


High Resolution Laser Picosecond Acoustics in Thin Films
book, January 1991


Time-resolved study of vibrations of a -Ge:H/ a -Si:H multilayers
journal, September 1988


Detection of Thin Interfacial Layers by Picosecond Ultrasonics
journal, January 1992


Kapitza conductance and heat flow between solids at temperatures from 50 to 300 K
journal, December 1993


Ultrasonic experiments at ultra-high frequency with picosecond time-resolution
conference, January 1990


Nondestructive testing of microstructures by picosecond ultrasonics
journal, December 1990


Physics of ultrafast phenomena in solid state plasmas
journal, January 1978


Detection of thermal waves through optical reflectance
journal, June 1985


Surface generation and detection of phonons by picosecond light pulses
journal, September 1986


Thermal and plasma wave depth profiling in silicon
journal, September 1985


Measurements of atomic sodium in flames by asynchronous optical sampling: theory and experiment
journal, January 1992


Phonon attenuation and velocity measurements in transparent materials by picosecond acoustic interferometry
journal, April 1991


Attenuation of longitudinal-acoustic phonons in amorphous SiO 2 at frequencies up to 440 GHz
journal, September 1991


Thin‐film thickness measurements with thermal waves
journal, July 1983


Detection of Titanium Silicide Formation and Phase Transformation by Picosecond Ultrasonics
journal, January 1992


Noninvasive picosecond ultrasonic detection of ultrathin interfacial layers: CF x at the Al/Si interface
journal, October 1992


Picosecond ultrasonics
journal, January 1989


Relationship between Interfacial Strain and the Elastic Response of Multilayer Metal Films
journal, November 1988


Asynchronous optical sampling:a new combustion diagnostic for potential use in turbulent, high-pressure flames
journal, January 1989


Picosecond optical studies of amorphous diamond and diamondlike carbon: Thermal conductivity and longitudinal sound velocity
journal, September 1994


Picosecond spectroscopy of semiconductors
journal, January 1978


Picosecond photoinduced electronic and acoustic effects in a-Si:H based multilayer structures
journal, December 1987


Elastic properties of silicon oxynitride films determined by picosecond acoustics
journal, December 1988


A New Method of Photothermal Displacement Measurement by Laser Interferometric Probe -Its Mechanism and Applications to Evaluation of Lattice Damage in Semiconductors
journal, November 1992


Studies of High-Frequency Acoustic Phonons Using Picosecond Optical Techniques
book, January 1986