Titanate and titania nanostructures and nanostructure assemblies, and methods of making same

Wong, Stanislaus S; Mao, Yuanbing

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A - human necessities
A01 - agriculture
A21 - baking
A22 - butchering
A23 - foods or foodstuffs
A24 - tobacco
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A42 - headwear
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A44 - haberdashery
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A46 - brushware
A47 - furniture
A61 - medical or veterinary science
A62 - life-saving
A63 - sports
A99 - subject matter not otherwise provided for in this section
B - performing operations
B01 - physical or chemical processes or apparatus in general
B02 - crushing, pulverising, or disintegrating
B03 - separation of solid materials using liquids or using pneumatic tables or jigs
B04 - centrifugal apparatus or machines for carrying-out physical or chemical processes
B05 - spraying or atomising in general
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Title: Titanate and titania nanostructures and nanostructure assemblies, and methods of making same

Abstract

The invention relates to nanomaterials and assemblies including, a micrometer-scale spherical aggregate comprising: a plurality of one-dimensional nanostructures comprising titanium and oxygen, wherein the one-dimensional nanostructures radiate from a hollow central core thereby forming a spherical aggregate.

Inventors:: Wong, Stanislaus S; Mao, Yuanbing

Issue Date:: Tue May 14 00:00:00 EDT 2013

Research Org.:: Brookhaven National Laboratory (BNL), Upton, NY (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1084069

Patent Number(s):: 8440162

Application Number:: 12/004,105

Assignee:: The Research Foundation of State University of New York (Albany, NY)

Patent Classifications (CPCs):: B - PERFORMING OPERATIONS B32 - LAYERED PRODUCTS B32B - LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM

B - PERFORMING OPERATIONS B82 - NANOTECHNOLOGY B82Y - SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES

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B - PERFORMING OPERATIONS B32 - LAYERED PRODUCTS B32B - LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
B32B18/00 - Layered products essentially comprising ceramics, e.g. refractory products
B32B2311/18 - Titanium

B - PERFORMING OPERATIONS B82 - NANOTECHNOLOGY B82Y - SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES
B82Y30/00 - Nanotechnology for materials or surface science, e.g. nanocomposites
B82Y40/00 - Manufacture or treatment of nanostructures

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C01B3/0026 - {of one single metal or a rare earth metal
C01B3/0031 - {Intermetallic compounds
C01B6/02 - Hydrides of transition elements
C01B6/24 - Hydrides containing at least two metals

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01D - COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
C01D13/00 - Compounds of sodium or potassium not provided for elsewhere

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01G - COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
C01G23/003 - {Titanates
C01G23/005 - {Alkali titanates}
C01G23/04 - Oxides
C01G23/043 - {Titanium sub-oxides}
C01G23/047 - Titanium dioxide
C01G23/08 - Drying

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01P - INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
C01P2002/72 - by d-values or two theta-values, e.g. as X-ray diagram
C01P2002/82 - by IR- or Raman-data
C01P2002/84 - by UV- or VIS- data
C01P2002/85 - by XPS, EDX or EDAX data
C01P2004/03 - obtained by SEM
C01P2004/04 - obtained by TEM, STEM, STM or AFM
C01P2004/10 - extending in one dimension, e.g. needle-like
C01P2004/13 - Nanotubes
C01P2004/16 - Nanowires or nanorods, i.e. solid nanofibres with two nearly equal dimensions between 1-100 nanometer
C01P2004/32 - Spheres
C01P2004/34 - hollow
C01P2004/50 - Agglomerated particles
C01P2004/61 - Micrometer sized, i.e. from 1-100 micrometer
C01P2004/62 - Submicrometer sized, i.e. from 0.1-1 micrometer
C01P2004/64 - Nanometer sized, i.e. from 1-100 nanometer

C - CHEMISTRY C04 - CEMENTS C04B - LIME, MAGNESIA
C04B2235/404 - Refractory metals
C04B2235/5264 - characterised by the diameter of the fibers
C04B2235/5284 - Hollow fibers, e.g. nanotubes
C04B35/62259 - {Fibres based on titanium oxide}

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02E - REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
Y02E60/32 - Hydrogen storage

