Method of making in-situ whisker reinforced glass ceramic

Brown, Jesse J; Hirschfeld, Deidre A; Lee, K H

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Title: Method of making in-situ whisker reinforced glass ceramic

Abstract

A heat processing procedure is used to create reinforcing whiskers of TiO.sub.2 in glass-ceramic materials in the LAS and MAS family. The heat processing procedure has particular application in creating TiO.sub.2 in-situ in a modified .beta.-eucryptite system.

Inventors:

Brown, Jesse J ^[1]; Hirschfeld, Deidre A ^[2]; Lee, K H ^[3]

Christiansburg, VA
Elliston, VA
Blacksburg, VA

Issue Date:: Tue Feb 16 00:00:00 EST 1993

OSTI Identifier:: 868659

Patent Number(s):: 5186729

Application Number:: 07/692,214

Assignee:: Center for Innovative Technology (Herndon, VA); VPI & SU (Blacksburg, VA)

Patent Classifications (CPCs):: C - CHEMISTRY C03 - GLASS C03C - CHEMICAL COMPOSITION OF GLASSES, GLAZES, OR VITREOUS ENAMELS

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C - CHEMISTRY C03 - GLASS C03C - CHEMICAL COMPOSITION OF GLASSES, GLAZES, OR VITREOUS ENAMELS
C03C10/0027 - {containing SiO2, Al2O3, Li2O as main constituents}
C03C10/0045 - {containing SiO2, Al2O3 and MgO as main constituents}
C03C14/00 - Glass compositions containing a non-glass component, e.g. compositions containing fibres, filaments, whiskers, platelets, or the like, dispersed in a glass matrix
C03C2214/06 - Whiskers ss
C03C2214/20 - Glass-ceramics matrix
C03C2214/30 - Methods of making the composites

Show less

DOE Contract Number:: 19X-22049C

Resource Type:: Patent

Country of Publication:: United States

Language:: English

Subject:: method; in-situ; whisker; reinforced; glass; ceramic; heat; processing; procedure; create; reinforcing; whiskers; glass-ceramic; materials; mas; family; particular; application; creating; modified; beta; -eucryptite; glass ceramic; particular application; ceramic material; ceramic materials; whisker reinforced; heat processing; ceramic mater; processing procedure; /65/501/

Citation Formats


                    Brown, Jesse J, Hirschfeld, Deidre A, and Lee, K H. Method of making in-situ whisker reinforced glass ceramic.  United States: N. p., 1993. 
        Web.

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                    Brown, Jesse J, Hirschfeld, Deidre A, & Lee, K H. Method of making in-situ whisker reinforced glass ceramic.  United States.

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                    Brown, Jesse J, Hirschfeld, Deidre A, and Lee, K H. Tue .  
        "Method of making in-situ whisker reinforced glass ceramic".  United States.  https://www.osti.gov/servlets/purl/868659.

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@article{osti_868659,

  title        = {Method of making in-situ whisker reinforced glass ceramic},

  author       = {Brown, Jesse J and Hirschfeld, Deidre A and Lee, K H},

  abstractNote = {A heat processing procedure is used to create reinforcing whiskers of TiO.sub.2 in glass-ceramic materials in the LAS and MAS family. The heat processing procedure has particular application in creating TiO.sub.2 in-situ in a modified .beta.-eucryptite system.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {Tue Feb 16 00:00:00 EST 1993},

  month        = {Tue Feb 16 00:00:00 EST 1993}

}

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Works referenced in this record:

Crack deflection processes—II. Experiment
journal, April 1983

Faber, K. T.; Evans, A. G.
Acta Metallurgica, Vol. 31, Issue 4
https://doi.org/10.1016/0001-6160(83)90047-0

Microstructural Characterization and Fracture Toughness of Cordierite-ZrO2 Glass-Ceramics
journal, August 1988

McCOY, Michael A.; Heuer, Arthur H.
Journal of the American Ceramic Society, Vol. 71, Issue 8
https://doi.org/10.1111/j.1151-2916.1988.tb06387.x

Microstructure and Kinetics of Crystallization of MgO-Al2O3-Si02 Glass-Ceramics
journal, May 1978

