Method of producing ternary lead molybdenum sulfides
Abstract
The method of preparing Pb.sub.x Mo.sub.y S.sub.z where x = 0.8-1.1, y = 4.5-5.6, and z = 5.4-7.2 comprising the steps of mixing commercial reagent grade powders of the reactants, heating in a sealed, evacuated reaction vessel to a temperature of 950.degree.-1150.degree. C, maintaining the temperature until the compound is formed, and then cooling the compound at a controlled rate not in excess of 4.degree. C per minute.
- Inventors:
-
- Belmont, MA
- (Danvers, MA)
- Danvers, MA
- Issue Date:
- OSTI Identifier:
- 862762
- Patent Number(s):
- 4006107
- Application Number:
- 05/604,384
- Assignee:
- United States of America as represented by United States Energy (Washington, DC)
- Patent Classifications (CPCs):
-
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01G - COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y10 - TECHNICAL SUBJECTS COVERED BY FORMER USPC Y10S - TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Resource Type:
- Patent
- Country of Publication:
- United States
- Language:
- English
- Subject:
- method; producing; ternary; lead; molybdenum; sulfides; preparing; pb; z; 8-1; 5-5; 4-7; comprising; steps; mixing; commercial; reagent; grade; powders; reactants; heating; sealed; evacuated; reaction; vessel; temperature; 950; degree; -1150; maintaining; compound; formed; cooling; controlled; rate; excess; minute; controlled rate; reaction vessel; molybdenum sulfide; molybdenum sulfides; /252/423/505/
Citation Formats
Foner, Simon, McNiff, Jr., Edward J., and Alexander, Edwin J. Method of producing ternary lead molybdenum sulfides. United States: N. p., 1977.
Web.
Foner, Simon, McNiff, Jr., Edward J., & Alexander, Edwin J. Method of producing ternary lead molybdenum sulfides. United States.
Foner, Simon, McNiff, Jr., Edward J., and Alexander, Edwin J. Tue .
"Method of producing ternary lead molybdenum sulfides". United States. https://www.osti.gov/servlets/purl/862762.
@article{osti_862762,
title = {Method of producing ternary lead molybdenum sulfides},
author = {Foner, Simon and McNiff, Jr., Edward J. and Alexander, Edwin J},
abstractNote = {The method of preparing Pb.sub.x Mo.sub.y S.sub.z where x = 0.8-1.1, y = 4.5-5.6, and z = 5.4-7.2 comprising the steps of mixing commercial reagent grade powders of the reactants, heating in a sealed, evacuated reaction vessel to a temperature of 950.degree.-1150.degree. C, maintaining the temperature until the compound is formed, and then cooling the compound at a controlled rate not in excess of 4.degree. C per minute.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue Feb 01 00:00:00 EST 1977},
month = {Tue Feb 01 00:00:00 EST 1977}
}
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