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Title: Microporous crystals and synthesis schemes

Abstract

Novel zeolites are produced by combining a polar solute, a silicon or phosphorous source, and a structure directing agent. Surfactants and a hydrophobic solvent are added to the previously mixed three species and shaken to disperse the surfactants. The reverse microemulsion is stirred overnight, at about room temperature and then iced for five to ten minutes. A metal source is added vigorously shaken for about two minutes. The mixture is then aged for about two hours at about room temperature. A mineralizer is added and the resultant mixture aged for about two hours at about room temperature. The mixture is heated to about 180.degree. C., for a suitable time period. The final novel product is then isolated.

Inventors:
 [1];  [1];  [1];  [2];  [1]
  1. Los Alamos, NM
  2. Penfield, NY
Issue Date:
Research Org.:
Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
958679
Patent Number(s):
7361327
Application Number:
11/206,330
Assignee:
Los Alamos National Security, LLC (Los Alamos, NM)
Patent Classifications (CPCs):
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y10 - TECHNICAL SUBJECTS COVERED BY FORMER USPC Y10S - TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
DOE Contract Number:  
W-7405 ENG-36
Resource Type:
Patent
Country of Publication:
United States
Language:
English

Citation Formats

Tumas, William, Ott, Kevin C, McCleskey, T Mark, Yates, Matthew Z, and Birnbaum, Eva R. Microporous crystals and synthesis schemes. United States: N. p., 2008. Web.
Tumas, William, Ott, Kevin C, McCleskey, T Mark, Yates, Matthew Z, & Birnbaum, Eva R. Microporous crystals and synthesis schemes. United States.
Tumas, William, Ott, Kevin C, McCleskey, T Mark, Yates, Matthew Z, and Birnbaum, Eva R. Tue . "Microporous crystals and synthesis schemes". United States. https://www.osti.gov/servlets/purl/958679.
@article{osti_958679,
title = {Microporous crystals and synthesis schemes},
author = {Tumas, William and Ott, Kevin C and McCleskey, T Mark and Yates, Matthew Z and Birnbaum, Eva R},
abstractNote = {Novel zeolites are produced by combining a polar solute, a silicon or phosphorous source, and a structure directing agent. Surfactants and a hydrophobic solvent are added to the previously mixed three species and shaken to disperse the surfactants. The reverse microemulsion is stirred overnight, at about room temperature and then iced for five to ten minutes. A metal source is added vigorously shaken for about two minutes. The mixture is then aged for about two hours at about room temperature. A mineralizer is added and the resultant mixture aged for about two hours at about room temperature. The mixture is heated to about 180.degree. C., for a suitable time period. The final novel product is then isolated.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2008},
month = {4}
}

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