Reactive decontamination formulation

Giletto, Anthony; White, William; Cisar, Alan J; Hitchens, G Duncan; Fyffe, James

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A - human necessities
A01 - agriculture
A21 - baking
A22 - butchering
A23 - foods or foodstuffs
A24 - tobacco
A41 - wearing apparel
A42 - headwear
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A44 - haberdashery
A45 - hand or travelling articles
A46 - brushware
A47 - furniture
A61 - medical or veterinary science
A62 - life-saving
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A99 - subject matter not otherwise provided for in this section
B - performing operations
B01 - physical or chemical processes or apparatus in general
B02 - crushing, pulverising, or disintegrating
B03 - separation of solid materials using liquids or using pneumatic tables or jigs
B04 - centrifugal apparatus or machines for carrying-out physical or chemical processes
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B62 - land vehicles for travelling otherwise than on rails
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C01 - inorganic chemistry
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Title: Reactive decontamination formulation

Abstract

The present invention provides a universal decontamination formulation and method for detoxifying chemical warfare agents (CWA's) and biological warfare agents (BWA's) without producing any toxic by-products, as well as, decontaminating surfaces that have come into contact with these agents. The formulation includes a sorbent material or gel, a peroxide source, a peroxide activator, and a compound containing a mixture of KHSO.sub.5, KHSO.sub.4 and K.sub.2 SO.sub.4. The formulation is self-decontaminating and once dried can easily be wiped from the surface being decontaminated. A method for decontaminating a surface exposed to chemical or biological agents is also disclosed.

Inventors:

Giletto, Anthony ^[1]; White, William ^[1]; Cisar, Alan J ^[2]; Hitchens, G Duncan ^[3]; Fyffe, James ^[3]

College Station, TX
Cypress, TX
Bryan, TX

Issue Date:: 2003-05-27

Research Org.:: Lynntech, Inc. (College Station, TX)

Sponsoring Org.:: USDOE

OSTI Identifier:: 921890

Patent Number(s):: 6569353

Application Number:: 09/096,435

Assignee:: Lynntech, Inc. (College Station, TX)

Patent Classifications (CPCs):: A - HUMAN NECESSITIES A61 - MEDICAL OR VETERINARY SCIENCE A61K - PREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES

A - HUMAN NECESSITIES A61 - MEDICAL OR VETERINARY SCIENCE A61Q - SPECIFIC USE OF COSMETICS OR SIMILAR TOILET PREPARATIONS

Show more

A - HUMAN NECESSITIES A61 - MEDICAL OR VETERINARY SCIENCE A61K - PREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
A61K8/25 - Silicon
A61K8/46 - containing sulfur

A - HUMAN NECESSITIES A61 - MEDICAL OR VETERINARY SCIENCE A61Q - SPECIFIC USE OF COSMETICS OR SIMILAR TOILET PREPARATIONS
A61Q17/00 - Barrier preparations

A - HUMAN NECESSITIES A62 - LIFE-SAVING A62D - CHEMICAL MEANS FOR EXTINGUISHING FIRES OR FOR COMBATING OR PROTECTING AGAINST HARMFUL CHEMICAL AGENTS
A62D2101/02 - Chemical warfare substances, e.g. cholinesterase inhibitors
A62D3/38 - by oxidation

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J20/06 - comprising oxides or hydroxides of metals not provided for in group B01J20/04
B01J20/08 - comprising aluminium oxide or hydroxide
B01J20/103 - {comprising silica}

Show less

DOE Contract Number:: FG03-97ER82420

Resource Type:: Patent

Country of Publication:: United States

Language:: English

Subject:: 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY

Citation Formats


                    Giletto, Anthony, White, William, Cisar, Alan J, Hitchens, G Duncan, and Fyffe, James. Reactive decontamination formulation.  United States: N. p., 2003. 
        Web.

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                    Giletto, Anthony, White, William, Cisar, Alan J, Hitchens, G Duncan, & Fyffe, James. Reactive decontamination formulation.  United States.

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                    Giletto, Anthony, White, William, Cisar, Alan J, Hitchens, G Duncan, and Fyffe, James. Tue .  
        "Reactive decontamination formulation".  United States.  https://www.osti.gov/servlets/purl/921890.

