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Title: Method for preparing high transition temperature Nb.sub.3 Ge superconductors

Abstract

Bulk coatings of Nb.sub.3 Ge superconductors having transition temperatures in excess of 20 K are readily formed by a chemical vapor deposition technique involving the coreduction of NbCl.sub.5 and GeCl.sub.4 in the presence of hydrogen. The NbCl.sub.5 vapor may advantageously be formed quantitatively in the temperature range of about 250.degree. to 260.degree. C by the chlorination of Nb metal provided the partial pressure of the product NbCl.sub.5 vapor is maintained at or below about 0.1 atm.

Inventors:
 [1];  [2]
  1. Los Alamos, NM
  2. Santa Fe, NM
Issue Date:
Research Org.:
Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
OSTI Identifier:
862943
Patent Number(s):
4054686
Assignee:
United States of America as represented by United States Energy (Washington, DC)
Patent Classifications (CPCs):
Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y10 - TECHNICAL SUBJECTS COVERED BY FORMER USPC Y10T - TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01L - SEMICONDUCTOR DEVICES
Resource Type:
Patent
Country of Publication:
United States
Language:
English
Subject:
method; preparing; transition; temperature; nb; superconductors; bulk; coatings; temperatures; excess; 20; readily; formed; chemical; vapor; deposition; technique; involving; coreduction; nbcl; gecl; presence; hydrogen; advantageously; quantitatively; range; 250; degree; 260; chlorination; metal; provided; partial; pressure; product; maintained; below; atm; chemical vapor; temperature range; vapor deposition; partial pressure; transition temperature; readily formed; transition temperatures; deposition technique; bulk coatings; /427/29/420/423/505/

Citation Formats

Newkirk, Lawrence R, and Valencia, Flavio A. Method for preparing high transition temperature Nb.sub.3 Ge superconductors. United States: N. p., 1977. Web.
Newkirk, Lawrence R, & Valencia, Flavio A. Method for preparing high transition temperature Nb.sub.3 Ge superconductors. United States.
Newkirk, Lawrence R, and Valencia, Flavio A. Sat . "Method for preparing high transition temperature Nb.sub.3 Ge superconductors". United States. https://www.osti.gov/servlets/purl/862943.
@article{osti_862943,
title = {Method for preparing high transition temperature Nb.sub.3 Ge superconductors},
author = {Newkirk, Lawrence R and Valencia, Flavio A},
abstractNote = {Bulk coatings of Nb.sub.3 Ge superconductors having transition temperatures in excess of 20 K are readily formed by a chemical vapor deposition technique involving the coreduction of NbCl.sub.5 and GeCl.sub.4 in the presence of hydrogen. The NbCl.sub.5 vapor may advantageously be formed quantitatively in the temperature range of about 250.degree. to 260.degree. C by the chlorination of Nb metal provided the partial pressure of the product NbCl.sub.5 vapor is maintained at or below about 0.1 atm.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {1977},
month = {1}
}

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