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Title: Composite coating for low friction and wear applications and method thereof

Abstract

An article having a multiphase composite lubricant coating of a hard refractory matrix phase of titanium nitride dispersed with particles of a solid lubricating phase of molybdenum disulfide is prepared by heating the article to temperatures between 350.degree. and 850.degree. C. in a reaction vessel at a reduced pressure and passing a gaseous mixture of Ti((CH.sub.3).sub.2 N).sub.4, MoF.sub.6, H.sub.2 S and NH.sub.3 over the heated article forming a multiphase composite lubricant coating on the article.

Inventors:
 [1];  [1];  [2];  [1]
  1. Oak Ridge, TN
  2. Knoxville, TN
Issue Date:
Research Org.:
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
OSTI Identifier:
871332
Patent Number(s):
5709936
Assignee:
Lockheed Martin Energy Systems, Inc. (Oak Ridge, TN)
Patent Classifications (CPCs):
C - CHEMISTRY C10 - PETROLEUM, GAS OR COKE INDUSTRIES C10M - LUBRICATING COMPOSITIONS
Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y10 - TECHNICAL SUBJECTS COVERED BY FORMER USPC Y10T - TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
DOE Contract Number:  
AC05-84OR21400
Resource Type:
Patent
Country of Publication:
United States
Language:
English
Subject:
composite; coating; friction; wear; applications; method; article; multiphase; lubricant; hard; refractory; matrix; phase; titanium; nitride; dispersed; particles; solid; lubricating; molybdenum; disulfide; prepared; heating; temperatures; 350; degree; 850; reaction; vessel; reduced; pressure; passing; gaseous; mixture; mof; nh; heated; forming; composite coating; matrix phase; reduced pressure; titanium nitride; gaseous mixture; reaction vessel; article forming; multiphase composite; composite lubricant; lubricant coating; refractory matrix; molybdenum disulfide; solid lubricating; nitride dispersed; hard refractory; lubricating phase; /428/

Citation Formats

Besmann, Theodore M, Blau, Peter J, Lee, Woo Y, and Bae, Yong W. Composite coating for low friction and wear applications and method thereof. United States: N. p., 1998. Web.
Besmann, Theodore M, Blau, Peter J, Lee, Woo Y, & Bae, Yong W. Composite coating for low friction and wear applications and method thereof. United States.
Besmann, Theodore M, Blau, Peter J, Lee, Woo Y, and Bae, Yong W. Tue . "Composite coating for low friction and wear applications and method thereof". United States. https://www.osti.gov/servlets/purl/871332.
@article{osti_871332,
title = {Composite coating for low friction and wear applications and method thereof},
author = {Besmann, Theodore M and Blau, Peter J and Lee, Woo Y and Bae, Yong W},
abstractNote = {An article having a multiphase composite lubricant coating of a hard refractory matrix phase of titanium nitride dispersed with particles of a solid lubricating phase of molybdenum disulfide is prepared by heating the article to temperatures between 350.degree. and 850.degree. C. in a reaction vessel at a reduced pressure and passing a gaseous mixture of Ti((CH.sub.3).sub.2 N).sub.4, MoF.sub.6, H.sub.2 S and NH.sub.3 over the heated article forming a multiphase composite lubricant coating on the article.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {1998},
month = {1}
}

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Works referenced in this record:

Composition Optimization of Self-Lubricating Chromium-Carbide-Based Composite Coatings for Use to 760°C
journal, January 1987


Effect of Silicon Carbide Whisker and Titanium Carbide Particulate Additions on the Friction and Wear Behavior of Silicon Nitride
journal, November 1990