Preparation of fullerene/glass composites

Mattes, Benjamin R; McBranch, Duncan W; Robinson, Jeanne M; Koskelo, Aaron C; Love, Steven P

Advanced Search OptionsAdvanced Search queries use a traditional Term Search. For more info, see our FAQ.

All Fields:

Patent Title:

Abstract:

Assignee:

Inventor(s):

Patent Number:

Patent Classification (CPC):

All Classifications
A - human necessities
A01 - agriculture
A21 - baking
A22 - butchering
A23 - foods or foodstuffs
A24 - tobacco
A41 - wearing apparel
A42 - headwear
A43 - footwear
A44 - haberdashery
A45 - hand or travelling articles
A46 - brushware
A47 - furniture
A61 - medical or veterinary science
A62 - life-saving
A63 - sports
A99 - subject matter not otherwise provided for in this section
B - performing operations
B01 - physical or chemical processes or apparatus in general
B02 - crushing, pulverising, or disintegrating
B03 - separation of solid materials using liquids or using pneumatic tables or jigs
B04 - centrifugal apparatus or machines for carrying-out physical or chemical processes
B05 - spraying or atomising in general
B06 - generating or transmitting mechanical vibrations in general
B07 - separating solids from solids
B08 - cleaning
B09 - disposal of solid waste
B21 - mechanical metal-working without essentially removing material
B22 - casting
B23 - machine tools
B24 - grinding
B25 - hand tools
B26 - hand cutting tools
B27 - working or preserving wood or similar material
B28 - working cement, clay, or stone
B29 - working of plastics
B30 - presses
B31 - making articles of paper, cardboard or material worked in a manner analogous to paper
B32 - layered products
B33 - additive manufacturing technology
B41 - printing
B42 - bookbinding
B43 - writing or drawing implements
B44 - decorative arts
B60 - vehicles in general
B61 - railways
B62 - land vehicles for travelling otherwise than on rails
B63 - ships or other waterborne vessels
B64 - aircraft
B65 - conveying
B66 - hoisting
B67 - opening, closing {or cleaning} bottles, jars or similar containers
B68 - saddlery
B81 - microstructural technology
B82 - nanotechnology
B99 - subject matter not otherwise provided for in this section
C - chemistry
C01 - inorganic chemistry
C02 - treatment of water, waste water, sewage, or sludge
C03 - glass
C04 - cements
C05 - fertilisers
C06 - explosives
C07 - organic chemistry
C08 - organic macromolecular compounds
C09 - dyes
C10 - petroleum, gas or coke industries
C11 - animal or vegetable oils, fats, fatty substances or waxes
C12 - biochemistry
C13 - sugar industry
C14 - skins
C21 - metallurgy of iron
C22 - metallurgy
C23 - coating metallic material
C25 - electrolytic or electrophoretic processes
C30 - crystal growth
C40 - combinatorial technology
C99 - subject matter not otherwise provided for in this section
D - textiles
D01 - natural or man-made threads or fibres
D02 - yarns
D03 - weaving
D04 - braiding
D05 - sewing
D06 - treatment of textiles or the like
D07 - ropes
D10 - indexing scheme associated with sublasses of section d, relating to textiles
D21 - paper-making
D99 - subject matter not otherwise provided for in this section
E - fixed constructions
E01 - construction of roads, railways, or bridges
E02 - hydraulic engineering
E03 - water supply
E04 - building
E05 - locks
E06 - doors, windows, shutters, or roller blinds in general
E21 - earth drilling
E99 - subject matter not otherwise provided for in this section
F - mechanical engineering
F01 - machines or engines in general
F02 - combustion engines
F03 - machines or engines for liquids
F04 - positive - displacement machines for liquids
F05 - indexing schemes relating to engines or pumps in various subclasses of classes f01-f04
F15 - fluid-pressure actuators
F16 - engineering elements and units
F17 - storing or distributing gases or liquids
F21 - lighting
F22 - steam generation
F23 - combustion apparatus
F24 - heating
F25 - refrigeration or cooling
F26 - drying
F27 - furnaces
F28 - heat exchange in general
F41 - weapons
F42 - ammunition
F99 - subject matter not otherwise provided for in this section
G - physics
G01 - measuring
G02 - optics
G03 - photography
G04 - horology
G05 - controlling
G06 - computing
G07 - checking-devices
G08 - signalling
G09 - education
G10 - musical instruments
G11 - information storage
G12 - instrument details
G16 - information and communication technology [ict] specially adapted for specific application fields
G21 - nuclear physics
G99 - subject matter not otherwise provided for in this section
H - electricity
H01 - basic electric elements
H02 - generation
H03 - basic electronic circuitry
H04 - electric communication technique
H05 - electric techniques not otherwise provided for
H99 - subject matter not otherwise provided for in this section
Y - new / cross sectional technologies
Y02 - technologies or applications for mitigation or adaptation against climate change
Y04 - information or communication technologies having an impact on other technology areas
Y10 - technical subjects covered by former uspc

More Options ...

