Enhanced spot preparation for liquid extractive sampling and analysis
Abstract
A method for performing surface sampling of an analyte, includes the step of placing the analyte on a stage with a material in molar excess to the analyte, such that analyte-analyte interactions are prevented and the analyte can be solubilized for further analysis. The material can be a matrix material that is mixed with the analyte. The material can be provided on a sample support. The analyte can then be contacted with a solvent to extract the analyte for further processing, such as by electrospray mass spectrometry.
- Inventors:
- Issue Date:
- Research Org.:
- Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 1215631
- Patent Number(s):
- 9140633
- Application Number:
- 13/488,141
- Assignee:
- UT-Battelle, LLC (Oak Ridge, TN)
- Patent Classifications (CPCs):
-
G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01J - ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- DOE Contract Number:
- AC05-00OR22725
- Resource Type:
- Patent
- Resource Relation:
- Patent File Date: 2012 Jun 04
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
Citation Formats
Van Berkel, Gary J., and King, Richard C. Enhanced spot preparation for liquid extractive sampling and analysis. United States: N. p., 2015.
Web.
Van Berkel, Gary J., & King, Richard C. Enhanced spot preparation for liquid extractive sampling and analysis. United States.
Van Berkel, Gary J., and King, Richard C. Tue .
"Enhanced spot preparation for liquid extractive sampling and analysis". United States. https://www.osti.gov/servlets/purl/1215631.
@article{osti_1215631,
title = {Enhanced spot preparation for liquid extractive sampling and analysis},
author = {Van Berkel, Gary J. and King, Richard C.},
abstractNote = {A method for performing surface sampling of an analyte, includes the step of placing the analyte on a stage with a material in molar excess to the analyte, such that analyte-analyte interactions are prevented and the analyte can be solubilized for further analysis. The material can be a matrix material that is mixed with the analyte. The material can be provided on a sample support. The analyte can then be contacted with a solvent to extract the analyte for further processing, such as by electrospray mass spectrometry.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue Sep 22 00:00:00 EDT 2015},
month = {Tue Sep 22 00:00:00 EDT 2015}
}
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