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Title: Systems and methods for the combinatorial synthesis of novel materials

Abstract

Methods and apparatus for the preparation of a substrate having an array of diverse materials in predefined regions thereon. A substrate having an array of diverse materials thereon is generally prepared by depositing components of target materials to predefined regions on the substrate, and, in some embodiments, simultaneously reacting the components to form at least two resulting materials. In particular, the present invention provides novel masking systems and methods for applying components of target materials onto a substrate in a combinatorial fashion, thus creating arrays of resulting materials that differ slightly in composition, stoichiometry, and/or thickness. Using the novel masking systems of the present invention, components can be delivered to each site in a uniform distribution, or in a gradient of stoichiometries, thicknesses, compositions, etc. Resulting materials which can be prepared using the methods and apparatus of the present invention include, for example, covalent network solids, ionic solids and molecular solids. Once prepared, these resulting materials can be screened sequentially, or in parallel, for useful properties including, for example, electrical, thermal, mechanical, morphological, optical, magnetic, chemical and other properties.

Inventors:
 [1];  [2];  [3]
  1. San Jose, CA
  2. Palo Alto, CA
  3. Menlo Park, CA
Issue Date:
Research Org.:
Lawrence Berkeley National Laboratory (LBNL), Berkeley, CA (United States)
OSTI Identifier:
872933
Patent Number(s):
6045671
Assignee:
Symyx Technologies, Inc. (Santa Clara, CA)
Patent Classifications (CPCs):
B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B - PERFORMING OPERATIONS B82 - NANOTECHNOLOGY B82Y - SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES
DOE Contract Number:  
AC03-76SF00098
Resource Type:
Patent
Country of Publication:
United States
Language:
English
Subject:
systems; methods; combinatorial; synthesis; novel; materials; apparatus; preparation; substrate; array; diverse; predefined; regions; thereon; prepared; depositing; components; target; embodiments; simultaneously; reacting; form; resulting; particular; provides; masking; applying; fashion; creating; arrays; slightly; composition; stoichiometry; thickness; delivered; site; uniform; distribution; gradient; stoichiometries; thicknesses; compositions; etc; example; covalent; network; solids; ionic; molecular; screened; sequentially; parallel; useful; properties; including; electrical; thermal; mechanical; morphological; optical; magnetic; chemical; materials thereon; target material; provides novel; predefined regions; diverse materials; novel materials; properties including; uniform distribution; useful properties; resulting material; combinatorial synthesis; simultaneously reacting; regions thereon; molecular solids; network solids; target materials; covalent network; ionic solids; target mater; /204/118/

Citation Formats

Wu, Xin Di, Wang, Youqi, and Goldwasser, Isy. Systems and methods for the combinatorial synthesis of novel materials. United States: N. p., 2000. Web.
Wu, Xin Di, Wang, Youqi, & Goldwasser, Isy. Systems and methods for the combinatorial synthesis of novel materials. United States.
Wu, Xin Di, Wang, Youqi, and Goldwasser, Isy. Sat . "Systems and methods for the combinatorial synthesis of novel materials". United States. https://www.osti.gov/servlets/purl/872933.
@article{osti_872933,
title = {Systems and methods for the combinatorial synthesis of novel materials},
author = {Wu, Xin Di and Wang, Youqi and Goldwasser, Isy},
abstractNote = {Methods and apparatus for the preparation of a substrate having an array of diverse materials in predefined regions thereon. A substrate having an array of diverse materials thereon is generally prepared by depositing components of target materials to predefined regions on the substrate, and, in some embodiments, simultaneously reacting the components to form at least two resulting materials. In particular, the present invention provides novel masking systems and methods for applying components of target materials onto a substrate in a combinatorial fashion, thus creating arrays of resulting materials that differ slightly in composition, stoichiometry, and/or thickness. Using the novel masking systems of the present invention, components can be delivered to each site in a uniform distribution, or in a gradient of stoichiometries, thicknesses, compositions, etc. Resulting materials which can be prepared using the methods and apparatus of the present invention include, for example, covalent network solids, ionic solids and molecular solids. Once prepared, these resulting materials can be screened sequentially, or in parallel, for useful properties including, for example, electrical, thermal, mechanical, morphological, optical, magnetic, chemical and other properties.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Sat Jan 01 00:00:00 EST 2000},
month = {Sat Jan 01 00:00:00 EST 2000}
}

Works referenced in this record:

Electroluminescence in ZnS: Mn x : Cu y rf–Sputtered Films
journal, January 1974


Calculation of composition of dilute cosputtered multicomponent films
journal, November 1973


Compositional Determination of rf Co-Sputtered Multicomponent Systems
journal, January 1971


The effect of grain size on the superconducting transition temperature of the transition metals
journal, October 1969


Radio‐Frequency‐Sputtered Films of β‐Tungsten Structure Compounds
journal, November 1970