Solids precipitation and polymerization of asphaltenes in coal-derived liquids

Title: Solids precipitation and polymerization of asphaltenes in coal-derived liquids

Full Record
Other Related Research

Abstract

The precipitation and removal of particulate solids from coal-derived liquids by adding a process-derived anti-solvent liquid fraction and continuing the precipitation process at a temperature above the melting point of the mixed liquids for sufficient time to allow the asphaltenes to polymerize and solids to settle at atmospheric pressure conditions. The resulting clarified light hydrocarbon overflow liquid contains less than about 0.02 W % ash and is suitable as turbine fuel or as boiler fuel for burning without particulate emission control equipment. An underflow liquid fraction containing less than about 0.1 W % solids along with low sulfur and nitrogen concentrations is suitable as a boiler fuel with emission control equipment.

Inventors:

Kydd, Paul H ^[1]

Lawrenceville, NJ

Issue Date:: 1984-01-01

Research Org.:: HYDROCARBON RESEARCH INC

OSTI Identifier:: 865155

Patent Number(s):: 4470900

Assignee:: HRI, Inc. (Gibbsboro, NJ)

Patent Classifications (CPCs):: C - CHEMISTRY C10 - PETROLEUM, GAS OR COKE INDUSTRIES C10G - CRACKING HYDROCARBON OILS

Show more

C - CHEMISTRY C10 - PETROLEUM, GAS OR COKE INDUSTRIES C10G - CRACKING HYDROCARBON OILS
C10G1/045 - {Separation of insoluble materials}
C10G1/06 - by destructive hydrogenation

Show less

DOE Contract Number:: AC05-77ET10152

Resource Type:: Patent

Country of Publication:: United States

Language:: English

Subject:: solids; precipitation; polymerization; asphaltenes; coal-derived; liquids; removal; particulate; adding; process-derived; anti-solvent; liquid; fraction; continuing; process; temperature; melting; mixed; sufficient; time; allow; polymerize; settle; atmospheric; pressure; conditions; resulting; clarified; light; hydrocarbon; overflow; contains; 02; ash; suitable; turbine; fuel; boiler; burning; emission; control; equipment; underflow; containing; sulfur; nitrogen; concentrations; particulate solids; coal-derived liquids; particulate solid; light hydrocarbon; mixed liquid; fraction containing; pressure conditions; atmospheric pressure; sufficient time; coal-derived liquid; liquid fraction; precipitation process; derived liquids; boiler fuel; particulate emission; /208/

Citation Formats


                    Kydd, Paul H. Solids precipitation and polymerization of asphaltenes in coal-derived liquids.  United States: N. p., 1984. 
        Web.

Copy to clipboard


                    Kydd, Paul H. Solids precipitation and polymerization of asphaltenes in coal-derived liquids.  United States.

Copy to clipboard


                    Kydd, Paul H. Sun .  
        "Solids precipitation and polymerization of asphaltenes in coal-derived liquids".  United States.  https://www.osti.gov/servlets/purl/865155.

Copy to clipboard


                    
@article{osti_865155,

  title        = {Solids precipitation and polymerization of asphaltenes in coal-derived liquids},

  author       = {Kydd, Paul H},

  abstractNote = {The precipitation and removal of particulate solids from coal-derived liquids by adding a process-derived anti-solvent liquid fraction and continuing the precipitation process at a temperature above the melting point of the mixed liquids for sufficient time to allow the asphaltenes to polymerize and solids to settle at atmospheric pressure conditions. The resulting clarified light hydrocarbon overflow liquid contains less than about 0.02 W % ash and is suitable as turbine fuel or as boiler fuel for burning without particulate emission control equipment. An underflow liquid fraction containing less than about 0.1 W % solids along with low sulfur and nitrogen concentrations is suitable as a boiler fuel with emission control equipment.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {1984},

  month        = {1}

}

Copy to clipboard

Patent:

View Patent

Save / Share:

Export Metadata

Save to My Library

Similar Records in DOE Patents and OSTI.GOV collections:

Apparatus and method for pumping hot, erosive slurry of coal solids in coal derived, water immiscible liquid

Patent Ackerman, Carl D [Olympia, WA]

An apparatus for and method of pumping hot, erosive slurry of coal solids in a coal derived, water immiscible liquid to higher pressure involves the use of a motive fluid which is miscible with the liquid of the slurry. The apparatus includes a pump 12, a remote check valve 14 and a chamber 16 between and in fluid communication with the pump 12 and check valve 14 through conduits 18,20. Pump 12 exerts pressure on the motive fluid and thereby on the slurry through a concentration gradient of coal solids within chamber 16 to alternately discharge slurry under pressure frommore »« less
Full Text Available
Reconstituted polymeric materials derived from post-consumer waste, industrial scrap and virgin resins made by solid state pulverization

Patent Khait, Klementina [Skokie, IL]

A method of making polymeric particulates wherein polymeric scrap material, virgin polymeric material and mixtures thereof are supplied to intermeshing extruder screws which are rotated to transport the polymeric material along their length and subject the polymeric material to solid state shear pulverization and in-situ polymer compatibilization, if two or more incompatible polymers are present. Uniform pulverized particulates are produced without addition of a compatibilizing agent. The pulverized particulates are directly melt processable (as powder feedstock) and surprisingly yield a substantially homogeneous light color product.
Full Text Available
Reconstituted polymeric materials derived from post-consumer waste, industrial scrap and virgin resins made by solid state shear pulverization

Patent Khait, Klementina [Skokie, IL]

A method of making polymeric particulates wherein polymeric scrap material, virgin polymeric material and mixtures thereof are supplied to intermeshing extruder screws which are rotated to transport the polymeric material along their length and subject the polymeric material to solid state shear pulverization and in-situ polymer compatibilization, if two or more incompatible polymers are present. Uniform pulverized particulates are produced without addition of a compatibilizing agent. The pulverized particulates are directly melt processable (as powder feedstock) and surprisingly yield a substantially homogeneous light color product.
Full Text Available
Reconstituted Polymeric Materials Derived From Post-Consumer Waste, Industrial Scrap And Virgin Resins Made By Solid State Shear Pulverizat

Patent Khait, Klementina [Skokie, IL]

A method of making polymeric particulates wherein polymeric scrap material, virgin polymeric material and mixtures thereof are supplied to intermeshing extruder screws which are rotated to transport the polymeric material along their length and subject the polymeric material to solid state shear pulverization and in-situ polymer compatibilization, if two or more incompatible polymers are present. Uniform pulverized particulates are produced without addition of a compatibilizing agent. The pulverized particulates are directly melt processable (as powder feedstock) and surprisingly yield a substantially homogeneous light color product.
Full Text Available
Polymer-encapsulated carbon capture liquids that tolerate precipitation of solids for increased capacity

Patent Aines, Roger D; Bourcier, William L; Spadaccini, Christopher M; ...

A system for carbon dioxide capture from flue gas and other industrial gas sources utilizes microcapsules with very thin polymer shells. The contents of the microcapsules can be liquids or mixtures of liquids and solids. The microcapsules are exposed to the flue gas and other industrial gas and take up carbon dioxide from the flue gas and other industrial gas and eventual precipitate solids in the capsule.
Full Text Available

Similar Records