Smooth diamond films as low friction, long wear surfaces

Gruen, Dieter M; Krauss, Alan R; Erdemir, Ali; Bindal, Cuma; Zuiker, Christopher D

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Title: Smooth diamond films as low friction, long wear surfaces

Abstract

An article and method of manufacture of a nanocrystalline diamond film. The nanocrystalline film is prepared by forming a carbonaceous vapor, providing an inert gas containing gas stream and combining the gas stream with the carbonaceous containing vapor. A plasma of the combined vapor and gas stream is formed in a chamber and fragmented carbon species are deposited onto a substrate to form the nanocrystalline diamond film having a root mean square flatness of about 50 nm deviation from flatness in the as deposited state.

Inventors:

Gruen, Dieter M ^[1]; Krauss, Alan R ^[2]; Erdemir, Ali ^[2]; Bindal, Cuma ^[3]; Zuiker, Christopher D ^[4]

Downers Grove, IL
Naperville, IL
Woodridge, IL
LaGrange, IL

Issue Date:: Fri Jan 01 00:00:00 EST 1999

Research Org.:: Argonne National Laboratory (ANL), Argonne, IL (United States)

OSTI Identifier:: 872685

Patent Number(s):: 5989511

Assignee:: University of Chicago (Chicago, IL)

Patent Classifications (CPCs):: C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS

C - CHEMISTRY C23 - COATING METALLIC MATERIAL C23C - COATING METALLIC MATERIAL

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C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C01B32/25 - Diamond
C01B32/26 - Preparation

C - CHEMISTRY C23 - COATING METALLIC MATERIAL C23C - COATING METALLIC MATERIAL
C23C14/0605 - {Carbon}
C23C14/0611 - {Diamond}
C23C14/221 - {Ion beam deposition
C23C16/27 - Diamond only
C23C16/274 - {using microwave discharges}
C23C16/277 - {using other elements in the gas phase besides carbon and hydrogen
C23C16/4481 - {by evaporation using carrier gas in contact with the source material

C - CHEMISTRY C30 - CRYSTAL GROWTH C30B - SINGLE-CRYSTAL-GROWTH
C30B23/00 - Single-crystal growth by condensing evaporated or sublimed materials
C30B23/02 - Epitaxial-layer growth
C30B25/105 - {by irradiation or electric discharge}
C30B29/04 - Diamond
C30B29/605 - {Products containing multiple oriented crystallites, e.g. columnar crystallites}
C30B33/00 - After-treatment of single crystals or homogeneous polycrystalline material with defined structure

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01J - ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
H01J9/025 - {of field emission cathodes}

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DOE Contract Number:: W-31109-ENG-38

Resource Type:: Patent

Country of Publication:: United States

Language:: English

Subject:: smooth; diamond; films; friction; wear; surfaces; article; method; manufacture; nanocrystalline; film; prepared; forming; carbonaceous; vapor; providing; inert; gas; containing; stream; combining; plasma; combined; formed; chamber; fragmented; carbon; species; deposited; substrate; form; root; mean; square; flatness; 50; nm; deviation; gas containing; gas stream; inert gas; containing gas; diamond film; diamond films; carbonaceous vapor; root mean; nanocrystalline diamond; wear surface; carbon species; mean square; wear surfaces; containing vapor; /423/117/

Citation Formats


                    Gruen, Dieter M, Krauss, Alan R, Erdemir, Ali, Bindal, Cuma, and Zuiker, Christopher D. Smooth diamond films as low friction, long wear surfaces.  United States: N. p., 1999. 
        Web.

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                    Gruen, Dieter M, Krauss, Alan R, Erdemir, Ali, Bindal, Cuma, & Zuiker, Christopher D. Smooth diamond films as low friction, long wear surfaces.  United States.

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                    Gruen, Dieter M, Krauss, Alan R, Erdemir, Ali, Bindal, Cuma, and Zuiker, Christopher D. Fri .  
        "Smooth diamond films as low friction, long wear surfaces".  United States.  https://www.osti.gov/servlets/purl/872685.