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@article{osti_921890,

  title        = {Reactive decontamination formulation},

  author       = {Giletto, Anthony and White, William and Cisar, Alan J and Hitchens, G Duncan and Fyffe, James},

  abstractNote = {The present invention provides a universal decontamination formulation and method for detoxifying chemical warfare agents (CWA's) and biological warfare agents (BWA's) without producing any toxic by-products, as well as, decontaminating surfaces that have come into contact with these agents. The formulation includes a sorbent material or gel, a peroxide source, a peroxide activator, and a compound containing a mixture of KHSO.sub.5, KHSO.sub.4 and K.sub.2 SO.sub.4. The formulation is self-decontaminating and once dried can easily be wiped from the surface being decontaminated. A method for decontaminating a surface exposed to chemical or biological agents is also disclosed.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2003},

  month        = {5}

}

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Works referenced in this record:

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Kolthoff, I. M.; Medalia, A. I.
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Opportunities and Challenges in the Application of Ozone in Food Processing
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Fenton Chemistry: An Introduction
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Radiation Research, Vol. 145, Issue 5
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The effect of sulfur mustard and nitrogen mustard on corneal collagen degradation induced by the enzyme collagenase
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Naderi, Mostafa; Jadidi, Khosro; Falahati, Farzaneh
Cutaneous and Ocular Toxicology, Vol. 29, Issue 4
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The effects of Fenton's reagent pretreatment on the biodegradability of nonionic surfactants
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Kitis, M.; Adams, C. D.; Daigger, G. T.
Water Research, Vol. 33, Issue 11
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Oxidative Degradation of Polyvinyl Alcohol by the Photochemically Enhanced Fenton Reaction. Evidence for the Formation of Super-Macromolecules
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Bossmann, Stefan H.; Oliveros, Esther; Göb, Sabine
Progress in Reaction Kinetics and Mechanism, Vol. 26, Issue 2-3
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Recent Advances in Biosensor Technology for Potential Applications – An Overview
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Vigneshvar, S.; Sudhakumari, C. C.; Senthilkumaran, Balasubramanian
Frontiers in Bioengineering and Biotechnology, Vol. 4
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Pathways for Extracellular Fenton Chemistry in the Brown Rot Basidiomycete Gloeophyllum trabeum
journal, June 2001

Jensen, K. A.; Houtman, C. J.; Ryan, Z. C.
Applied and Environmental Microbiology, Vol. 67, Issue 6
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Detection of chemical warfare agents using nanostructured metal oxide sensors
journal, July 2005

Tomchenko, Alexey A.; Harmer, Gregory P.; Marquis, Brent T.
Sensors and Actuators B: Chemical, Vol. 108, Issue 1-2
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Operating characteristics and kinetic studies of surfactant wastewater treatment by Fenton oxidation
journal, May 1999

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Oxidative degradation of poly vinyl alcohol by the photochemically enhanced Fenton reaction
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Lei, Lecheng; Hu, Xijun; Yue, Po Lock
Journal of Photochemistry and Photobiology A: Chemistry, Vol. 116, Issue 2
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Pyridinium Oximes as Cholinesterase Reactivators. Structure-Activity Relationship and Efficacy in the Treatment of Poisoning with Organophosphorus Compounds
journal, June 2009

Jokanovic, Milan; Prostran, Milica
Current Medicinal Chemistry, Vol. 16, Issue 17
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Overview of URBAN 2000: A Multiscale Field Study of Dispersion through an Urban Environment
journal, April 2002

Allwine, K. J.; Shinn, J. H.; Streit, G. E.
Bulletin of the American Meteorological Society, Vol. 83, Issue 4, p. 521-536
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Oxidative degradation of dyes and surfactant in the Fenton and photo-Fenton treatment of dyehouse effluents
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journal, December 1992

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Chemical Reviews, Vol. 92, Issue 8
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Similar Records

Title: Reactive decontamination formulation

Abstract

Citation Formats

The Reaction between Ferrous Iron and Peroxides. I. Reaction with Hydrogen Peroxide in the Absence of Oxygen journal, November 1949

Opportunities and Challenges in the Application of Ozone in Food Processing book, January 2014

