Microporous crystals and synthesis schemes
Abstract
Novel zeolites are produced by combining a polar solute, a silicon or phosphorous source, and a structure directing agent. Surfactants and a hydrophobic solvent are added to the previously mixed three species and shaken to disperse the surfactants. The reverse microemulsion is stirred overnight, at about room temperature and then iced for five to ten minutes. A metal source is added vigorously shaken for about two minutes. The mixture is then aged for about two hours at about room temperature. A mineralizer is added and the resultant mixture aged for about two hours at about room temperature. The mixture is heated to about 180.degree. C., for a suitable time period. The final novel product is then isolated.
- Inventors:
- Issue Date:
- Research Org.:
- Univ. of California, Oakland, CA (United States)
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 1175508
- Patent Number(s):
- 6949238
- Application Number:
- 10/360,544
- Assignee:
- The Regents of the University of California (Oakland, CA)
- Patent Classifications (CPCs):
-
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y10 - TECHNICAL SUBJECTS COVERED BY FORMER USPC Y10S - TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- DOE Contract Number:
- W-7405 ENG-36
- Resource Type:
- Patent
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
Citation Formats
Tumas, William, Ott, Kevin C., McCleskey, T. Mark, Yates, Matthew Z., and Birnbaum, Eva R. Microporous crystals and synthesis schemes. United States: N. p., 2005.
Web.
Tumas, William, Ott, Kevin C., McCleskey, T. Mark, Yates, Matthew Z., & Birnbaum, Eva R. Microporous crystals and synthesis schemes. United States.
Tumas, William, Ott, Kevin C., McCleskey, T. Mark, Yates, Matthew Z., and Birnbaum, Eva R. Tue .
"Microporous crystals and synthesis schemes". United States. https://www.osti.gov/servlets/purl/1175508.
@article{osti_1175508,
title = {Microporous crystals and synthesis schemes},
author = {Tumas, William and Ott, Kevin C. and McCleskey, T. Mark and Yates, Matthew Z. and Birnbaum, Eva R.},
abstractNote = {Novel zeolites are produced by combining a polar solute, a silicon or phosphorous source, and a structure directing agent. Surfactants and a hydrophobic solvent are added to the previously mixed three species and shaken to disperse the surfactants. The reverse microemulsion is stirred overnight, at about room temperature and then iced for five to ten minutes. A metal source is added vigorously shaken for about two minutes. The mixture is then aged for about two hours at about room temperature. A mineralizer is added and the resultant mixture aged for about two hours at about room temperature. The mixture is heated to about 180.degree. C., for a suitable time period. The final novel product is then isolated.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue Sep 27 00:00:00 EDT 2005},
month = {Tue Sep 27 00:00:00 EDT 2005}
}
Works referenced in this record:
Hydrothermal Synthesis of Molecular Sieve Fibers: Using Microemulsions To Control Crystal Morphology
journal, January 2002
- Yates, Matthew Z.; Ott, Kevin C.; Birnbaum, Eva R.
- Angewandte Chemie International Edition, Vol. 41, Issue 3, p. 476-478