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Title: Synthesis of 3,3-dinitroazetidine

Abstract

The compound, 3,3-dinitroazetidine, and a process of preparing 3,3-dinitroazetidine including reacting a mixture of 1-tertiary-butyl-3,3-dinitroazetidine and benzyl chloroformate to form 1-(benzyloxycarbonyl)-3,3-dinitroazetidine, reacting the 1-(benzyloxycarbonyl)-3,3-dinitroazetidine and trifluoromethanesulfonic acid to form 3,3-dinitroazetidinium trifluoromethanesulfonate, and neutralizing the 3,3-dinitroazetidinium trifluoromethanesulfonate with a base to form 3,3-dinitroazetidine are provided. Salts of the 3,3-dinitroazetidine and preparation of such salts are also disclosed.

Inventors:
 [1]
  1. Los Alamos, NM
Issue Date:
Research Org.:
Los Alamos National Laboratory (LANL), Los Alamos, NM
OSTI Identifier:
869779
Patent Number(s):
5395945
Assignee:
United States of America as represented by United States (Washington, DC)
Resource Type:
Patent
Country of Publication:
United States
Language:
English
Subject:
synthesis; 3-dinitroazetidine; compound; process; preparing; including; reacting; mixture; 1-tertiary-butyl-3; benzyl; chloroformate; form; 1-; benzyloxycarbonyl; -3; trifluoromethanesulfonic; acid; 3-dinitroazetidinium; trifluoromethanesulfonate; neutralizing; base; provided; salts; preparation; disclosed; sulfonic acid; including reacting; /999/

Citation Formats

Hiskey, Michael A. Synthesis of 3,3-dinitroazetidine. United States: N. p., 1995. Web.
Hiskey, Michael A. Synthesis of 3,3-dinitroazetidine. United States.
Hiskey, Michael A. Sun . "Synthesis of 3,3-dinitroazetidine". United States. https://www.osti.gov/servlets/purl/869779.
@article{osti_869779,
title = {Synthesis of 3,3-dinitroazetidine},
author = {Hiskey, Michael A},
abstractNote = {The compound, 3,3-dinitroazetidine, and a process of preparing 3,3-dinitroazetidine including reacting a mixture of 1-tertiary-butyl-3,3-dinitroazetidine and benzyl chloroformate to form 1-(benzyloxycarbonyl)-3,3-dinitroazetidine, reacting the 1-(benzyloxycarbonyl)-3,3-dinitroazetidine and trifluoromethanesulfonic acid to form 3,3-dinitroazetidinium trifluoromethanesulfonate, and neutralizing the 3,3-dinitroazetidinium trifluoromethanesulfonate with a base to form 3,3-dinitroazetidine are provided. Salts of the 3,3-dinitroazetidine and preparation of such salts are also disclosed.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {1995},
month = {1}
}

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