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Title: Acid hydrolysis of cellulose to yield glucose

Abstract

A process to yield glucose from cellulose through acid hydrolysis. Cellulose is recovered from cellulosic materials, preferably by pretreating the cellulosic materials by dissolving the cellulosic materials in Cadoxen or a chelating metal caustic swelling solvent and then precipitating the cellulose therefrom. Hydrolysis is accomplished using an acid, preferably dilute sulfuric acid, and the glucose is yielded substantially without side products. Lignin may be removed either before or after hydrolysis.

Inventors:
 [1];  [1];  [1]
  1. West Lafayette, IN
Issue Date:
OSTI Identifier:
863453
Patent Number(s):
4174976
Assignee:
Purdue Research Foundation (West Lafayette, IN)
Patent Classifications (CPCs):
C - CHEMISTRY C13 - SUGAR INDUSTRY C13K - SACCHARIDES, OTHER THAN SUCROSE, OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DI-, OLIGO- OR POLYSACCHARIDES
DOE Contract Number:  
E(11-1)-2755
Resource Type:
Patent
Country of Publication:
United States
Language:
English
Subject:
acid; hydrolysis; cellulose; yield; glucose; process; recovered; cellulosic; materials; preferably; pretreating; dissolving; cadoxen; chelating; metal; caustic; swelling; solvent; precipitating; therefrom; accomplished; dilute; sulfuric; yielded; substantially; products; lignin; removed; cellulosic material; cellulosic materials; sulfuric acid; acid hydrolysis; dilute sulfuric; yield glucose; /127/

Citation Formats

Tsao, George T, Ladisch, Michael R, and Bose, Arindam. Acid hydrolysis of cellulose to yield glucose. United States: N. p., 1979. Web.
Tsao, George T, Ladisch, Michael R, & Bose, Arindam. Acid hydrolysis of cellulose to yield glucose. United States.
Tsao, George T, Ladisch, Michael R, and Bose, Arindam. Mon . "Acid hydrolysis of cellulose to yield glucose". United States. https://www.osti.gov/servlets/purl/863453.
@article{osti_863453,
title = {Acid hydrolysis of cellulose to yield glucose},
author = {Tsao, George T and Ladisch, Michael R and Bose, Arindam},
abstractNote = {A process to yield glucose from cellulose through acid hydrolysis. Cellulose is recovered from cellulosic materials, preferably by pretreating the cellulosic materials by dissolving the cellulosic materials in Cadoxen or a chelating metal caustic swelling solvent and then precipitating the cellulose therefrom. Hydrolysis is accomplished using an acid, preferably dilute sulfuric acid, and the glucose is yielded substantially without side products. Lignin may be removed either before or after hydrolysis.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Mon Jan 01 00:00:00 EST 1979},
month = {Mon Jan 01 00:00:00 EST 1979}
}