Accommodating subject and instrument variations in spectroscopic determinations
Abstract
A method and apparatus for measuring a biological attribute, such as the concentration of an analyte, particularly a blood analyte in tissue such as glucose. The method utilizes spectrographic techniques in conjunction with an improved instrument-tailored or subject-tailored calibration model. In a calibration phase, calibration model data is modified to reduce or eliminate instrument-specific attributes, resulting in a calibration data set modeling intra-instrument or intra-subject variation. In a prediction phase, the prediction process is tailored for each target instrument separately using a minimal number of spectral measurements from each instrument or subject.
- Inventors:
-
- Albuquerque, NM
- Corrales, NM
- Issue Date:
- Research Org.:
- Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 908262
- Patent Number(s):
- 7098037
- Application Number:
- 10/222,721
- Assignee:
- InLight Solutions, Inc. (Albuquerque, NM)
- Patent Classifications (CPCs):
-
A - HUMAN NECESSITIES A61 - MEDICAL OR VETERINARY SCIENCE A61B - DIAGNOSIS
G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- DOE Contract Number:
- AC04-94AL85000
- Resource Type:
- Patent
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 47 OTHER INSTRUMENTATION
Citation Formats
Haas, Michael J, Rowe, Robert K, and Thomas, Edward V. Accommodating subject and instrument variations in spectroscopic determinations. United States: N. p., 2006.
Web.
Haas, Michael J, Rowe, Robert K, & Thomas, Edward V. Accommodating subject and instrument variations in spectroscopic determinations. United States.
Haas, Michael J, Rowe, Robert K, and Thomas, Edward V. Tue .
"Accommodating subject and instrument variations in spectroscopic determinations". United States. https://www.osti.gov/servlets/purl/908262.
@article{osti_908262,
title = {Accommodating subject and instrument variations in spectroscopic determinations},
author = {Haas, Michael J and Rowe, Robert K and Thomas, Edward V},
abstractNote = {A method and apparatus for measuring a biological attribute, such as the concentration of an analyte, particularly a blood analyte in tissue such as glucose. The method utilizes spectrographic techniques in conjunction with an improved instrument-tailored or subject-tailored calibration model. In a calibration phase, calibration model data is modified to reduce or eliminate instrument-specific attributes, resulting in a calibration data set modeling intra-instrument or intra-subject variation. In a prediction phase, the prediction process is tailored for each target instrument separately using a minimal number of spectral measurements from each instrument or subject.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2006},
month = {8}
}
Works referenced in this record:
Improvement of multivariate calibration through instrument standardization
journal, March 1992
- Wang, Yongdong.; Lysaght, Michael J.; Kowalski, Bruce R.
- Analytical Chemistry, Vol. 64, Issue 5
Post-Prandial Blood Glucose Determination by Quantitative Mid-Infrared Spectroscopy
journal, June 1992
- Ward, Kenneth J.; Haaland, David M.; Robinson, M. Ries
- Applied Spectroscopy, Vol. 46, Issue 6
Fundamentals of Calibration Transfer through Procrustes Analysis
journal, October 1999
- Anderson, Chad E.; Kalivas, John H.
- Applied Spectroscopy, Vol. 53, Issue 10
On-line monitoring of the delivery of the hemodialysis prescription
journal, January 1995
- Keshaviah, Prakash R.; Ebben, James P.; Emerson, Paul F.
- Pediatric Nephrology, Vol. 9, Issue S1
Noninvasive Blood Glucose Sensors Based on Near-Infrared Spectroscopy
journal, June 1994
- Heise, H. M.; Marbach, R.; Koschinsky, Th.
- Artificial Organs, Vol. 18, Issue 6
Noninvasive Glucose Monitoring in Diabetic Patients: A Preliminary Evaluation
journal, September 1992
- Robinson, M. R.; Eaton, R. P.; Haaland, D. M.
- Clinical Chemistry, Vol. 38, Issue 9
Glucose measurement in patients with diabetes mellitus with dermal interstitial fluid
journal, October 1997
- Bantle, John P.; Thomas, William
- Journal of Laboratory and Clinical Medicine, Vol. 130, Issue 4
Dermal Interstitial Glucose as an Indicator of Ambient Glycemia
journal, September 1997
- Service, F. J.; O'Brien, P. C.; Wise, S. D.
- Diabetes Care, Vol. 20, Issue 9
Reagentless Near-Infrared Determination of Glucose in Whole Blood Using Multivariate Calibration
journal, October 1992
- Haaland, David M.; Robinson, M. Ries; Koepp, Gary W.
- Applied Spectroscopy, Vol. 46, Issue 10
Noninvasive Blood Glucose Assay by Near-Infrared Diffuse Reflectance Spectroscopy of the Human Inner Lip
journal, July 1993
- Marbach, R.; Koschinsky, Th.; Gries, F. A.
- Applied Spectroscopy, Vol. 47, Issue 7
Non-Invasive Monitoring of Metabolites Using Near Infrared Spectroscopy: State of the Art
journal, October 1996
- Heise, H.
