skip to main content
DOE Patents title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: CONVERSION OF DIMETHYL ETHER-BORON TRIFLUORIDE COMPLEX TO POTASSIUM FLUOBORATE

Abstract

A method of preparing KBF/sub 4/ from the dimethyl ether complex of BF/sub 3/ is given. This may be accomplished by introducing the dimethyl ether complex of BF/sub 3/ into an aqueous solution of KF and alcohol, expelling the ether liberated from the complex by heating or stirring and recovering the KBF/sub 4/ so formed. The KBF/sub 4/ is then filtered from the alcohol-water solution, which may be recycled, to reduce the loss of KBF/sub 4/ which is not recovered by filtration.

Inventors:
Issue Date:
Research Org.:
Originating Research Org. not identified
Sponsoring Org.:
USDOE
OSTI Identifier:
4342753
Patent Number(s):
2796323
Assignee:
U.S. Atomic Energy Commission DTIE; NSA-11-011503
NSA Number:
NSA-11-011503
Resource Type:
Patent
Resource Relation:
Other Information: Orig. Receipt Date: 31-DEC-57
Country of Publication:
United States
Language:
English
Subject:
PATENTS; ALCOHOLS; BORATES; BORON FLUORIDES; COMPLEXES; ETHERS; HEATING; LOSSES; POTASSIUM FLUORIDES; PREPARATION; RECOVERY; SOLUTIONS; WATER

Citation Formats

Eberle, A.R. CONVERSION OF DIMETHYL ETHER-BORON TRIFLUORIDE COMPLEX TO POTASSIUM FLUOBORATE. United States: N. p., 1957. Web.
Eberle, A.R. CONVERSION OF DIMETHYL ETHER-BORON TRIFLUORIDE COMPLEX TO POTASSIUM FLUOBORATE. United States.
Eberle, A.R. Tue . "CONVERSION OF DIMETHYL ETHER-BORON TRIFLUORIDE COMPLEX TO POTASSIUM FLUOBORATE". United States.
@article{osti_4342753,
title = {CONVERSION OF DIMETHYL ETHER-BORON TRIFLUORIDE COMPLEX TO POTASSIUM FLUOBORATE},
author = {Eberle, A.R.},
abstractNote = {A method of preparing KBF/sub 4/ from the dimethyl ether complex of BF/sub 3/ is given. This may be accomplished by introducing the dimethyl ether complex of BF/sub 3/ into an aqueous solution of KF and alcohol, expelling the ether liberated from the complex by heating or stirring and recovering the KBF/sub 4/ so formed. The KBF/sub 4/ is then filtered from the alcohol-water solution, which may be recycled, to reduce the loss of KBF/sub 4/ which is not recovered by filtration.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {1957},
month = {6}
}