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y10 - TECHNICAL SUBJECTS COVERED BY FORMER USPC Y10S - TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
Y10S977/762 - Nanowire or quantum wire, i.e. axially elongated structure having two dimensions of 100 nm or less
Y10S977/773 - Nanoparticle, i.e. structure having three dimensions of 100 nm or less
Y10S977/811 - Of specified metal oxide composition, e.g. conducting or semiconducting compositions such as ITO, ZnOx
Y10S977/896 - Chemical synthesis, e.g. chemical bonding or breaking

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y10 - TECHNICAL SUBJECTS COVERED BY FORMER USPC Y10T - TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
Y10T428/24058 - including grain, strips, or filamentary elements in respective layers or components in angular relation
Y10T428/298 - Physical dimension

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DOE Contract Number:: AC02-98CH10886

Resource Type:: Patent

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE

Citation Formats


                    Wong, Stanislaus S, and Mao, Yuanbing. Titanate and titania nanostructures and nanostructure assemblies, and methods of making same.  United States: N. p., 2013. 
        Web.

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                    Wong, Stanislaus S, & Mao, Yuanbing. Titanate and titania nanostructures and nanostructure assemblies, and methods of making same.  United States.

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                    Wong, Stanislaus S, and Mao, Yuanbing. Tue .  
        "Titanate and titania nanostructures and nanostructure assemblies, and methods of making same".  United States.  https://www.osti.gov/servlets/purl/1084069.

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@article{osti_1084069,

  title        = {Titanate and titania nanostructures and nanostructure assemblies, and methods of making same},

  author       = {Wong, Stanislaus S and Mao, Yuanbing},

  abstractNote = {The invention relates to nanomaterials and assemblies including, a micrometer-scale spherical aggregate comprising: a plurality of one-dimensional nanostructures comprising titanium and oxygen, wherein the one-dimensional nanostructures radiate from a hollow central core thereby forming a spherical aggregate.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {Tue May 14 00:00:00 EDT 2013},

  month        = {Tue May 14 00:00:00 EDT 2013}

}

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Works referenced in this record:

Synthesis of Crystal-Axis-Oriented BaTiO ₃ and Anatase Platelike Particles by a Hydrothermal Soft Chemical Process
journal, February 2001

Feng, Qi; Hirasawa, Manabu; Yanagisawa, Kazumichi
Chemistry of Materials, Vol. 13, Issue 2
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The effect of hydrothermal conditions on the mesoporous structure of TiO2 nanotubes
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Bavykin, Dmitry V.; Parmon, Valentin N.; Lapkin, Alexei A.
Journal of Materials Chemistry, Vol. 14, Issue 22
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Enhanced Catalytic Activity of Hemoglobin in Organic Solvents by Layered Titanate Immobilization
journal, November 2004

Wang, Qigang; Gao, Qiuming; Shi, Jianlin
Journal of the American Chemical Society, Vol. 126, Issue 44
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Extreme Changes in the Electrical Resistance of Titania Nanotubes with Hydrogen Exposure
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Preparing Single-Phase Nanocrystalline Anatase from Amorphous Titania with Particle Sizes Tailored by Temperature
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Zhang, Hengzhong; Finnegan, Michael; Banfield, Jillian F.
Nano Letters, Vol. 1, Issue 2
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Strong Room-Temperature Ferromagnetism in Co ²⁺ -Doped TiO ₂ Made from Colloidal Nanocrystals
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Journal of the American Chemical Society, Vol. 126, Issue 37
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Chemistry and Properties of Nanocrystals of Different Shapes
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Burda, Clemens; Chen, Xiaobo; Narayanan, Radha
Chemical Reviews, Vol. 105, Issue 4
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Low-temperature preparation of titania nanorods through direct oxidation of titanium with hydrogen peroxide
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Li, Guangshe; Li, Liping; Boerio-Goates, Juliana
Journal of the American Chemical Society, Vol. 127, Issue 24
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Synthesis and Growth Mechanism of Titanate and Titania One-Dimensional Nanostructures Self-Assembled into Hollow Micrometer-Scale Spherical Aggregates
journal, January 2006

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Photosensitization of ion-exchangeable titanate nanotubes by CdS nanoparticles
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Similar Records

Title: Titanate and titania nanostructures and nanostructure assemblies, and methods of making same

Abstract

Citation Formats

Synthesis of Crystal-Axis-Oriented BaTiO 3 and Anatase Platelike Particles by a Hydrothermal Soft Chemical Process journal, February 2001

