Spectrometer capillary vessel and method of making same

Linehan, John C; Yonker, Clement R; Zemanian, Thomas S; Franz, James A

Title: Spectrometer capillary vessel and method of making same

Abstract

The present invention is an arrangement of a glass capillary tube for use in spectroscopy. In particular, the invention is a capillary arranged in a manner permitting a plurality or multiplicity of passes of a sample material through a spectroscopic measurement zone. In a preferred embodiment, the multi-pass capillary is insertable within a standard NMR sample tube. The present invention further includes a method of making the multi-pass capillary tube and an apparatus for spinning the tube.

Inventors:

Linehan, John C ^[1]; Yonker, Clement R ^[2]; Zemanian, Thomas S ^[1]; Franz, James A ^[2]

Richland, WA
Kennewick, WA

Issue Date:: 1995-01-01

Research Org.:: Pacific Northwest National Laboratory (PNNL), Richland, WA (United States)

OSTI Identifier:: 870173

Patent Number(s):: 5469061

Assignee:: Battelle Memorial Institute (Richland, WA)

Patent Classifications (CPCs):: G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES

G - PHYSICS G01 - MEASURING G01R - MEASURING ELECTRIC VARIABLES

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G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
G01N2021/0346 - {Capillary cells
G01N21/05 - Flow-through cuvettes

G - PHYSICS G01 - MEASURING G01R - MEASURING ELECTRIC VARIABLES
G01R33/30 - Sample handling arrangements, e.g. sample cells, spinning mechanisms
G01R33/307 - {specially adapted for moving the sample relative to the MR system, e.g. spinning mechanisms, flow cells or means for positioning the sample inside a spectrometer}

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DOE Contract Number:: AC06-76RL01830

Resource Type:: Patent

Country of Publication:: United States

Language:: English

Subject:: spectrometer; capillary; vessel; method; arrangement; glass; tube; spectroscopy; particular; arranged; manner; permitting; plurality; multiplicity; passes; sample; material; spectroscopic; measurement; zone; preferred; embodiment; multi-pass; insertable; standard; nmr; apparatus; spinning; capillary tube; preferred embodiment; sample material; sample tube; manner permitting; spectroscopic measurement; glass capillary; /324/

Citation Formats


                    Linehan, John C, Yonker, Clement R, Zemanian, Thomas S, and Franz, James A. Spectrometer capillary vessel and method of making same.  United States: N. p., 1995. 
        Web.

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                    Linehan, John C, Yonker, Clement R, Zemanian, Thomas S, & Franz, James A. Spectrometer capillary vessel and method of making same.  United States.

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                    Linehan, John C, Yonker, Clement R, Zemanian, Thomas S, and Franz, James A. Sun .  
        "Spectrometer capillary vessel and method of making same".  United States.  https://www.osti.gov/servlets/purl/870173.

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@article{osti_870173,

  title        = {Spectrometer capillary vessel and method of making same},

  author       = {Linehan, John C and Yonker, Clement R and Zemanian, Thomas S and Franz, James A},

  abstractNote = {The present invention is an arrangement of a glass capillary tube for use in spectroscopy. In particular, the invention is a capillary arranged in a manner permitting a plurality or multiplicity of passes of a sample material through a spectroscopic measurement zone. In a preferred embodiment, the multi-pass capillary is insertable within a standard NMR sample tube. The present invention further includes a method of making the multi-pass capillary tube and an apparatus for spinning the tube.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {1995},

  month        = {1}

}

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Works referenced in this record:

Nuclear Magnetic Resonance and Laser Scattering Techniques at High Pressure
book, January 1987

Jonas, Jiri
High Pressure Chemistry and Biochemistry
https://doi.org/10.1007/978-94-009-3827-4_8

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