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Title: Method and solvent composition for regenerating an ion exchange resin

Abstract

A method and composition for removing perchlorate from a highly selective ion exchange resin is disclosed. The disclosed approach comprises treating the resin in a solution of super critical or liquid carbon dioxide and one or more quaternary ammonium chloride surfactant compounds.

Inventors:
 [1];  [1];  [1];  [1];  [2];  [1]
  1. Livermore, CA
  2. Knoxville, TN
Issue Date:
Research Org.:
Sandia National Laboratories (SNL), Albuquerque, NM, and Livermore, CA (United States)
OSTI Identifier:
874521
Patent Number(s):
6407143
Assignee:
Sandia Corporation (Livermore, CA)
Patent Classifications (CPCs):
B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
C - CHEMISTRY C08 - ORGANIC MACROMOLECULAR COMPOUNDS C08J - WORKING-UP
DOE Contract Number:  
AC04-94AL85000
Resource Type:
Patent
Country of Publication:
United States
Language:
English
Subject:
method; solvent; composition; regenerating; exchange; resin; removing; perchlorate; highly; selective; disclosed; approach; treating; solution; super; critical; liquid; carbon; dioxide; quaternary; ammonium; chloride; surfactant; compounds; carbon dioxide; exchange resin; highly selective; solvent composition; comprises treating; /521/

Citation Formats

Even, William R, Irvin, David J, Irvin, Jennifer A, Tarver, Edward E, Brown, Gilbert M, and Wang, James C. F. Method and solvent composition for regenerating an ion exchange resin. United States: N. p., 2002. Web.
Even, William R, Irvin, David J, Irvin, Jennifer A, Tarver, Edward E, Brown, Gilbert M, & Wang, James C. F. Method and solvent composition for regenerating an ion exchange resin. United States.
Even, William R, Irvin, David J, Irvin, Jennifer A, Tarver, Edward E, Brown, Gilbert M, and Wang, James C. F. Tue . "Method and solvent composition for regenerating an ion exchange resin". United States. https://www.osti.gov/servlets/purl/874521.
@article{osti_874521,
title = {Method and solvent composition for regenerating an ion exchange resin},
author = {Even, William R and Irvin, David J and Irvin, Jennifer A and Tarver, Edward E and Brown, Gilbert M and Wang, James C. F.},
abstractNote = {A method and composition for removing perchlorate from a highly selective ion exchange resin is disclosed. The disclosed approach comprises treating the resin in a solution of super critical or liquid carbon dioxide and one or more quaternary ammonium chloride surfactant compounds.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2002},
month = {1}
}

Works referenced in this record:

Supercritical fluid extraction of polar analytes using in situ chemical derivatization
journal, February 1992


Perchlorate Chemistry: Implications for Analysis and Remediation
journal, September 1998


Ion pair partition chromatography of organic ammonium compounds
journal, October 1973


Ternary Systems of Liquid Carbon Dioxide
journal, December 1954


State‐of‐the‐art on the supercritical extraction of organics from hazardous wastes
journal, January 1985


Quantitative extraction of linear alkylbenzenesulfonates using supercritical carbon dioxide and a simple device for adding modifiers
journal, January 1991