Title: Preparation of fullerene/glass composites

Abstract

Synthesis of fullerene/glass composites. A direct method for preparing solid solutions of C.sub.60 in silicon dioxide (SiO.sub.2) glass matrices by means of sol-gel chemistry is described. In order to produce highly concentrated fullerene-sol-gel-composites it is necessary to increase the solubility of these "guests" in a delivery solvent which is compatible with the starter sol (receiving solvent). Sonication results in aggregate disruption by treatment with high frequency sound waves, thereby accelerating the rate of hydrolysis of the alkoxide precursor, and the solution process for the C.sub.60. Depending upon the preparative procedure, C.sub.60 dispersed within the glass matrix as microcrystalline domains, or dispersed as true molecular solutions of C.sub.60 in a solid glass matrix, is generated by the present method.

Inventors:

Mattes, Benjamin R ^[1]; McBranch, Duncan W ^[1]; Robinson, Jeanne M ^[2]; Koskelo, Aaron C ^[2]; Love, Steven P ^[2]

Santa Fe, NM
Los Alamos, NM

Issue Date:: 1995-01-01

Research Org.:: Los Alamos National Laboratory (LANL), Los Alamos, NM (United States)

OSTI Identifier:: 869907

Patent Number(s):: 5420081

Assignee:: Regents of University of California Office of Technology Transfer (Alameda, CA)

Patent Classifications (CPCs):: C - CHEMISTRY C03 - GLASS C03C - CHEMICAL COMPOSITION OF GLASSES, GLAZES, OR VITREOUS ENAMELS

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y10 - TECHNICAL SUBJECTS COVERED BY FORMER USPC Y10T - TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION

Show more

C - CHEMISTRY C03 - GLASS C03C - CHEMICAL COMPOSITION OF GLASSES, GLAZES, OR VITREOUS ENAMELS
C03C14/008 - {the non-glass component being in molecular form}
C03C2214/32 - comprising a sol-gel process

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y10 - TECHNICAL SUBJECTS COVERED BY FORMER USPC Y10T - TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
Y10T29/49014 - Superconductor

Show less

DOE Contract Number:: W-7405-ENG-36

Resource Type:: Patent

Country of Publication:: United States

Language:: English

Subject:: preparation; fullerene; glass; composites; synthesis; direct; method; preparing; solid; solutions; 60; silicon; dioxide; sio; matrices; means; sol-gel; chemistry; described; produce; highly; concentrated; fullerene-sol-gel-composites; increase; solubility; guests; delivery; solvent; compatible; starter; sol; receiving; sonication; results; aggregate; disruption; treatment; frequency; sound; waves; accelerating; rate; hydrolysis; alkoxide; precursor; solution; process; depending; preparative; procedure; dispersed; matrix; microcrystalline; domains; true; molecular; generated; sound waves; solid solution; silicon dioxide; glass matrix; highly concentrated; solid solutions; sol-gel chemistry; oxide precursor; produce highly; solution process; solid glass; glass composites; alkoxide precursor; sound wave; direct method; /501/

Citation Formats


                    Mattes, Benjamin R, McBranch, Duncan W, Robinson, Jeanne M, Koskelo, Aaron C, and Love, Steven P. Preparation of fullerene/glass composites.  United States: N. p., 1995. 
        Web.

Copy to clipboard


                    Mattes, Benjamin R, McBranch, Duncan W, Robinson, Jeanne M, Koskelo, Aaron C, & Love, Steven P. Preparation of fullerene/glass composites.  United States.

Copy to clipboard


                    Mattes, Benjamin R, McBranch, Duncan W, Robinson, Jeanne M, Koskelo, Aaron C, and Love, Steven P. Sun .  
        "Preparation of fullerene/glass composites".  United States.  https://www.osti.gov/servlets/purl/869907.

Copy to clipboard


                    
@article{osti_869907,

  title        = {Preparation of fullerene/glass composites},

  author       = {Mattes, Benjamin R and McBranch, Duncan W and Robinson, Jeanne M and Koskelo, Aaron C and Love, Steven P},

  abstractNote = {Synthesis of fullerene/glass composites. A direct method for preparing solid solutions of C.sub.60 in silicon dioxide (SiO.sub.2) glass matrices by means of sol-gel chemistry is described. In order to produce highly concentrated fullerene-sol-gel-composites it is necessary to increase the solubility of these "guests" in a delivery solvent which is compatible with the starter sol (receiving solvent). Sonication results in aggregate disruption by treatment with high frequency sound waves, thereby accelerating the rate of hydrolysis of the alkoxide precursor, and the solution process for the C.sub.60. Depending upon the preparative procedure, C.sub.60 dispersed within the glass matrix as microcrystalline domains, or dispersed as true molecular solutions of C.sub.60 in a solid glass matrix, is generated by the present method.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {1995},

  month        = {1}

}

Copy to clipboard

Patent:

