Synthesis of 2H- and 13C-substituted dithanes

Title: Synthesis of 2H- and 13C-substituted dithanes

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Abstract

The present invention is directed to labeled compounds, [2-.sup.13 C]dithiane wherein the .sup.13 C atom is directly bonded to one or two deuterium atoms. The present invention is also directed to processes of preparing [2-.sup.13 C]dithiane wherein the .sup.13 C atom is directly bonded to one or two deuterium atoms. The present invention is also directed to labeled compounds, e.g., [.sup.2 H.sub.1-2, .sup.13 C]methanol (arylthio)-, acetates wherein the .sup.13 C atom is directly bonded to exactly one or two deuterium atoms.

Inventors:

Martinez, Rodolfo A. ^[1]; Alvarez, Marc A. ^[1]; Silks, III, Louis A. ^[2]; Unkefer, Clifford J. ^[2]

(Santa Fe, NM)
(Los Alamos, NM)

Issue Date:: 2003-01-01

Research Org.:: Los Alamos National Laboratory (LANL), Los Alamos, NM

OSTI Identifier:: 875140

Patent Number(s):: 6541671

Assignee:: The Regents of the University of California (Los Alamos, NM) LANL

DOE Contract Number:: W-7405-ENG-36

Resource Type:: Patent

Country of Publication:: United States

Language:: English

Subject:: synthesis; 2h-; 13c-substituted; dithanes; directed; labeled; compounds; 2-sup13; cdithiane; sup13; atom; directly; bonded; deuterium; atoms; processes; preparing; sup2; hsub1-2; cmethanol; arylthio-; acetates; exactly; labeled compounds; /999/424/

Citation Formats


                    Martinez, Rodolfo A., Alvarez, Marc A., Silks, III, Louis A., and Unkefer, Clifford J. Synthesis of 2H- and 13C-substituted dithanes.  United States: N. p., 2003. 
        Web.

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                    Martinez, Rodolfo A., Alvarez, Marc A., Silks, III, Louis A., & Unkefer, Clifford J. Synthesis of 2H- and 13C-substituted dithanes.  United States.

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                    Martinez, Rodolfo A., Alvarez, Marc A., Silks, III, Louis A., and Unkefer, Clifford J. Wed .  
        "Synthesis of 2H- and 13C-substituted dithanes".  United States.  https://www.osti.gov/servlets/purl/875140.

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@article{osti_875140,

  title        = {Synthesis of 2H- and 13C-substituted dithanes},

  author       = {Martinez, Rodolfo A. and Alvarez, Marc A. and Silks, III, Louis A. and Unkefer, Clifford J.},

  abstractNote = {The present invention is directed to labeled compounds, [2-.sup.13 C]dithiane wherein the .sup.13 C atom is directly bonded to one or two deuterium atoms. The present invention is also directed to processes of preparing [2-.sup.13 C]dithiane wherein the .sup.13 C atom is directly bonded to one or two deuterium atoms. The present invention is also directed to labeled compounds, e.g., [.sup.2 H.sub.1-2, .sup.13 C]methanol (arylthio)-, acetates wherein the .sup.13 C atom is directly bonded to exactly one or two deuterium atoms.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2003},

  month        = {1}

}

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