Method of recycling lithium borate to lithium borohydride through methyl borate
Abstract
This invention provides a method for the recycling of lithium borate to lithium borohydride which can be reacted with water to generate hydrogen for utilization as a fuel. The lithium borate by-product of the hydrogen generation reaction is reacted with hydrogen chloride and water to produce boric acid and lithium chloride. The boric acid and lithium chloride are converted to lithium borohydride through a methyl borate intermediate to complete the recycle scheme.
- Inventors:
- Issue Date:
- Research Org.:
- Aerojet Nuclear Co., Idaho Falls, ID (United States). Idaho National Engineering Lab.
- Sponsoring Org.:
- US Energy Research and Development Administration (ERDA)
- OSTI Identifier:
- 862741
- Patent Number(s):
- 4002726
- Application Number:
- 05/596550
- Assignee:
- United States of America as represented by United States Energy (Washington, DC)
- Patent Classifications (CPCs):
-
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
- DOE Contract Number:
- AT(10-1)-1375
- Resource Type:
- Patent
- Resource Relation:
- Patent File Date: 1975 Jun 16
- Country of Publication:
- United States
- Language:
- English
- Subject:
- method; recycling; lithium; borate; borohydride; methyl; provides; reacted; water; generate; hydrogen; utilization; fuel; by-product; generation; reaction; chloride; produce; boric; acid; converted; intermediate; complete; recycle; scheme; lithium chloride; lithium borohydride; lithium borate; boric acid; hydrogen chloride; hydrogen generation; recycling lithium; methyl borate; generate hydrogen; generation reaction; /423/
Citation Formats
Filby, Evan E. Method of recycling lithium borate to lithium borohydride through methyl borate. United States: N. p., 1977.
Web.
Filby, Evan E. Method of recycling lithium borate to lithium borohydride through methyl borate. United States.
Filby, Evan E. Sat .
"Method of recycling lithium borate to lithium borohydride through methyl borate". United States. https://www.osti.gov/servlets/purl/862741.
@article{osti_862741,
title = {Method of recycling lithium borate to lithium borohydride through methyl borate},
author = {Filby, Evan E.},
abstractNote = {This invention provides a method for the recycling of lithium borate to lithium borohydride which can be reacted with water to generate hydrogen for utilization as a fuel. The lithium borate by-product of the hydrogen generation reaction is reacted with hydrogen chloride and water to produce boric acid and lithium chloride. The boric acid and lithium chloride are converted to lithium borohydride through a methyl borate intermediate to complete the recycle scheme.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {1977},
month = {1}
}