- Hormone and Metabolic Research, Vol. 28, Issue 10
Additive Background Correction in Multivariate Instrument Standardization
journal, July 1995
- Wang, Ziyi.; Dean, Thomas.; Kowalski, Bruce R.
- Analytical Chemistry, Vol. 67, Issue 14
Temperatures of skin, subcutaneous tissue, muscle and core in resting men in cold, comfortable and hot conditions
journal, January 1992
- Webb, Paul
- European Journal of Applied Physiology and Occupational Physiology, Vol. 64, Issue 5
Standardization of Fiber-Optic Probes for Near-Infrared Multivariate Calibrations
journal, June 1998
- Sum, Stephen T.; Brown, Steven D.
- Applied Spectroscopy, Vol. 52, Issue 6
The Measurement of Dialysis Access Recirculation
journal, October 1993
- Sherman, Richard A.
- American Journal of Kidney Diseases, Vol. 22, Issue 4
Local centering in multivariate calibration
journal, May 1996
- Lorber, Avraham; Faber, Klaas; Kowalski, Bruce R.
- Journal of Chemometrics, Vol. 10, Issue 3, p. 215-220
Theory and validation of access flow measurement by dilution technique during hemodialysis
journal, July 1995
- Krivitski, Nikolai M.
- Kidney International, Vol. 48, Issue 1
On-Line Urea Monitoring: A Further Step towards Adequate Dialysis Prescription and Delivery
journal, September 1995
- Ronco, C.; Brendolan, A.; Crepaldi, C.
- The International Journal of Artificial Organs, Vol. 18, Issue 9
Improvement of PLS model transferability by robust wavelength selection
journal, July 1998
- Swierenga, H.; de Groot, P. J.; de Weijer, A. P.
- Chemometrics and Intelligent Laboratory Systems, Vol. 41, Issue 2
Spectroscopic and Clinical Aspects of Noninvasive Glucose Measurements
journal, February 1999
- Khalil, Omar S.
- Clinical Chemistry, Vol. 45, Issue 2
Optical Matching of near Infrared Reflectance Monochromator Instruments for the Analysis of Ground and Whole Wheat
journal, June 1999
- Osborne, B. G.; Kotwal, Z.; Wesley, I. J.
- Journal of Near Infrared Spectroscopy, Vol. 7, Issue 3
Transfer of Near-Infrared Multivariate Calibrations without Standards
journal, September 1996
- Blank, Thomas B.; Sum, Stephen T.; Brown, Steven D.
- Analytical Chemistry, Vol. 68, Issue 17, p. 2987-2995
Infrared Diffuse Reflectance Accessory for Local Analysis on Bulky Samples
journal, January 1988
- Korte, E. H.; Otto, A.
- Applied Spectroscopy, Vol. 42, Issue 1
Noninvasive Prediction of Glucose by Near-Infrared Diffuse Reflectance Spectroscopy
journal, September 1999
- Malin, Stephen F.; Ruchti, Timothy L.; Blank, Thomas B.
- Clinical Chemistry, Vol. 45, Issue 9
Comparison of Two Different Approaches toward Model Transferability in NIR Spectroscopy
journal, January 1998
- Swierenga, H.; Haanstra, W. G.; De Weijer, A. P.
- Applied Spectroscopy, Vol. 52, Issue 1
Optical diffuse reflectance accessory for measurements of skin tissue by near-infrared spectroscopy
journal, January 1995
- Marbach, R.; Heise, H. M.
- Applied Optics, Vol. 34, Issue 4
Calibration Transfer and Measurement Stability of Near-Infrared Spectrometers
journal, May 1992
- Wang, Yongdong; Kowalski, Bruce R.
- Applied Spectroscopy, Vol. 46, Issue 5
Effects of Dose of Dialysis on Morbidity and Mortality
journal, May 1994
- Hakim, Raymond M.; Breyer, Julia; Ismail, Nuhad
- American Journal of Kidney Diseases, Vol. 23, Issue 5
Hybrid Calibration Models: An Alternative to Calibration Transfer
journal, April 1998
- Ozdemir, Durmus; Mosley, Matt; Williams, Ron
- Applied Spectroscopy, Vol. 52, Issue 4
Application of Near-Infrared Spectroscopy for Non-Invasive Determination of Blood/Tissue Glucose Using Neural Networks
journal, January 1995
- Jagemann, Kay-Uwe; Fischbacher, Christoph; Danzer, Klaus
- Zeitschrift für Physikalische Chemie, Vol. 191, Issue Part_2
An evaluation of orthogonal signal correction applied to calibration transfer of near infrared spectra
journal, December 1998
- Sjöblom, Jonas; Svensson, Olof; Josefson, Mats
- Chemometrics and Intelligent Laboratory Systems, Vol. 44, Issue 1-2
A Disposable Urea Sensor for Continuous Monitoring of Hemodialysis Efficiency
journal, January 1993
- Jacobs, Paul; Suls, Jan; Sansen, Willy
- ASAIO Journal, Vol. 39, Issue 3