Methods for making lithium vanadium oxide electrode materials

Schutts, Scott M; Kinney, Robert J

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Title: Methods for making lithium vanadium oxide electrode materials

Abstract

A method of making vanadium oxide formulations is presented. In one method of preparing lithium vanadium oxide for use as an electrode material, the method involves: admixing a particulate form of a lithium compound and a particulate form of a vanadium compound; jet milling the particulate admixture of the lithium and vanadium compounds; and heating the jet milled particulate admixture at a temperature below the melting temperature of the admixture to form lithium vanadium oxide.

Inventors:

Schutts, Scott M ^[1]; Kinney, Robert J ^[2]

Menomonie, WI
Woodbury, MN

Issue Date:: Sat Jan 01 00:00:00 EST 2000

Research Org.:: United States Advanced Battery Consortium, Dearborn, MI (US)

OSTI Identifier:: 873330

Patent Number(s):: 6136476

Assignee:: Hydro-Quebec Corporation (Montreal, CA); 3M Innovative Properties Company (St. Paul, MN)

Patent Classifications (CPCs):: C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01G - COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01M - PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY

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C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01G - COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
C01G31/00 - Compounds of vanadium

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01M - PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
H01M4/131 - Electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
H01M4/485 - of mixed oxides or hydroxides for inserting or intercalating light metals, e.g. LiTi2O4 or LiTi2OxFy

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02E - REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
Y02E60/10 - Energy storage

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DOE Contract Number:: FC02-91CE50336

Resource Type:: Patent

Country of Publication:: United States

Language:: English

Subject:: methods; lithium; vanadium; oxide; electrode; materials; method; formulations; preparing; material; involves; admixing; particulate; form; compound; jet; milling; admixture; compounds; heating; milled; temperature; below; melting; oxide electrode; vanadium oxide; melting temperature; temperature below; method involves; electrode material; particulate form; electrode materials; lithium compound; lithium vanadium; method involve; oxide formulations; oxide form; /429/

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                    Schutts, Scott M, and Kinney, Robert J. Methods for making lithium vanadium oxide electrode materials.  United States: N. p., 2000. 
        Web.

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                    Schutts, Scott M, & Kinney, Robert J. Methods for making lithium vanadium oxide electrode materials.  United States.

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                    Schutts, Scott M, and Kinney, Robert J. Sat .  
        "Methods for making lithium vanadium oxide electrode materials".  United States.  https://www.osti.gov/servlets/purl/873330.

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@article{osti_873330,

  title        = {Methods for making lithium vanadium oxide electrode materials},

  author       = {Schutts, Scott M and Kinney, Robert J},

  abstractNote = {A method of making vanadium oxide formulations is presented. In one method of preparing lithium vanadium oxide for use as an electrode material, the method involves: admixing a particulate form of a lithium compound and a particulate form of a vanadium compound; jet milling the particulate admixture of the lithium and vanadium compounds; and heating the jet milled particulate admixture at a temperature below the melting temperature of the admixture to form lithium vanadium oxide.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {Sat Jan 01 00:00:00 EST 2000},

  month        = {Sat Jan 01 00:00:00 EST 2000}

}

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Works referenced in this record:

Study of amorphous and crystalline Li1+xV3O8 by FTIR, XAS and electrochemical techniques
journal, October 1992

Tossici, R.; Marassi, R.; Berrettoni, M.
Solid State Ionics, Vol. 57, Issue 3-4
https://doi.org/10.1016/0167-2738(92)90152-F

Comparison of LiV[sub 3]O[sub 8] Cathode Materials Prepared by Different Methods
journal, January 1996

West, K.
Journal of The Electrochemical Society, Vol. 143, Issue 3
https://doi.org/10.1149/1.1836543

Vanadium oxides as electrode materials for rechargeable lithium cells
journal, May 1987

West, K.; Zachau-Christiansen, B.; Østergård, M. J. L.
Journal of Power Sources, Vol. 20, Issue 1-2
https://doi.org/10.1016/0378-7753(87)80107-6

