SEPARATING PROTOACTINIUM WITH MANGANESE DIOXIDE
Abstract
The preparation of U/sup 235/ and an improved method for isolating Pa/ sup 233/ from foreign products present in neutronirradiated thorium is described. The method comprises forming a solution of neutron-irradiated thorium together with a manganous salt, then adding potassium permanganate to precipitate the manganese as manganese dioxide whereby protoactinium is carried down with the nnanganese dioxide dissolving the precipitate, adding a soluble zirconium salt, and adding phosphate ion to precipitate zirconium phosphate whereby protoactinium is then carried down with the zirconium phosphate to effect a further concentration.
- Inventors:
- Issue Date:
- Research Org.:
- Originating Research Org. not identified
- OSTI Identifier:
- 4309760
- Patent Number(s):
- 2831750
- Assignee:
- U.S. Atomic Energy Commission
- Patent Classifications (CPCs):
-
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01G - COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- NSA Number:
- NSA-12-014396
- Resource Type:
- Patent
- Resource Relation:
- Other Information: Orig. Receipt Date: 31-DEC-58
- Country of Publication:
- United States
- Language:
- English
- Subject:
- PATENTS; ENRICHMENT; IONS; IRRADIATION; MANGANESE COMPOUNDS; MANGANESE OXIDES; NEUTRON BEAMS; PATENT; PERMANGANATES; PHOSPHATES; POTASSIUM; POTASSIUM COMPOUNDS; PRECIPITATION; PROTACTINIUM 233; SOLUBILITY; SOLUTIONS; THORIUM; URANIUM 233; ZIRCONIUM COMPOUNDS
Citation Formats
Seaborg, G T, Gofman, J W, and Stoughton, R W. SEPARATING PROTOACTINIUM WITH MANGANESE DIOXIDE. United States: N. p., 1958.
Web.
Seaborg, G T, Gofman, J W, & Stoughton, R W. SEPARATING PROTOACTINIUM WITH MANGANESE DIOXIDE. United States.
Seaborg, G T, Gofman, J W, and Stoughton, R W. Tue .
"SEPARATING PROTOACTINIUM WITH MANGANESE DIOXIDE". United States.
@article{osti_4309760,
title = {SEPARATING PROTOACTINIUM WITH MANGANESE DIOXIDE},
author = {Seaborg, G T and Gofman, J W and Stoughton, R W},
abstractNote = {The preparation of U/sup 235/ and an improved method for isolating Pa/ sup 233/ from foreign products present in neutronirradiated thorium is described. The method comprises forming a solution of neutron-irradiated thorium together with a manganous salt, then adding potassium permanganate to precipitate the manganese as manganese dioxide whereby protoactinium is carried down with the nnanganese dioxide dissolving the precipitate, adding a soluble zirconium salt, and adding phosphate ion to precipitate zirconium phosphate whereby protoactinium is then carried down with the zirconium phosphate to effect a further concentration.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {1958},
month = {4}
}