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Title: MASS SPECTROMETRY

Abstract

method is described for operating a mass spectrometer to improve its resolution qualities and to extend its period of use substantially between cleanings. In this method, a small amount of a beta emitting gas such as hydrogen titride or carbon-14 methane is added to the sample being supplied to the spectrometer for investigation. The additive establishes leakage paths on the surface of the non-conducting film accumulating within the vacuum chamber of the spectrometer, thereby reducing the effect of an accumulated static charge on the electrostatic and magnetic fields established within the instrument. (AEC)

Inventors:
Issue Date:
Research Org.:
Originating Research Org. not identified
OSTI Identifier:
4827161
Patent Number(s):
3016459
Assignee:
U.S. Atomic Energy Commission DTIE; NSA-16-004266
NSA Number:
NSA-16-004266
Resource Type:
Patent
Resource Relation:
Other Information: Orig. Receipt Date: 31-DEC-62
Country of Publication:
United States
Language:
English
Subject:
ENGINEERING AND EQUIPMENT; BETA DECAY; CARBON 14; CLEANING; ELECTRIC CHARGES; GASES; HYDROGEN; LEAKS; MAGNETIC FIELDS; MASS SPECTROMETERS; RESOLUTION; TRACER TECHNIQUES; TRITIUM

Citation Formats

Friedman, L. MASS SPECTROMETRY. United States: N. p., 1962. Web.
Friedman, L. MASS SPECTROMETRY. United States.
Friedman, L. Mon . "MASS SPECTROMETRY". United States.
@article{osti_4827161,
title = {MASS SPECTROMETRY},
author = {Friedman, L.},
abstractNote = {method is described for operating a mass spectrometer to improve its resolution qualities and to extend its period of use substantially between cleanings. In this method, a small amount of a beta emitting gas such as hydrogen titride or carbon-14 methane is added to the sample being supplied to the spectrometer for investigation. The additive establishes leakage paths on the surface of the non-conducting film accumulating within the vacuum chamber of the spectrometer, thereby reducing the effect of an accumulated static charge on the electrostatic and magnetic fields established within the instrument. (AEC)},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {1962},
month = {1}
}