Zdaniewski, Wieslaw A.
Journal of the American Ceramic Society, Vol. 61, Issue 5-6
https://doi.org/10.1111/j.1151-2916.1978.tb09278.x

Crack deflection processes—I. Theory
journal, April 1983

Faber, K. T.; Evans, A. G.
Acta Metallurgica, Vol. 31, Issue 4
https://doi.org/10.1016/0001-6160(83)90046-9

Crystallization of MgO-Al2O3-SiO2-ZrO2 Glasses
journal, March 1986

McCOY, M.; Lee, W. E.; Heuer, A. H.
Journal of the American Ceramic Society, Vol. 69, Issue 3
https://doi.org/10.1111/j.1151-2916.1986.tb07430.x

Effect of Crystallites on Subcritical Crack Growth and Strain-Rate Sensitivity of Strength of Cordierite Glass-Ceramics
journal, March 1985

Baskaran, S.; Bhaduri, S. B.; Hasselman, D. P. H.
Journal of the American Ceramic Society, Vol. 68, Issue 3
https://doi.org/10.1111/j.1151-2916.1985.tb09647.x

Effect of Crystallites on Surface Damage and Fracture Behavior of a Glass-Ceramic
journal, October 1983

Morena, R.; Niihara, K.; Haselman, D. P. H.
Journal of the American Ceramic Society, Vol. 66, Issue 10
https://doi.org/10.1111/j.1151-2916.1983.tb10528.x

Role of crack size in the bi-modal static fatigue failure of a cordierite glass and glass-ceramic
journal, March 1987

Baskaran, Suresh; Lee, Hong Lim; Hasselman, D. P. H.
Journal of Materials Science, Vol. 22, Issue 3
https://doi.org/10.1007/BF01103523

Strength and Microstructure in Lithium Disilicate Glass-Ceramics
journal, September 1975

Borom, Marcus P.; Turkalo, Anna M.; Doremus, Robert H.
Journal of the American Ceramic Society, Vol. 58, Issue 9-10
https://doi.org/10.1111/j.1151-2916.1975.tb19004.x

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Similar Records

Title: Method of making in-situ whisker reinforced glass ceramic

Abstract

Citation Formats

Crack deflection processes—II. Experiment journal, April 1983

Microstructural Characterization and Fracture Toughness of Cordierite-ZrO2 Glass-Ceramics journal, August 1988

Microstructure and Kinetics of Crystallization of MgO-Al2O3-Si02 Glass-Ceramics journal, May 1978

Crack deflection processes—I. Theory journal, April 1983

Crystallization of MgO-Al2O3-SiO2-ZrO2 Glasses journal, March 1986

Effect of Crystallites on Subcritical Crack Growth and Strain-Rate Sensitivity of Strength of Cordierite Glass-Ceramics journal, March 1985

Effect of Crystallites on Surface Damage and Fracture Behavior of a Glass-Ceramic journal, October 1983

Role of crack size in the bi-modal static fatigue failure of a cordierite glass and glass-ceramic journal, March 1987

Strength and Microstructure in Lithium Disilicate Glass-Ceramics journal, September 1975

Crack deflection processes—II. Experiment
journal, April 1983

Microstructural Characterization and Fracture Toughness of Cordierite-ZrO2 Glass-Ceramics
journal, August 1988

Microstructure and Kinetics of Crystallization of MgO-Al2O3-Si02 Glass-Ceramics
journal, May 1978

Crack deflection processes—I. Theory
journal, April 1983

Crystallization of MgO-Al2O3-SiO2-ZrO2 Glasses
journal, March 1986

Effect of Crystallites on Subcritical Crack Growth and Strain-Rate Sensitivity of Strength of Cordierite Glass-Ceramics
journal, March 1985

Effect of Crystallites on Surface Damage and Fracture Behavior of a Glass-Ceramic
journal, October 1983

Role of crack size in the bi-modal static fatigue failure of a cordierite glass and glass-ceramic
journal, March 1987

Strength and Microstructure in Lithium Disilicate Glass-Ceramics
journal, September 1975