Method of making thermally removable epoxies
Abstract
A method of making a thermally-removable epoxy by mixing a bis(maleimide) compound to a monomeric furan compound containing an oxirane group to form a di-epoxy mixture and then adding a curing agent at temperatures from approximately room temperature to less than approximately 90.degree. C. to form a thermally-removable epoxy. The thermally-removable epoxy can be easily removed within approximately an hour by heating to temperatures greater than approximately 90.degree. C. in a polar solvent. The epoxy material can be used in protecting electronic components that may require subsequent removal of the solid material for component repair, modification or quality control.
- Inventors:
-
- Albuquerque, NM
- Rio Rancho, NM
- late of Albuquerque, NM
- Issue Date:
- Research Org.:
- Sandia National Laboratories (SNL), Albuquerque, NM, and Livermore, CA (United States)
- OSTI Identifier:
- 874198
- Patent Number(s):
- 6337384
- Assignee:
- Sandia Corporation (Albuquerque, NM)
- Patent Classifications (CPCs):
-
C - CHEMISTRY C08 - ORGANIC MACROMOLECULAR COMPOUNDS C08G - MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
C - CHEMISTRY C08 - ORGANIC MACROMOLECULAR COMPOUNDS C08L - COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- DOE Contract Number:
- AC04-94AL85000
- Resource Type:
- Patent
- Country of Publication:
- United States
- Language:
- English
- Subject:
- method; thermally; removable; epoxies; thermally-removable; epoxy; mixing; bismaleimide; compound; monomeric; furan; containing; oxirane; form; di-epoxy; mixture; adding; curing; agent; temperatures; approximately; temperature; 90degree; easily; removed; hour; heating; polar; solvent; material; protecting; electronic; components; require; subsequent; removal; solid; component; repair; modification; quality; control; solid material; easily removed; curing agent; /528/521/523/525/
Citation Formats
Loy, Douglas A, Wheeler, David R, Russick, Edward M, McElhanon, James R, and Saunders, Randall S. Method of making thermally removable epoxies. United States: N. p., 2002.
Web.
Loy, Douglas A, Wheeler, David R, Russick, Edward M, McElhanon, James R, & Saunders, Randall S. Method of making thermally removable epoxies. United States.
Loy, Douglas A, Wheeler, David R, Russick, Edward M, McElhanon, James R, and Saunders, Randall S. Tue .
"Method of making thermally removable epoxies". United States. https://www.osti.gov/servlets/purl/874198.
@article{osti_874198,
title = {Method of making thermally removable epoxies},
author = {Loy, Douglas A and Wheeler, David R and Russick, Edward M and McElhanon, James R and Saunders, Randall S},
abstractNote = {A method of making a thermally-removable epoxy by mixing a bis(maleimide) compound to a monomeric furan compound containing an oxirane group to form a di-epoxy mixture and then adding a curing agent at temperatures from approximately room temperature to less than approximately 90.degree. C. to form a thermally-removable epoxy. The thermally-removable epoxy can be easily removed within approximately an hour by heating to temperatures greater than approximately 90.degree. C. in a polar solvent. The epoxy material can be used in protecting electronic components that may require subsequent removal of the solid material for component repair, modification or quality control.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue Jan 01 00:00:00 EST 2002},
month = {Tue Jan 01 00:00:00 EST 2002}
}
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Works referenced in this record:
The application of the Diels-Alder reaction to polymers bearing furan moieties. 1. Reactions with maleimides
journal, August 1997
- Laita, H.; Boufi, S.; Gandini, A.
- European Polymer Journal, Vol. 33, Issue 8