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Title: TREATMENT OF AMMONIUM NITRATE SOLUTIONS

Abstract

The treatment of waste solutions obtained in the processing of neutron- irradiated uranium containing fission products and ammonium nitrate is described. The object of this process is to provide a method whereby the ammonium nitrate is destroyed and removed from the solution so as to permit subsequent concentration of the solution.. In accordance with the process the residual nitrate solutions are treated with an excess of alkyl acid anhydride, such as acetic anhydride. Preferably, the residual nitrate solution is added to an excess of the acetic anhydride at such a rate that external heat is not required. The result of this operation is that the ammonium nitrate and acetic anhydride react to form N/sub 2/ O and acetic acid.

Inventors:
; ;
Issue Date:
Research Org.:
Originating Research Org. not identified
OSTI Identifier:
4310773
Patent Number(s):
2838368
Assignee:
U.S. Atomic Energy Commission
Patent Classifications (CPCs):
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01C - AMMONIA
NSA Number:
NSA-12-014413
Resource Type:
Patent
Resource Relation:
Other Information: Orig. Receipt Date: 31-DEC-58
Country of Publication:
United States
Language:
English
Subject:
PATENTS; ACETIC ACID; ACIDS; ALKYL RADICALS; AMMONIUM COMPOUNDS; CHEMICAL REACTIONS; ENRICHMENT; FISSION PRODUCTS; HEATING; NEUTRON BEAMS; NITRATES; NITROGEN OXIDES; NUCLEAR REACTIONS; PATENT; SOLUTIONS; URANIUM; WASTE SOLUTIONS

Citation Formats

Boyer, T W, MacHutchin, J G, and Yaffe, L. TREATMENT OF AMMONIUM NITRATE SOLUTIONS. United States: N. p., 1958. Web.
Boyer, T W, MacHutchin, J G, & Yaffe, L. TREATMENT OF AMMONIUM NITRATE SOLUTIONS. United States.
Boyer, T W, MacHutchin, J G, and Yaffe, L. Tue . "TREATMENT OF AMMONIUM NITRATE SOLUTIONS". United States.
@article{osti_4310773,
title = {TREATMENT OF AMMONIUM NITRATE SOLUTIONS},
author = {Boyer, T W and MacHutchin, J G and Yaffe, L},
abstractNote = {The treatment of waste solutions obtained in the processing of neutron- irradiated uranium containing fission products and ammonium nitrate is described. The object of this process is to provide a method whereby the ammonium nitrate is destroyed and removed from the solution so as to permit subsequent concentration of the solution.. In accordance with the process the residual nitrate solutions are treated with an excess of alkyl acid anhydride, such as acetic anhydride. Preferably, the residual nitrate solution is added to an excess of the acetic anhydride at such a rate that external heat is not required. The result of this operation is that the ammonium nitrate and acetic anhydride react to form N/sub 2/ O and acetic acid.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {1958},
month = {6}
}

Patent:
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