Save / Share:

Export Metadata

Save to My Library

Works referenced in this record:

Diffusion of C60 in porous sol-gel glass
journal, February 1994

Zerda, T. W.; Brodka, A.; Coffer, J.
Journal of Non-Crystalline Solids, Vol. 168, Issue 1-2
https://doi.org/10.1016/0022-3093(94)90117-1

Preparation of C70-Doped Solid Silica Gel via Sol-Gel Process
journal, October 1992

Dai, Sheng; Compton, Robert N.; Young, Jack P.
Journal of the American Ceramic Society, Vol. 75, Issue 10
https://doi.org/10.1111/j.1151-2916.1992.tb05518.x

Similar Records in DOE Patents and OSTI.GOV collections:

Solid state electrolyte composites based on complex hydrides and metal doped fullerenes/fulleranes for batteries and electrochemical applications

Patent Zidan, Ragaiy; Teprovich, Jr., Joseph A.; Colon-Mercado, Hector R.; ...

A LiBH₄--C₆₀ nanocomposite that displays fast lithium ionic conduction in the solid state is provided. The material is a homogenous nanocomposite that contains both LiBH₄ and a hydrogenated fullerene species. In the presence of C₆₀, the lithium ion mobility of LiBH₄ is significantly enhanced in the as prepared state when compared to pure LiBH₄. After the material is annealed the lithium ion mobility is further enhanced. Constant current cycling demonstrated that the material is stable in the presence of metallic lithium electrodes. The material can serve as a solid state electrolyte in a solid-state lithium ion battery.
Full Text Available
Graphene macro-assembly-fullerene composite for electrical energy storage

Patent Campbell, Patrick G.; Baumann, Theodore F.; Biener, Juergen; ...

Disclosed here is a method for producing a graphene macro-assembly (GMA)-fullerene composite, comprising providing a GMA comprising a three-dimensional network of graphene sheets crosslinked by covalent carbon bonds, and incorporating at least 20 wt. % of at least one fullerene compound into the GMA based on the initial weight of the GMA to obtain a GMA-fullerene composite. Also described are a GMA-fullerene composite produced, an electrode comprising the GMA-fullerene composite, and a supercapacitor comprising the electrode and optionally an organic or ionic liquid electrolyte in contact with the electrode.
Full Text Available
Solid state electrolyte composites based on complex hydrides and metal doped fullerenes/fulleranes for batteries and electrochemical applications

Patent Zidan, Ragaiy; Teprovich, Joseph A.; Colon-Mercado, Hector R.; ...

A LiBH4—C₆₀ nanocomposite that displays fast lithium ionic conduction in the solid state is provided. The material is a homogenous nanocomposite that contains both LiBH₄ and a hydrogenated fullerene species. In the presence of C₆₀, the lithium ion mobility of LiBH₄ is significantly enhanced in the as prepared state when compared to pure LiBH₄. After the material is annealed the lithium ion mobility is further enhanced. Constant current cycling demonstrated that the material is stable in the presence of metallic lithium electrodes. The material can serve as a solid state electrolyte in a solid-state lithium ion battery.
Full Text Available
Graphene macro-assembly-fullerene composite for electrical energy storage

Patent Campbell, Patrick G.; Baumann, Theodore F.; Biener, Juergen; ...

Disclosed here is a method for producing a graphene macro-assembly (GMA)-fullerene composite, comprising providing a GMA comprising a three-dimensional network of graphene sheets crosslinked by covalent carbon bonds, and incorporating at least 20 wt. % of at least one fullerene compound into the GMA based on the initial weight of the GMA to obtain a GMA-fullerene composite. Also described are a GMA-fullerene composite produced, an electrode comprising the GMA-fullerene composite, and a supercapacitor comprising the electrode and optionally an organic or ionic liquid electrolyte in contact with the electrode.
Full Text Available
Graphene macro-assembly-fullerene composite for electrical energy storage

Patent Campbell, Patrick G.; Biener, Monika M.; Hernandez, Maira Raquel Ceron

Disclosed here is a method for producing a graphene macro-assembly (GMA)-fullerene composite, comprising providing a mixture of graphene oxide and water, adding a hydroxylated fullerene to the mixture, and forming a gel of the hydroxylated fullerene and the mixture. Also described are a GMA-fullerene composite produced, an electrode comprising the GMA-fullerene composite, and a supercapacitor comprising the electrode.
Full Text Available

Similar Records

Title: Preparation of fullerene/glass composites

Abstract

Citation Formats

Diffusion of C60 in porous sol-gel glass journal, February 1994

Preparation of C70-Doped Solid Silica Gel via Sol-Gel Process journal, October 1992

Diffusion of C60 in porous sol-gel glass
journal, February 1994

Preparation of C70-Doped Solid Silica Gel via Sol-Gel Process
journal, October 1992