CONVERSION OF DIMETHYL ETHER-BORON TRIFLUORIDE COMPLEX TO POTASSIUM FLUOBORATE
Abstract
A method of preparing KBF/sub 4/ from the dimethyl ether complex of BF/sub 3/ is given. This may be accomplished by introducing the dimethyl ether complex of BF/sub 3/ into an aqueous solution of KF and alcohol, expelling the ether liberated from the complex by heating or stirring and recovering the KBF/sub 4/ so formed. The KBF/sub 4/ is then filtered from the alcohol-water solution, which may be recycled, to reduce the loss of KBF/sub 4/ which is not recovered by filtration.
- Inventors:
- Issue Date:
- Research Org.:
- Originating Research Org. not identified
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 4342753
- Patent Number(s):
- 2796323
- Assignee:
- U.S. Atomic Energy Commission
- Patent Classifications (CPCs):
-
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
- NSA Number:
- NSA-11-011503
- Resource Type:
- Patent
- Resource Relation:
- Other Information: Orig. Receipt Date: 31-DEC-57
- Country of Publication:
- United States
- Language:
- English
- Subject:
- PATENTS; ALCOHOLS; BORATES; BORON FLUORIDES; COMPLEXES; ETHERS; HEATING; LOSSES; POTASSIUM FLUORIDES; PREPARATION; RECOVERY; SOLUTIONS; WATER
Citation Formats
Eberle, A R. CONVERSION OF DIMETHYL ETHER-BORON TRIFLUORIDE COMPLEX TO POTASSIUM FLUOBORATE. United States: N. p., 1957.
Web.
Eberle, A R. CONVERSION OF DIMETHYL ETHER-BORON TRIFLUORIDE COMPLEX TO POTASSIUM FLUOBORATE. United States.
Eberle, A R. Tue .
"CONVERSION OF DIMETHYL ETHER-BORON TRIFLUORIDE COMPLEX TO POTASSIUM FLUOBORATE". United States.
@article{osti_4342753,
title = {CONVERSION OF DIMETHYL ETHER-BORON TRIFLUORIDE COMPLEX TO POTASSIUM FLUOBORATE},
author = {Eberle, A R},
abstractNote = {A method of preparing KBF/sub 4/ from the dimethyl ether complex of BF/sub 3/ is given. This may be accomplished by introducing the dimethyl ether complex of BF/sub 3/ into an aqueous solution of KF and alcohol, expelling the ether liberated from the complex by heating or stirring and recovering the KBF/sub 4/ so formed. The KBF/sub 4/ is then filtered from the alcohol-water solution, which may be recycled, to reduce the loss of KBF/sub 4/ which is not recovered by filtration.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue Jun 18 00:00:00 EDT 1957},
month = {Tue Jun 18 00:00:00 EDT 1957}
}
Search for the full text at the U.S. Patent and Trademark Office
Note: You will be redirected to the USPTO site, which may require a pop-up blocker to be deactivated to view the patent. If so, you will need to manually turn off your browser's pop-up blocker, typically found within the browser settings. (See DOE Patents FAQs for more information.)
Save to My Library
You must Sign In or Create an Account in order to save documents to your library.