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Title: Process for reproducibly preparing titanium subhydride

Abstract

Titanium subhydride is produced in a reactor by heating a selected amount of finely divided titanium compound at a selected temperature for a selected period of time under dynamic vacuum conditions. Hydrogen is removed substantially uniformly from each powder grain and there is produced a subhydride of substantially uniform titanium-hydrogen composition. Selection of the amount, temperature and time produces a subhydride of selected titanium-hydrogen composition.

Inventors:
 [1]
  1. West Alexandria, OH
Issue Date:
Research Org.:
Mound Lab., Miamisburg, OH (USA)
OSTI Identifier:
864091
Patent Number(s):
4309230
Assignee:
United States of America as represented by United States (Washington, DC)
Patent Classifications (CPCs):
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C - CHEMISTRY C06 - EXPLOSIVES C06B - EXPLOSIVES OR THERMIC COMPOSITIONS
DOE Contract Number:  
EY-76-C-04-0053
Resource Type:
Patent
Country of Publication:
United States
Language:
English
Subject:
process; reproducibly; preparing; titanium; subhydride; produced; reactor; heating; selected; amount; finely; divided; compound; temperature; period; time; dynamic; vacuum; conditions; hydrogen; removed; substantially; uniformly; powder; grain; uniform; titanium-hydrogen; composition; selection; produces; vacuum conditions; dynamic vacuum; substantially uniformly; substantially uniform; finely divided; selected temperature; titanium compound; preparing titanium; selected period; selected amount; reproducibly preparing; titanium subhydride; divided titanium; /149/423/

Citation Formats

Carlson, Richard S. Process for reproducibly preparing titanium subhydride. United States: N. p., 1982. Web.
Carlson, Richard S. Process for reproducibly preparing titanium subhydride. United States.
Carlson, Richard S. Fri . "Process for reproducibly preparing titanium subhydride". United States. https://www.osti.gov/servlets/purl/864091.
@article{osti_864091,
title = {Process for reproducibly preparing titanium subhydride},
author = {Carlson, Richard S},
abstractNote = {Titanium subhydride is produced in a reactor by heating a selected amount of finely divided titanium compound at a selected temperature for a selected period of time under dynamic vacuum conditions. Hydrogen is removed substantially uniformly from each powder grain and there is produced a subhydride of substantially uniform titanium-hydrogen composition. Selection of the amount, temperature and time produces a subhydride of selected titanium-hydrogen composition.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Fri Jan 01 00:00:00 EST 1982},
month = {Fri Jan 01 00:00:00 EST 1982}
}