Fenton Chemistry: An Introduction journal, May 1996

The effect of sulfur mustard and nitrogen mustard on corneal collagen degradation induced by the enzyme collagenase journal, June 2010

The effects of Fenton's reagent pretreatment on the biodegradability of nonionic surfactants journal, August 1999

Oxidative Degradation of Polyvinyl Alcohol by the Photochemically Enhanced Fenton Reaction. Evidence for the Formation of Super-Macromolecules journal, June 2001

Recent Advances in Biosensor Technology for Potential Applications – An Overview journal, February 2016

Pathways for Extracellular Fenton Chemistry in the Brown Rot Basidiomycete Gloeophyllum trabeum journal, June 2001

Detection of chemical warfare agents using nanostructured metal oxide sensors journal, July 2005

Operating characteristics and kinetic studies of surfactant wastewater treatment by Fenton oxidation journal, May 1999

Oxidative degradation of poly vinyl alcohol by the photochemically enhanced Fenton reaction journal, July 1998

Pyridinium Oximes as Cholinesterase Reactivators. Structure-Activity Relationship and Efficacy in the Treatment of Poisoning with Organophosphorus Compounds journal, June 2009

Overview of URBAN 2000: A Multiscale Field Study of Dispersion through an Urban Environment journal, April 2002

Oxidative degradation of dyes and surfactant in the Fenton and photo-Fenton treatment of dyehouse effluents journal, May 2000

Introduction book, January 1996

Chemical warfare agents journal, January 2010

Oxidation of alcohols by Fenton's reagent. Effect of copper ion journal, August 1971

Biodegradative mechanism of the brown rot basidiomycete Gloeophyllum trabeum : evidence for an extracellular hydroquinone-driven fenton reaction journal, March 1999

Enhanced Degradation of Polyvinyl Alcohol byPycnoporus cinnabarinus after Pretreatment with Fenton’s Reagent journal, April 1999

Decontamination of chemical warfare agents journal, December 1992

The Reaction between Ferrous Iron and Peroxides. I. Reaction with Hydrogen Peroxide in the Absence of Oxygen
journal, November 1949

Opportunities and Challenges in the Application of Ozone in Food Processing
book, January 2014

Fenton Chemistry: An Introduction
journal, May 1996

The effect of sulfur mustard and nitrogen mustard on corneal collagen degradation induced by the enzyme collagenase
journal, June 2010

The effects of Fenton's reagent pretreatment on the biodegradability of nonionic surfactants
journal, August 1999

Oxidative Degradation of Polyvinyl Alcohol by the Photochemically Enhanced Fenton Reaction. Evidence for the Formation of Super-Macromolecules
journal, June 2001

Recent Advances in Biosensor Technology for Potential Applications – An Overview
journal, February 2016

Pathways for Extracellular Fenton Chemistry in the Brown Rot Basidiomycete Gloeophyllum trabeum
journal, June 2001

Detection of chemical warfare agents using nanostructured metal oxide sensors
journal, July 2005

Operating characteristics and kinetic studies of surfactant wastewater treatment by Fenton oxidation
journal, May 1999

Oxidative degradation of poly vinyl alcohol by the photochemically enhanced Fenton reaction
journal, July 1998

Pyridinium Oximes as Cholinesterase Reactivators. Structure-Activity Relationship and Efficacy in the Treatment of Poisoning with Organophosphorus Compounds
journal, June 2009

Overview of URBAN 2000: A Multiscale Field Study of Dispersion through an Urban Environment
journal, April 2002

Oxidative degradation of dyes and surfactant in the Fenton and photo-Fenton treatment of dyehouse effluents
journal, May 2000

Introduction
book, January 1996

Chemical warfare agents
journal, January 2010

Oxidation of alcohols by Fenton's reagent. Effect of copper ion
journal, August 1971

Biodegradative mechanism of the brown rot basidiomycete Gloeophyllum trabeum : evidence for an extracellular hydroquinone-driven fenton reaction
journal, March 1999

Enhanced Degradation of Polyvinyl Alcohol byPycnoporus cinnabarinus after Pretreatment with Fenton’s Reagent
journal, April 1999

Decontamination of chemical warfare agents
journal, December 1992