Method of determining the extent to which a nickel structure has been attached by a fluorine-containing gas
Abstract
The method of determining the extent to which a nickel structure has been attacked by a halogen containing gas to which it has been exposed which comprises preparing a quantity of water substantially free from dissolved oxygen, passing ammonia gas through a cuprammonium solution to produce ammonia substantially free from oxygen, dissolving said oxygen-free ammonia in said water to produce a saturated aqueous ammonia solution free from uncombined oxygen, treating at least a portion of said nickel structure of predetermined weight with said solution to dissolve nickel compounds from the surface of said structure without dissolving an appreciable amount of said nickel and analyzing the resulting solution to determine the quantity of said nickel compounds that was associated with said said portion of said structure to determine the proportion of combined nickel in said nickel structure.
- Inventors:
-
- Oak Ridge, TN
- Issue Date:
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 920042
- Patent Number(s):
- 6761862
- Application Number:
- 02/618,355
- Assignee:
- The United States of America as represented by the United States Department of Energy (Washington, DC)
- Patent Classifications (CPCs):
-
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01G - COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
C - CHEMISTRY C23 - COATING METALLIC MATERIAL C23G - CLEANING OR DEGREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- Resource Type:
- Patent
- Country of Publication:
- United States
- Language:
- English
Citation Formats
Brusie, James P. Method of determining the extent to which a nickel structure has been attached by a fluorine-containing gas. United States: N. p., 2004.
Web.
Brusie, James P. Method of determining the extent to which a nickel structure has been attached by a fluorine-containing gas. United States.
Brusie, James P. Tue .
"Method of determining the extent to which a nickel structure has been attached by a fluorine-containing gas". United States. https://www.osti.gov/servlets/purl/920042.
@article{osti_920042,
title = {Method of determining the extent to which a nickel structure has been attached by a fluorine-containing gas},
author = {Brusie, James P},
abstractNote = {The method of determining the extent to which a nickel structure has been attacked by a halogen containing gas to which it has been exposed which comprises preparing a quantity of water substantially free from dissolved oxygen, passing ammonia gas through a cuprammonium solution to produce ammonia substantially free from oxygen, dissolving said oxygen-free ammonia in said water to produce a saturated aqueous ammonia solution free from uncombined oxygen, treating at least a portion of said nickel structure of predetermined weight with said solution to dissolve nickel compounds from the surface of said structure without dissolving an appreciable amount of said nickel and analyzing the resulting solution to determine the quantity of said nickel compounds that was associated with said said portion of said structure to determine the proportion of combined nickel in said nickel structure.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue Jul 13 00:00:00 EDT 2004},
month = {Tue Jul 13 00:00:00 EDT 2004}
}