A Polymeric Electrolyte Rechargeable Lithium Battery
journal, January 1988

Bonino, F.; Ottaviani, M.; Scrosati, B.
Journal of The Electrochemical Society, Vol. 135, Issue 1
https://doi.org/10.1149/1.2095538

The quenching and electrochemical behavior of Li2OV2O5 glasses
journal, June 1981

Nassau, K.; Murphy, D. W.
Journal of Non-Crystalline Solids, Vol. 44, Issue 2-3
https://doi.org/10.1016/0022-3093(81)90032-6

Crystal chemistry of non-stoichiometric pentavalent vandadium oxides: crystal structure of Li1+xV3O8
journal, April 1957

Wadsley, A. D.
Acta Crystallographica, Vol. 10, Issue 4
https://doi.org/10.1107/S0365110X57000821

Structural characterization of Li1+xV3O8 insertion electrodes by single-crystal X-ray diffraction
journal, August 1993

Depicciotto, L.; Adendorff, K.; Liles, D.
Solid State Ionics, Vol. 62, Issue 3-4
https://doi.org/10.1016/0167-2738(93)90386-H

The Role of Ternary Phases in Cathode Reactions
journal, January 1976

Whittingham, M. Stanley
Journal of The Electrochemical Society, Vol. 123, Issue 3
https://doi.org/10.1149/1.2132817

Li∕Li[sub 1+x]V[sub 3]O[sub 8] Batteries
journal, January 1986

Pasquali, M.
Journal of The Electrochemical Society, Vol. 133, Issue 12
https://doi.org/10.1149/1.2108449

All solid state Li-Li1+x V3O8 secondary batteries
journal, December 1988

Hammou, A.; Hammouche, A.
Electrochimica Acta, Vol. 33, Issue 12
https://doi.org/10.1016/0013-4686(88)85005-9

Solid solutions Li1+xV3O8 as cathodes for high rate secondary Li batteries
journal, August 1984

Pistoia, G.
Solid State Ionics, Vol. 13, Issue 4
https://doi.org/10.1016/0167-2738(84)90073-0

Lithium insertion reactions in tungsten and vanadium oxide bronzes
journal, December 1983

Raistrick, I.
Solid State Ionics, Vol. 9-10
https://doi.org/10.1016/0167-2738(83)90270-9

Formation, structure, and topotactic exchange reactions of the layered hydrogen bronze H _x V ₃ O ₈
journal, January 1979

Schöllhorn, Robert; Klein-Reesink, Franz; Reimold, Renate
J. Chem. Soc., Chem. Commun., Issue 9
https://doi.org/10.1039/C39790000398

Rechargeable lithium batteries based on Li1 + xV3O8 thin films
journal, August 1995

Bonino, F.; Panero, S.; Pasquali, M.
Journal of Power Sources, Vol. 56, Issue 2
https://doi.org/10.1016/0378-7753(95)80033-D

Rechargeable Li∕Li[sub 1+x]V[sub 3]O[sub 8] Cells
journal, January 1983

Panero, S.
Journal of The Electrochemical Society, Vol. 130, Issue 5
https://doi.org/10.1149/1.2119923

Li / Li1 + x V 3 O 8 Secondary Batteries: Synthesis and Characterization of an Amorphous Form of the Cathode
journal, August 1990

Pistoia, G.; Pasquali, M.; Wang, G.
Journal of The Electrochemical Society, Vol. 137, Issue 8
https://doi.org/10.1149/1.2086945

Electrode kinetics in poly(ethylene oxide)-based electrolytes
journal, July 1987

Bonino, F.; Ottaviani, M.; Scrosati, B.
Journal of Power Sources, Vol. 20, Issue 3-4
https://doi.org/10.1016/0378-7753(87)80132-5

