Process for synthesis of beryllium chloride dietherate
Abstract
A low temperature method of producing beryllium chloride dietherate through the addition of hydrogen chloride gas to a mixture of beryllium metal in ether in a reaction vessel is described. A reflux condenser provides an exit for hydrogen produced form the reaction. A distillation condenser later replaces the reflux condenser for purifying the resultant product.
- Inventors:
-
- Baton Rouge, LA
- Kendall Park, NJ
- Lynchburg, VA
- Issue Date:
- OSTI Identifier:
- 867697
- Patent Number(s):
- 4990325
- Assignee:
- Babcock & Wilcox Company (New Orleans, LA)
- Patent Classifications (CPCs):
-
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01F - COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
C - CHEMISTRY C07 - ORGANIC CHEMISTRY C07F - ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- DOE Contract Number:
- BNL-307348-S
- Resource Type:
- Patent
- Country of Publication:
- United States
- Language:
- English
- Subject:
- process; synthesis; beryllium; chloride; dietherate; temperature; method; producing; addition; hydrogen; gas; mixture; metal; reaction; vessel; described; reflux; condenser; provides; exit; produced; form; distillation; replaces; purifying; resultant; product; resultant product; reaction vessel; hydrogen chloride; reflux condenser; hydrogen produced; chloride gas; chloride dietherate; temperature method; beryllium chloride; /423/999/
Citation Formats
Bergeron, Charles, Bullard, John E, and Morgan, Evan. Process for synthesis of beryllium chloride dietherate. United States: N. p., 1991.
Web.
Bergeron, Charles, Bullard, John E, & Morgan, Evan. Process for synthesis of beryllium chloride dietherate. United States.
Bergeron, Charles, Bullard, John E, and Morgan, Evan. Tue .
"Process for synthesis of beryllium chloride dietherate". United States. https://www.osti.gov/servlets/purl/867697.
@article{osti_867697,
title = {Process for synthesis of beryllium chloride dietherate},
author = {Bergeron, Charles and Bullard, John E and Morgan, Evan},
abstractNote = {A low temperature method of producing beryllium chloride dietherate through the addition of hydrogen chloride gas to a mixture of beryllium metal in ether in a reaction vessel is described. A reflux condenser provides an exit for hydrogen produced form the reaction. A distillation condenser later replaces the reflux condenser for purifying the resultant product.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {1991},
month = {1}
}
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