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@article{osti_872685,

  title        = {Smooth diamond films as low friction, long wear surfaces},

  author       = {Gruen, Dieter M and Krauss, Alan R and Erdemir, Ali and Bindal, Cuma and Zuiker, Christopher D},

  abstractNote = {An article and method of manufacture of a nanocrystalline diamond film. The nanocrystalline film is prepared by forming a carbonaceous vapor, providing an inert gas containing gas stream and combining the gas stream with the carbonaceous containing vapor. A plasma of the combined vapor and gas stream is formed in a chamber and fragmented carbon species are deposited onto a substrate to form the nanocrystalline diamond film having a root mean square flatness of about 50 nm deviation from flatness in the as deposited state.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {Fri Jan 01 00:00:00 EST 1999},

  month        = {Fri Jan 01 00:00:00 EST 1999}

}

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Works referenced in this record:

Activated C70 and diamond
journal, November 1991

Meilunas, R.; Chang, R. P. H.; Liu, Shengzhong
Nature, Vol. 354, Issue 6351
https://doi.org/10.1038/354271a0

Near specular reflection of C60 ions in collisions with an HOPG graphite surface
journal, December 1991

Busmann, H. -G.; Lill, Th.; Hertel, I. V.
Chemical Physics Letters, Vol. 187, Issue 5
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First easily reproduced solution-phase synthesis and confirmation of superconductivity in the fullerene KxC60 (Tc = 18.0 .+-. 0.1 K)
journal, July 1991

Wang, H. Hau; Kini, Aravinda M.; Savall, Brad M.
Inorganic Chemistry, Vol. 30, Issue 14
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Nucleation of diamond films on surfaces using carbon clusters
journal, December 1991

Meilunas, R. J.; Chang, R. P. H.; Liu, Shengzhong
Applied Physics Letters, Vol. 59, Issue 26
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Metastable Growth of Diamond and Diamond-Like Phases
journal, August 1991

Angus, J. C.; Wang, Y.; Sunkara, M.
Annual Review of Materials Science, Vol. 21, Issue 1
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Crushing C60 to diamond at room temperature
journal, January 1992

Regueiro, Manual Núñez; Monceau, Pierre; Hodeau, Jean-Louis
Nature, Vol. 355, Issue 6357
https://doi.org/10.1038/355237a0

Growth mechanism of vapor-deposited diamond
journal, February 1988

Frenklach, Michael; Spear, Karl E.
Journal of Materials Research, Vol. 3, Issue 1
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Free-standing diamond membranes: optical, morphological and mechanical properties
journal, April 1992

Windischmann, Henry; Epps, Glenn F.
Diamond and Related Materials, Vol. 1, Issue 5-6
https://doi.org/10.1016/0925-9635(92)90185-Q

C60: Buckminsterfullerene
journal, September 1991

Kroto, H. W.; Allaf, A. W.; Balm, S. P.
Chemical Reviews, Vol. 91, Issue 6
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Triplet states of fullerenes C60 and C70. Electron paramagnetic resonance spectra, photophysics, and electronic structures
journal, March 1991

Wasielewski, Michael R.; O'Neil, Michael P.; Lykke, Keith R.
Journal of the American Chemical Society, Vol. 113, Issue 7
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High-yield synthesis, separation, and mass-spectrometric characterization of fullerenes C60 to C266
journal, September 1991

Parker, Deborah Holmes; Wurz, Peter; Chatterjee, Kuntal
Journal of the American Chemical Society, Vol. 113, Issue 20
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Superconductivity at 28.6 K in a rubidium-C60 fullerene compound, RbxC60, synthesized by a solution-phase technique
journal, July 1991

Wang, H. Hau; Kini, Aravinda M.; Savall, Brad M.
Inorganic Chemistry, Vol. 30, Issue 15
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Laser deposition of carbon clusters on surfaces: A new approach to the study of Fullerenes
journal, December 1990

Meijer, Gerard; Bethune, Donald S.
The Journal of Chemical Physics, Vol. 93, Issue 11
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Fullerenes
journal, October 1991

Curl, Robert F.; Smalley, Richard E.
Scientific American, Vol. 265, Issue 4
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Delayed electron emission from photoexcited C ₆₀
journal, November 1991

