Method for the production of high-purity triaminotrinitrobenzene
Abstract
Triaminotrinitrobenzene is readily formed by the nitration of 1,3,5-trichlorobenzene to 1,3,5-trichloro-2,4,6-trinitrobenzene followed by amination to triaminotrinitrobenzene. The purity of the triaminotrinitrobenzene is significantly improved if, during the amination step, sufficient water is present that the byproduct ammonium chloride formed during the amination is rendered at least semideliquescent.
- Inventors:
-
- Santa Fe, NM
- Issue Date:
- Research Org.:
- Los Alamos National Laboratory (LANL), Los Alamos, NM (United States)
- OSTI Identifier:
- 862870
- Patent Number(s):
- 4032377
- Assignee:
- United States of America as represented by United States Energy (Washington, DC)
- Patent Classifications (CPCs):
-
C - CHEMISTRY C06 - EXPLOSIVES C06B - EXPLOSIVES OR THERMIC COMPOSITIONS
C - CHEMISTRY C07 - ORGANIC CHEMISTRY C07C - ACYCLIC OR CARBOCYCLIC COMPOUNDS
- Resource Type:
- Patent
- Country of Publication:
- United States
- Language:
- English
- Subject:
- method; production; high-purity; triaminotrinitrobenzene; readily; formed; nitration; 5-trichlorobenzene; 5-trichloro-2; 6-trinitrobenzene; followed; amination; purity; significantly; improved; step; sufficient; water; byproduct; ammonium; chloride; rendered; semideliquescent; chloride form; significantly improved; sufficient water; ammonium chloride; readily formed; significantly improve; /999/149/
Citation Formats
Benziger, Theodore M. Method for the production of high-purity triaminotrinitrobenzene. United States: N. p., 1977.
Web.
Benziger, Theodore M. Method for the production of high-purity triaminotrinitrobenzene. United States.
Benziger, Theodore M. Sat .
"Method for the production of high-purity triaminotrinitrobenzene". United States. https://www.osti.gov/servlets/purl/862870.
@article{osti_862870,
title = {Method for the production of high-purity triaminotrinitrobenzene},
author = {Benziger, Theodore M},
abstractNote = {Triaminotrinitrobenzene is readily formed by the nitration of 1,3,5-trichlorobenzene to 1,3,5-trichloro-2,4,6-trinitrobenzene followed by amination to triaminotrinitrobenzene. The purity of the triaminotrinitrobenzene is significantly improved if, during the amination step, sufficient water is present that the byproduct ammonium chloride formed during the amination is rendered at least semideliquescent.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Sat Jan 01 00:00:00 EST 1977},
month = {Sat Jan 01 00:00:00 EST 1977}
}
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