Process for synthesizing titanium carbide, titanium nitride and titanium carbonitride
Abstract
A process is disclosed for synthesizing titanium carbide, titanium nitride or titanium carbonitride. The process comprises placing particles of titanium, a titanium salt or titanium dioxide within a vessel and providing a carbon-containing atmosphere within the vessel. The vessel is heated to a pyrolysis temperature sufficient to pyrolyze the carbon to thereby coat the particles with a carbon coating. Thereafter, the carbon-coated particles are heated in an inert atmosphere to produce titanium carbide, or in a nitrogen atmosphere to produce titanium nitride or titanium carbonitride, with the heating being of a temperature and time sufficient to produce a substantially complete solid solution.
- Inventors:
- Issue Date:
- Research Org.:
- National Renewable Energy Laboratory (NREL), Golden, CO (United States)
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 55818
- Patent Number(s):
- 5417952
- Application Number:
- PAN: 8-249,340
- Assignee:
- Midwest Research Institute, Kansas City, MO (United States)
- DOE Contract Number:
- AC02-83CH10093
- Resource Type:
- Patent
- Resource Relation:
- Other Information: PBD: 23 May 1995
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; TITANIUM CARBIDES; SYNTHESIS; TITANIUM NITRIDES; CARBONITRIDES; TITANIUM COMPOUNDS; CONTROLLED ATMOSPHERES
Citation Formats
Koc, R., and Glatzmaier, G. C. Process for synthesizing titanium carbide, titanium nitride and titanium carbonitride. United States: N. p., 1995.
Web.
Koc, R., & Glatzmaier, G. C. Process for synthesizing titanium carbide, titanium nitride and titanium carbonitride. United States.
Koc, R., and Glatzmaier, G. C. Tue .
"Process for synthesizing titanium carbide, titanium nitride and titanium carbonitride". United States.
@article{osti_55818,
title = {Process for synthesizing titanium carbide, titanium nitride and titanium carbonitride},
author = {Koc, R. and Glatzmaier, G. C.},
abstractNote = {A process is disclosed for synthesizing titanium carbide, titanium nitride or titanium carbonitride. The process comprises placing particles of titanium, a titanium salt or titanium dioxide within a vessel and providing a carbon-containing atmosphere within the vessel. The vessel is heated to a pyrolysis temperature sufficient to pyrolyze the carbon to thereby coat the particles with a carbon coating. Thereafter, the carbon-coated particles are heated in an inert atmosphere to produce titanium carbide, or in a nitrogen atmosphere to produce titanium nitride or titanium carbonitride, with the heating being of a temperature and time sufficient to produce a substantially complete solid solution.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue May 23 00:00:00 EDT 1995},
month = {Tue May 23 00:00:00 EDT 1995}
}
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