Production of the ammonium salt of 3,5-dinitro-1,2,4-triazole by solvent extraction
Abstract
The ammonium salt of 3,5-dinitro-1,2,4-triazole has utility as a chemical explosive. In accordance with the present invention, it may readily be produced by solvent extraction using high-molecular weight, water-insoluble amines, followed by amination with anhydrous ammonia gas. The aqueous reaction mixture produced in the synthesis of the parent compound, 3,5-dinitro-1,2,4-triazole, is quite suitable - and indeed is preferred - for use as the feed material in the process of the invention.
- Inventors:
- Issue Date:
- OSTI Identifier:
- 6927071
- Assignee:
- Dept. of Energy
- DOE Contract Number:
- W-7405-ENG-36
- Resource Type:
- Patent
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 45 MILITARY TECHNOLOGY, WEAPONRY, AND NATIONAL DEFENSE; CHEMICAL EXPLOSIVES; PRODUCTION; AMMONIUM COMPOUNDS; SOLVENT EXTRACTION; TRIAZOLES; AZOLES; EXPLOSIVES; EXTRACTION; HETEROCYCLIC COMPOUNDS; ORGANIC COMPOUNDS; ORGANIC NITROGEN COMPOUNDS; SEPARATION PROCESSES; 450100* - Military Technology, Weaponry, & National Defense- Chemical Explosions & Explosives
Citation Formats
Lee, K Y, and Ott, D G. Production of the ammonium salt of 3,5-dinitro-1,2,4-triazole by solvent extraction. United States: N. p., 1979.
Web.
Lee, K Y, & Ott, D G. Production of the ammonium salt of 3,5-dinitro-1,2,4-triazole by solvent extraction. United States.
Lee, K Y, and Ott, D G. Wed .
"Production of the ammonium salt of 3,5-dinitro-1,2,4-triazole by solvent extraction". United States.
@article{osti_6927071,
title = {Production of the ammonium salt of 3,5-dinitro-1,2,4-triazole by solvent extraction},
author = {Lee, K Y and Ott, D G},
abstractNote = {The ammonium salt of 3,5-dinitro-1,2,4-triazole has utility as a chemical explosive. In accordance with the present invention, it may readily be produced by solvent extraction using high-molecular weight, water-insoluble amines, followed by amination with anhydrous ammonia gas. The aqueous reaction mixture produced in the synthesis of the parent compound, 3,5-dinitro-1,2,4-triazole, is quite suitable - and indeed is preferred - for use as the feed material in the process of the invention.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {1979},
month = {11}
}
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