Composite hydrogen separation element and module

Edlund, David J

Title: Composite hydrogen separation element and module

Abstract

There are disclosed improvements in multicomponent composite metal membranes useful for the separation of hydrogen, the improvements comprising the provision of a flexible porous intermediate layer between a support layer and a nonporous hydrogen-permeable coating metal layer, and the provision of a textured coating metal layer.

Inventors:

Edlund, David J ^[1]

Redmond, OR

Issue Date:: 1996-03-12

Research Org.:: Bend Research, Inc. (Bend, OR)

Sponsoring Org.:: USDOE

OSTI Identifier:: 870333

Patent Number(s):: 5498278

Assignee:: Bend Research, Inc. (Bend, OR)

Patent Classifications (CPCs):: C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY

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C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C01B2203/0485 - the impurity being a sulfur compound
C01B3/34 - by reaction of hydrocarbons with gasifying agents

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J19/2475 - {Membrane reactors}

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION
B01D67/0065 - {by anodic oxidation}

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C01B2203/048 - the impurity being an organic compound

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION
B01D53/226 - {in serial connexion}
B01D69/141 - {Heterogeneous membranes, e.g. containing dispersed material
B01D53/22 - by diffusion

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J2219/2453 - Plates arranged in parallel

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C01B2203/0475 - the impurity being carbon dioxide

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J2219/2485 - Metals or alloys

C - CHEMISTRY C07 - ORGANIC CHEMISTRY C07C - ACYCLIC OR CARBOCYCLIC COMPOUNDS
C07C5/32 - by dehydrogenation with formation of free hydrogen

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION
B01D67/0046 - {by slurry techniques, e.g. die or slip-casting}

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J2219/2487 - Ceramics

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C01B3/505 - {Membranes containing palladium}

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J19/249 - {Plate-type reactors}

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION
B01D67/0041 - {by agglomeration of particles in the dry state, e.g. sintering}

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02E - REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
Y02E60/36 - Hydrogen production from non-carbon containing sources

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J2219/2498 - Additional structures inserted in the channels, e.g. plates, catalyst holding meshes

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION
B01D67/0072 - {by deposition from the gaseous phase, e.g. sputtering, CVD, PVD}
B01D2325/04 - Characteristic thickness

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C01B2203/0405 - Purification by membrane separation

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J2219/00159 - controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION
B01D2323/08 - Specific temperatures applied

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01C - AMMONIA
C01C1/0405 - {from N2 and H2 in presence of a catalyst}

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C01B3/12 - by reaction of water vapour with carbon monoxide

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J2219/2493 - Means for assembling plates together, e.g. sealing means, screws, bolts

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION
B01D2257/108 - Hydrogen

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J2219/2486 - Steel
B01J2219/00108 - involving reactant vapours

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C01B3/501 - {by diffusion}

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION
B01D69/12 - Composite membranes

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C01B2203/0495 - the impurity being water

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J2219/2467 - Additional heat exchange means, e.g. electric resistance heaters, coils

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C01B3/04 - by decomposition of inorganic compounds, e.g. ammonia {

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION
B01D71/02 - Inorganic material

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C01B3/503 - {characterised by the membrane}

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION
B01D2323/10 - Specific pressure applied

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C01B17/0456 - {the hydrogen sulfide-containing gas being a Claus process tail gas}

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION
B01D67/0069 - {by deposition from the liquid phase, e.g. electrochemical deposition

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C01B2203/0465 - Composition of the impurity
C01B17/0495 - {by dissociation of hydrogen sulfide into the elements}
C01B2203/047 - the impurity being carbon monoxide

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J2219/2475 - Separation means, e.g. membranes inside the reactor

C - CHEMISTRY C07 - ORGANIC CHEMISTRY C07C - ACYCLIC OR CARBOCYCLIC COMPOUNDS
C07C1/04 - from carbon monoxide with hydrogen

C - CHEMISTRY C23 - COATING METALLIC MATERIAL C23C - COATING METALLIC MATERIAL
C23C28/00 - Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION
B01D53/228 - {characterised by specific membranes}

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J2219/2496 - Means for assembling modules together, e.g. casings, holders, fluidic connectors

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02P - CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
Y02P20/52 - using catalysts, e.g. selective catalysts

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DOE Contract Number:: FG03-91ER81228; FG03-91ER81229

Resource Type:: Patent

Country of Publication:: United States

Language:: English

Subject:: composite; hydrogen; separation; element; module; disclosed; improvements; multicomponent; metal; membranes; useful; comprising; provision; flexible; porous; intermediate; layer; support; nonporous; hydrogen-permeable; coating; textured; coating metal; membranes useful; composite metal; metal layer; intermediate layer; support layer; metal membrane; separation element; metal membranes; hydrogen separation; multicomponent composite; composite hydrogen; improvements comprising; disclosed improvements; /96/55/95/

Citation Formats


                    Edlund, David J. Composite hydrogen separation element and module.  United States: N. p., 1996. 
        Web.

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                    Edlund, David J. Composite hydrogen separation element and module.  United States.

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                    Edlund, David J. Tue .  
        "Composite hydrogen separation element and module".  United States.  https://www.osti.gov/servlets/purl/870333.

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@article{osti_870333,

  title        = {Composite hydrogen separation element and module},

  author       = {Edlund, David J},

  abstractNote = {There are disclosed improvements in multicomponent composite metal membranes useful for the separation of hydrogen, the improvements comprising the provision of a flexible porous intermediate layer between a support layer and a nonporous hydrogen-permeable coating metal layer, and the provision of a textured coating metal layer.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {1996},

  month        = {3}

}

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Works referenced in this record:

Preparation and catalysis over palladium composite membranes
journal, March 1993

Gryaznov, V. M.; Serebryannikova, O. S.; Serov, Yu. M.
Applied Catalysis A: General, Vol. 96, Issue 1, p. 15-23
https://doi.org/10.1016/0926-860X(93)80003-9

Studies of hydrogen spillover. Part 1.—Study of the rate, extent and products of hydrogen spillover from platinum to the trioxides of tungsten and molybdenum
journal, January 1976

Sermon, Paul A.; Bond, Geoffrey C.
Journal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases, Vol. 72, Issue 0
https://doi.org/10.1039/f19767200730

Deposition of H2-permselective SiO2 films
journal, January 1989

Gavalas, G. R.; Megiris, C. E.; Nam, S. W.
Chemical Engineering Science, Vol. 44, Issue 9
https://doi.org/10.1016/0009-2509(89)85125-5

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Title: Composite hydrogen separation element and module

Abstract

Citation Formats

Preparation and catalysis over palladium composite membranes journal, March 1993

Studies of hydrogen spillover. Part 1.—Study of the rate, extent and products of hydrogen spillover from platinum to the trioxides of tungsten and molybdenum journal, January 1976

Deposition of H2-permselective SiO2 films journal, January 1989

Preparation and catalysis over palladium composite membranes
journal, March 1993

Studies of hydrogen spillover. Part 1.—Study of the rate, extent and products of hydrogen spillover from platinum to the trioxides of tungsten and molybdenum
journal, January 1976

Deposition of H2-permselective SiO2 films
journal, January 1989