Li/LiV3O8 polymer electrolyte rechargeable batteries
journal, September 1988

Bonino, F.; Selvaggi, A.; Scrosati, B.
Solid State Ionics, Vol. 28-30
https://doi.org/10.1016/S0167-2738(88)80158-9

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Similar Records

Title: Methods for making lithium vanadium oxide electrode materials

Abstract

Citation Formats

Study of amorphous and crystalline Li1+xV3O8 by FTIR, XAS and electrochemical techniques journal, October 1992

Comparison of LiV[sub 3]O[sub 8] Cathode Materials Prepared by Different Methods journal, January 1996

Vanadium oxides as electrode materials for rechargeable lithium cells journal, May 1987

A Polymeric Electrolyte Rechargeable Lithium Battery journal, January 1988

The quenching and electrochemical behavior of Li2OV2O5 glasses journal, June 1981

Crystal chemistry of non-stoichiometric pentavalent vandadium oxides: crystal structure of Li1+xV3O8 journal, April 1957

Structural characterization of Li1+xV3O8 insertion electrodes by single-crystal X-ray diffraction journal, August 1993

The Role of Ternary Phases in Cathode Reactions journal, January 1976

Li∕Li[sub 1+x]V[sub 3]O[sub 8] Batteries journal, January 1986

All solid state Li-Li1+x V3O8 secondary batteries journal, December 1988

Solid solutions Li1+xV3O8 as cathodes for high rate secondary Li batteries journal, August 1984

Lithium insertion reactions in tungsten and vanadium oxide bronzes journal, December 1983

Formation, structure, and topotactic exchange reactions of the layered hydrogen bronze H x V 3 O 8 journal, January 1979

Rechargeable lithium batteries based on Li1 + xV3O8 thin films journal, August 1995

Rechargeable Li∕Li[sub 1+x]V[sub 3]O[sub 8] Cells journal, January 1983

Li / Li1 + x V 3 O 8 Secondary Batteries: Synthesis and Characterization of an Amorphous Form of the Cathode journal, August 1990

Electrode kinetics in poly(ethylene oxide)-based electrolytes journal, July 1987

Li/LiV3O8 polymer electrolyte rechargeable batteries journal, September 1988

Study of amorphous and crystalline Li1+xV3O8 by FTIR, XAS and electrochemical techniques
journal, October 1992

Comparison of LiV[sub 3]O[sub 8] Cathode Materials Prepared by Different Methods
journal, January 1996

Vanadium oxides as electrode materials for rechargeable lithium cells
journal, May 1987

A Polymeric Electrolyte Rechargeable Lithium Battery
journal, January 1988

The quenching and electrochemical behavior of Li2OV2O5 glasses
journal, June 1981

Crystal chemistry of non-stoichiometric pentavalent vandadium oxides: crystal structure of Li1+xV3O8
journal, April 1957

Structural characterization of Li1+xV3O8 insertion electrodes by single-crystal X-ray diffraction
journal, August 1993

The Role of Ternary Phases in Cathode Reactions
journal, January 1976

Li∕Li[sub 1+x]V[sub 3]O[sub 8] Batteries
journal, January 1986

All solid state Li-Li1+x V3O8 secondary batteries
journal, December 1988

Solid solutions Li1+xV3O8 as cathodes for high rate secondary Li batteries
journal, August 1984

Lithium insertion reactions in tungsten and vanadium oxide bronzes
journal, December 1983

Formation, structure, and topotactic exchange reactions of the layered hydrogen bronze H _x V ₃ O ₈
journal, January 1979

Rechargeable lithium batteries based on Li1 + xV3O8 thin films
journal, August 1995

Rechargeable Li∕Li[sub 1+x]V[sub 3]O[sub 8] Cells
journal, January 1983

Li / Li1 + x V 3 O 8 Secondary Batteries: Synthesis and Characterization of an Amorphous Form of the Cathode
journal, August 1990

Electrode kinetics in poly(ethylene oxide)-based electrolytes
journal, July 1987

Li/LiV3O8 polymer electrolyte rechargeable batteries
journal, September 1988