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Title: Method of producing ternary lead molybdenum sulfides

Abstract

The method of preparing Pb.sub.x Mo.sub.y S.sub.z where x = 0.8-1.1, y = 4.5-5.6, and z = 5.4-7.2 comprising the steps of mixing commercial reagent grade powders of the reactants, heating in a sealed, evacuated reaction vessel to a temperature of 950.degree.-1150.degree. C, maintaining the temperature until the compound is formed, and then cooling the compound at a controlled rate not in excess of 4.degree. C per minute.

Inventors:
 [1];  [2];  [3]
  1. Belmont, MA
  2. (Danvers, MA)
  3. Danvers, MA
Issue Date:
OSTI Identifier:
862762
Patent Number(s):
4006107
Application Number:
05/604,384
Assignee:
United States of America as represented by United States Energy (Washington, DC)
Patent Classifications (CPCs):
Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y10 - TECHNICAL SUBJECTS COVERED BY FORMER USPC Y10S - TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01L - SEMICONDUCTOR DEVICES
Resource Type:
Patent
Country of Publication:
United States
Language:
English
Subject:
method; producing; ternary; lead; molybdenum; sulfides; preparing; pb; z; 8-1; 5-5; 4-7; comprising; steps; mixing; commercial; reagent; grade; powders; reactants; heating; sealed; evacuated; reaction; vessel; temperature; 950; degree; -1150; maintaining; compound; formed; cooling; controlled; rate; excess; minute; controlled rate; reaction vessel; molybdenum sulfide; molybdenum sulfides; /252/423/505/

Citation Formats

Foner, Simon, McNiff, Jr., Edward J., and Alexander, Edwin J. Method of producing ternary lead molybdenum sulfides. United States: N. p., 1977. Web.
Foner, Simon, McNiff, Jr., Edward J., & Alexander, Edwin J. Method of producing ternary lead molybdenum sulfides. United States.
Foner, Simon, McNiff, Jr., Edward J., and Alexander, Edwin J. Tue . "Method of producing ternary lead molybdenum sulfides". United States. https://www.osti.gov/servlets/purl/862762.
@article{osti_862762,
title = {Method of producing ternary lead molybdenum sulfides},
author = {Foner, Simon and McNiff, Jr., Edward J. and Alexander, Edwin J},
abstractNote = {The method of preparing Pb.sub.x Mo.sub.y S.sub.z where x = 0.8-1.1, y = 4.5-5.6, and z = 5.4-7.2 comprising the steps of mixing commercial reagent grade powders of the reactants, heating in a sealed, evacuated reaction vessel to a temperature of 950.degree.-1150.degree. C, maintaining the temperature until the compound is formed, and then cooling the compound at a controlled rate not in excess of 4.degree. C per minute.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {1977},
month = {2}
}

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