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Title: Process for making solid-state radiation-emitting composition

Abstract

The invention provides a process for loading an aerogel substrate with tritium and the resultant compositions. According to the process, an aerogel substrate is hydrolyzed so that surface OH groups are formed. The hydrolyzed aerogel is then subjected to tritium exchange employing, for example, a tritium-containing gas, whereby tritium atoms replace H atoms of surface OH groups. OH and/or CH groups of residual alcohol present in the aerogel may also undergo tritium exchange.

Inventors:
 [1];  [2];  [3];  [4]
  1. 14316 Bauer Rd., N.E., Albuquerque, NM 87123
  2. 14 Eagle Nest Dr., N.E., Albuquerque, NM 87122
  3. 10308 Leymon Court, N.W., Albuquerque, NM 87114
  4. 3215 Blume, N.E., Albuquerque, NM 87111
Issue Date:
Research Org.:
AT&T
OSTI Identifier:
868903
Patent Number(s):
5240647
Assignee:
Ashley, Carol S. (14316 Bauer Rd., N.E., Albuquerque, NM 87123);Brinker, C. Jeffrey (14 Eagle Nest Dr., N.E., Albuquerque, NM 87122);Reed, Scott (10308 Leymon Court, N.W., Albuquerque, NM 87114);Walko, Robert J. (3215 Blume, N.E., Albuquerque, NM 87111)
Patent Classifications (CPCs):
C - CHEMISTRY C09 - DYES C09K - MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
DOE Contract Number:  
AC04-76DP00789
Resource Type:
Patent
Country of Publication:
United States
Language:
English
Subject:
process; solid-state; radiation-emitting; composition; provides; loading; aerogel; substrate; tritium; resultant; compositions; according; hydrolyzed; surface; oh; formed; subjected; exchange; employing; example; tritium-containing; gas; whereby; atoms; replace; residual; alcohol; undergo; containing gas; aerogel substrate; tritium atoms; solid-state radiation-emitting; surface oh; resultant compositions; radiation-emitting composition; /252/250/362/428/

Citation Formats

Ashley, Carol S, Brinker, C Jeffrey, Reed, Scott, and Walko, Robert J. Process for making solid-state radiation-emitting composition. United States: N. p., 1993. Web.
Ashley, Carol S, Brinker, C Jeffrey, Reed, Scott, & Walko, Robert J. Process for making solid-state radiation-emitting composition. United States.
Ashley, Carol S, Brinker, C Jeffrey, Reed, Scott, and Walko, Robert J. Fri . "Process for making solid-state radiation-emitting composition". United States. https://www.osti.gov/servlets/purl/868903.
@article{osti_868903,
title = {Process for making solid-state radiation-emitting composition},
author = {Ashley, Carol S and Brinker, C Jeffrey and Reed, Scott and Walko, Robert J},
abstractNote = {The invention provides a process for loading an aerogel substrate with tritium and the resultant compositions. According to the process, an aerogel substrate is hydrolyzed so that surface OH groups are formed. The hydrolyzed aerogel is then subjected to tritium exchange employing, for example, a tritium-containing gas, whereby tritium atoms replace H atoms of surface OH groups. OH and/or CH groups of residual alcohol present in the aerogel may also undergo tritium exchange.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Fri Jan 01 00:00:00 EST 1993},
month = {Fri Jan 01 00:00:00 EST 1993}
}

Works referenced in this record:

Phosphors Versus the Periodic System of the Elements
journal, May 1944


Scintillation Counters
journal, January 1954


Development and Applications of Transparent Cathode-Ray Screens
journal, July 1958


The Efficiency of Cathode-Ray Phosphors
journal, January 1970


The Efficiency of Cathode-Ray Phosphors
journal, January 1970


Radioisotope-Powered Photovoltaic Generator
journal, May 1979