Automated process for solvent separation of organic/inorganic substance

Title: Automated process for solvent separation of organic/inorganic substance

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Abstract

There is described an automated process for the solvent separation of organic/inorganic substances that operates continuously and unattended and eliminates potential errors resulting from subjectivity and the aging of the sample during analysis. In the process, metered amounts of one or more solvents are passed sequentially through a filter containing the sample under the direction of a microprocessor control apparatus. The mixture in the filter is agitated by ultrasonic cavitation for a timed period and the filtrate is collected. The filtrate of each solvent extraction is collected individually and the residue on the filter element is collected to complete the extraction process.

Inventors:

Schweighardt, Frank K ^[1]

Upper Macungie, PA

Issue Date:: 1986-01-01

Research Org.:: International Coal Refining Co

OSTI Identifier:: 865938

Patent Number(s):: 4603115

Assignee:: International Coal Refining Company (Allentown, PA)

Patent Classifications (CPCs):: Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y10 - TECHNICAL SUBJECTS COVERED BY FORMER USPC Y10T - TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION

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Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y10 - TECHNICAL SUBJECTS COVERED BY FORMER USPC Y10T - TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
Y10T436/255 - including use of a solid sorbent, semipermeable membrane, or liquid extraction

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION
B01D11/0219 - {Fixed bed of solid material}

C - CHEMISTRY C10 - PETROLEUM, GAS OR COKE INDUSTRIES C10G - CRACKING HYDROCARBON OILS
C10G1/045 - {Separation of insoluble materials}
C10G1/04 - by extraction

G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
G01N25/14 - by using distillation, extraction, sublimation, condensation, freezing, or crystallisation

C - CHEMISTRY C10 - PETROLEUM, GAS OR COKE INDUSTRIES C10G - CRACKING HYDROCARBON OILS
C10G1/008 - {Controlling or regulating of liquefaction processes

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION
B01D11/0207 - {Control systems}

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y10 - TECHNICAL SUBJECTS COVERED BY FORMER USPC Y10T - TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
Y10T436/21 - Hydrocarbon

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION
B01D11/0261 - {comprising vibrating mechanisms, e.g. mechanical, acoustical}

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DOE Contract Number:: AC05-78OR03054

Resource Type:: Patent

Country of Publication:: United States

Language:: English

Subject:: automated; process; solvent; separation; organic; inorganic; substance; described; substances; operates; continuously; unattended; eliminates; potential; errors; resulting; subjectivity; aging; sample; analysis; metered; amounts; solvents; passed; sequentially; filter; containing; direction; microprocessor; control; apparatus; mixture; agitated; ultrasonic; cavitation; timed; period; filtrate; collected; extraction; individually; residue; element; complete; extraction process; solvent extraction; filter element; control apparatus; ultrasonic cavitation; automated process; microprocessor control; solvent separation; organic substance; organic substances; operates continuously; errors resulting; filter containing; eliminates potential; solvent extract; potential errors; /436/210/422/

Citation Formats


                    Schweighardt, Frank K. Automated process for solvent separation of organic/inorganic substance.  United States: N. p., 1986. 
        Web.

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                    Schweighardt, Frank K. Automated process for solvent separation of organic/inorganic substance.  United States.

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                    Schweighardt, Frank K. Wed .  
        "Automated process for solvent separation of organic/inorganic substance".  United States.  https://www.osti.gov/servlets/purl/865938.

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@article{osti_865938,

  title        = {Automated process for solvent separation of organic/inorganic substance},

  author       = {Schweighardt, Frank K},

  abstractNote = {There is described an automated process for the solvent separation of organic/inorganic substances that operates continuously and unattended and eliminates potential errors resulting from subjectivity and the aging of the sample during analysis. In the process, metered amounts of one or more solvents are passed sequentially through a filter containing the sample under the direction of a microprocessor control apparatus. The mixture in the filter is agitated by ultrasonic cavitation for a timed period and the filtrate is collected. The filtrate of each solvent extraction is collected individually and the residue on the filter element is collected to complete the extraction process.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {1986},

  month        = {1}

}

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