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Title: In situ calibration of inductively coupled plasma-atomic emission and mass spectroscopy

Abstract

A method and apparatus for in situ addition calibration of an inductively coupled plasma atomic emission spectrometer or mass spectrometer using a precision gas metering valve to introduce a volatile calibration gas of an element of interest directly into an aerosol particle stream. The present situ calibration technique is suitable for various remote, on-site sampling systems such as laser ablation or nebulization.

Inventors:
 [1]
  1. Ames, IA
Issue Date:
Research Org.:
Ames Laboratory (AMES), Ames, IA; Iowa State Univ., Ames, IA (United States)
OSTI Identifier:
870464
Patent Number(s):
5526110
Application Number:
08/273,024
Assignee:
Iowa State University Research Foundation, Inc. (Ames, IA)
Patent Classifications (CPCs):
G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01J - ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
DOE Contract Number:  
W-7405-ENG-82
Resource Type:
Patent
Country of Publication:
United States
Language:
English
Subject:
situ; calibration; inductively; coupled; plasma-atomic; emission; mass; spectroscopy; method; apparatus; addition; plasma; atomic; spectrometer; precision; gas; metering; valve; introduce; volatile; element; directly; aerosol; particle; stream; technique; suitable; various; remote; on-site; sampling; systems; laser; ablation; nebulization; aerosol particle; inductively coupled; mass spectrometer; coupled plasma; laser ablation; mass spectroscopy; calibration gas; situ calibration; metering valve; various remote; sampling systems; emission spectrometer; calibration technique; /356/250/

Citation Formats

Braymen, Steven D. In situ calibration of inductively coupled plasma-atomic emission and mass spectroscopy. United States: N. p., 1996. Web.
Braymen, Steven D. In situ calibration of inductively coupled plasma-atomic emission and mass spectroscopy. United States.
Braymen, Steven D. Mon . "In situ calibration of inductively coupled plasma-atomic emission and mass spectroscopy". United States. https://www.osti.gov/servlets/purl/870464.
@article{osti_870464,
title = {In situ calibration of inductively coupled plasma-atomic emission and mass spectroscopy},
author = {Braymen, Steven D},
abstractNote = {A method and apparatus for in situ addition calibration of an inductively coupled plasma atomic emission spectrometer or mass spectrometer using a precision gas metering valve to introduce a volatile calibration gas of an element of interest directly into an aerosol particle stream. The present situ calibration technique is suitable for various remote, on-site sampling systems such as laser ablation or nebulization.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {1996},
month = {1}
}

Works referenced in this record:

An Efficient and Inexpensive Ultrasonic Nebulizer for Atomic Spectrometry
journal, February 1990


Studies of Aerosols Generated by Electrically Vaporized Thin Films for ICP-AES
journal, March 1990