The effect of hydrothermal conditions on the mesoporous structure of TiO2 nanotubes journal, January 2004

Enhanced Catalytic Activity of Hemoglobin in Organic Solvents by Layered Titanate Immobilization journal, November 2004

Extreme Changes in the Electrical Resistance of Titania Nanotubes with Hydrogen Exposure journal, April 2003

Preparing Single-Phase Nanocrystalline Anatase from Amorphous Titania with Particle Sizes Tailored by Temperature journal, February 2001

Strong Room-Temperature Ferromagnetism in Co 2+ -Doped TiO 2 Made from Colloidal Nanocrystals journal, September 2004

Chemistry and Properties of Nanocrystals of Different Shapes journal, April 2005

Low-temperature preparation of titania nanorods through direct oxidation of titanium with hydrogen peroxide journal, September 2004

Cation Exchange Reactions in Ionic Nanocrystals journal, November 2004

High Purity Anatase TiO 2 Nanocrystals: Near Room-Temperature Synthesis, Grain Growth Kinetics, and Surface Hydration Chemistry journal, June 2005

Synthesis and Growth Mechanism of Titanate and Titania One-Dimensional Nanostructures Self-Assembled into Hollow Micrometer-Scale Spherical Aggregates journal, January 2006

Large Oriented Arrays and Continuous Films of TiO 2 -Based Nanotubes journal, October 2003

Photosensitization of ion-exchangeable titanate nanotubes by CdS nanoparticles journal, December 2004

Syntheses of TiO2(B) nanowires and TiO2 anatase nanowires by hydrothermal and post-heat treatments journal, July 2005

Growth and mechanism of titania nanowires journal, June 2003

Environmental Applications of Semiconductor Photocatalysis journal, January 1995

TiO2-B Nanowires journal, April 2004

Structural Features of Titanate Nanotubes/Nanobelts Revealed by Raman, X-ray Absorption Fine Structure and Electron Diffraction Characterizations journal, April 2005

Characterization of a New Potassium Titanate, KTiO 2 (OH) Synthesized via Hydrothermal Method journal, January 2002

Synthesis of Crystal-Axis-Oriented BaTiO ₃ and Anatase Platelike Particles by a Hydrothermal Soft Chemical Process
journal, February 2001

The effect of hydrothermal conditions on the mesoporous structure of TiO2 nanotubes
journal, January 2004

Enhanced Catalytic Activity of Hemoglobin in Organic Solvents by Layered Titanate Immobilization
journal, November 2004

Extreme Changes in the Electrical Resistance of Titania Nanotubes with Hydrogen Exposure
journal, April 2003

Preparing Single-Phase Nanocrystalline Anatase from Amorphous Titania with Particle Sizes Tailored by Temperature
journal, February 2001

Strong Room-Temperature Ferromagnetism in Co ²⁺ -Doped TiO ₂ Made from Colloidal Nanocrystals
journal, September 2004

Chemistry and Properties of Nanocrystals of Different Shapes
journal, April 2005

Low-temperature preparation of titania nanorods through direct oxidation of titanium with hydrogen peroxide
journal, September 2004

Cation Exchange Reactions in Ionic Nanocrystals
journal, November 2004

High Purity Anatase TiO ₂ Nanocrystals: Near Room-Temperature Synthesis, Grain Growth Kinetics, and Surface Hydration Chemistry
journal, June 2005

Synthesis and Growth Mechanism of Titanate and Titania One-Dimensional Nanostructures Self-Assembled into Hollow Micrometer-Scale Spherical Aggregates
journal, January 2006

Large Oriented Arrays and Continuous Films of TiO ₂ -Based Nanotubes
journal, October 2003

Photosensitization of ion-exchangeable titanate nanotubes by CdS nanoparticles
journal, December 2004

Syntheses of TiO₂(B) nanowires and TiO₂ anatase nanowires by hydrothermal and post-heat treatments
journal, July 2005

Growth and mechanism of titania nanowires
journal, June 2003

Environmental Applications of Semiconductor Photocatalysis
journal, January 1995

TiO₂-B Nanowires
journal, April 2004

Structural Features of Titanate Nanotubes/Nanobelts Revealed by Raman, X-ray Absorption Fine Structure and Electron Diffraction Characterizations
journal, April 2005

Characterization of a New Potassium Titanate, KTiO ₂ (OH) Synthesized via Hydrothermal Method
journal, January 2002