PRODUCTION OF TRIFLUOROACETIC ACID
Abstract
A method is given for the production of improved yields of trifluoroacetic acid. The compound is prepared by oxidizing m-aminobenzotrifluoride with an alkali metal or alkaline earth metal permanganate at a temperature in the range of 80 deg C to 100 deg C while dissolved ln a mixture of water with glacial acetic acid and/or trifluoroacetic acid. Preferably a mixture of water and trifluoroacetic acid ls used as the solvent.
- Inventors:
- Issue Date:
- Research Org.:
- Originating Research Org. not identified
- OSTI Identifier:
- 4337321
- Patent Number(s):
- 2476490
- Assignee:
- U.S. Atomic Energy Commission
- Patent Classifications (CPCs):
-
C - CHEMISTRY C07 - ORGANIC CHEMISTRY C07C - ACYCLIC OR CARBOCYCLIC COMPOUNDS
- NSA Number:
- NSA-12-004580
- Resource Type:
- Patent
- Resource Relation:
- Other Information: (U.S. Atomic Energy Commission). U.S. Patent 2,476,490. Orig. Receipt Date: 31-DEC-58
- Country of Publication:
- United States
- Language:
- English
- Subject:
- PATENTS; ACETIC ACID; ACIDS; ALKALI METALS; ALKALINE EARTH METALS; BENZENE; FLUORINE COMPOUNDS; ORGANIC FLUORINE COMPOUNDS; OXIDATION; PATENT; PRODUCTION; SOLVENTS; TEMPERATURE; WATER
Citation Formats
Haworth, W N, and Stacey, M. PRODUCTION OF TRIFLUOROACETIC ACID. United States: N. p., 1949.
Web.
Haworth, W N, & Stacey, M. PRODUCTION OF TRIFLUOROACETIC ACID. United States.
Haworth, W N, and Stacey, M. Tue .
"PRODUCTION OF TRIFLUOROACETIC ACID". United States.
@article{osti_4337321,
title = {PRODUCTION OF TRIFLUOROACETIC ACID},
author = {Haworth, W N and Stacey, M},
abstractNote = {A method is given for the production of improved yields of trifluoroacetic acid. The compound is prepared by oxidizing m-aminobenzotrifluoride with an alkali metal or alkaline earth metal permanganate at a temperature in the range of 80 deg C to 100 deg C while dissolved ln a mixture of water with glacial acetic acid and/or trifluoroacetic acid. Preferably a mixture of water and trifluoroacetic acid ls used as the solvent.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {1949},
month = {7}
}
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