Wurz, Peter; Lykke, Keith R.
The Journal of Chemical Physics, Vol. 95, Issue 9
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When Diamonds Met Buckyballs
journal, November 1991

Moffat, A. S.
Science, Vol. 254, Issue 5033
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Diamond Film Semiconductors
journal, October 1992

Geis, Michael W.; Angus, John C.
Scientific American, Vol. 267, Issue 4
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Resilience of all-carbon molecules C60, C70, and C84: a surface-scattering time-of-flight investigation
journal, October 1991

Beck, Rainer D.; St. John, Pamela; Alvarez, Marcos M.
The Journal of Physical Chemistry, Vol. 95, Issue 21
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Solid C60: a new form of carbon
journal, September 1990

Krätschmer, W.; Lamb, Lowell D.; Fostiropoulos, K.
Nature, Vol. 347, Issue 6291
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Similar Records

Title: Smooth diamond films as low friction, long wear surfaces

Abstract

Citation Formats

Activated C70 and diamond journal, November 1991

Near specular reflection of C60 ions in collisions with an HOPG graphite surface journal, December 1991

First easily reproduced solution-phase synthesis and confirmation of superconductivity in the fullerene KxC60 (Tc = 18.0 .+-. 0.1 K) journal, July 1991

Nucleation of diamond films on surfaces using carbon clusters journal, December 1991

Metastable Growth of Diamond and Diamond-Like Phases journal, August 1991

Crushing C60 to diamond at room temperature journal, January 1992

Growth mechanism of vapor-deposited diamond journal, February 1988

Free-standing diamond membranes: optical, morphological and mechanical properties journal, April 1992

C60: Buckminsterfullerene journal, September 1991

Triplet states of fullerenes C60 and C70. Electron paramagnetic resonance spectra, photophysics, and electronic structures journal, March 1991

High-yield synthesis, separation, and mass-spectrometric characterization of fullerenes C60 to C266 journal, September 1991

Superconductivity at 28.6 K in a rubidium-C60 fullerene compound, RbxC60, synthesized by a solution-phase technique journal, July 1991

Laser deposition of carbon clusters on surfaces: A new approach to the study of Fullerenes journal, December 1990

Fullerenes journal, October 1991

Delayed electron emission from photoexcited C 60 journal, November 1991

When Diamonds Met Buckyballs journal, November 1991

Diamond Film Semiconductors journal, October 1992

Resilience of all-carbon molecules C60, C70, and C84: a surface-scattering time-of-flight investigation journal, October 1991

Solid C60: a new form of carbon journal, September 1990

Activated C70 and diamond
journal, November 1991

Near specular reflection of C60 ions in collisions with an HOPG graphite surface
journal, December 1991

First easily reproduced solution-phase synthesis and confirmation of superconductivity in the fullerene KxC60 (Tc = 18.0 .+-. 0.1 K)
journal, July 1991

Nucleation of diamond films on surfaces using carbon clusters
journal, December 1991

Metastable Growth of Diamond and Diamond-Like Phases
journal, August 1991

Crushing C60 to diamond at room temperature
journal, January 1992

Growth mechanism of vapor-deposited diamond
journal, February 1988

Free-standing diamond membranes: optical, morphological and mechanical properties
journal, April 1992

C60: Buckminsterfullerene
journal, September 1991

Triplet states of fullerenes C60 and C70. Electron paramagnetic resonance spectra, photophysics, and electronic structures
journal, March 1991

High-yield synthesis, separation, and mass-spectrometric characterization of fullerenes C60 to C266
journal, September 1991

Superconductivity at 28.6 K in a rubidium-C60 fullerene compound, RbxC60, synthesized by a solution-phase technique
journal, July 1991

Laser deposition of carbon clusters on surfaces: A new approach to the study of Fullerenes
journal, December 1990

Fullerenes
journal, October 1991

Delayed electron emission from photoexcited C ₆₀
journal, November 1991

When Diamonds Met Buckyballs
journal, November 1991

Diamond Film Semiconductors
journal, October 1992

Resilience of all-carbon molecules C60, C70, and C84: a surface-scattering time-of-flight investigation
journal, October 1991

Solid C60: a new form of carbon
journal, September 1990