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Title: NON-AQUEOUS DISSOLUTION OF MASSIVE PLUTONIUM

Abstract

A method is presented for obtaining non-aqueous solutions or plutonium from massive forms of the metal. In the present invention massive plutonium is added to a salt melt consisting of 10 to 40 weight per cent of sodium chloride and the balance zinc chloride. The plutonium reacts at about 800 deg C with the zinc chloride to form a salt bath of plutonium trichloride, sodium chloride, and metallic zinc. The zinc is separated from the salt melt by forcing the molten mixture through a Pyrex filter.

Inventors:
; ;
Issue Date:
Research Org.:
Originating Research Org. not identified
OSTI Identifier:
4212401
Patent Number(s):
2886410
Assignee:
U.S. Atomic Energy Commission
Patent Classifications (CPCs):
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01G - COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
C - CHEMISTRY C22 - METALLURGY C22B - PRODUCTION AND REFINING OF METALS
NSA Number:
NSA-13-022507
Resource Type:
Patent
Resource Relation:
Other Information: Orig. Receipt Date: 31-DEC-59
Country of Publication:
United States
Language:
English
Subject:
METALLURGY AND CERAMICS; FILTERS; FUSED SALTS; GLASS; HIGH TEMPERATURE; PLUTONIUM; PLUTONIUM CHLORIDES; PYREX; SEPARATION PROCESSES; SODIUM CHLORIDES; SOLUTIONS; ZINC; ZINC CHLORIDES

Citation Formats

Reavis, J G, Leary, J A, and Walsh, K A. NON-AQUEOUS DISSOLUTION OF MASSIVE PLUTONIUM. United States: N. p., 1959. Web.
Reavis, J G, Leary, J A, & Walsh, K A. NON-AQUEOUS DISSOLUTION OF MASSIVE PLUTONIUM. United States.
Reavis, J G, Leary, J A, and Walsh, K A. Tue . "NON-AQUEOUS DISSOLUTION OF MASSIVE PLUTONIUM". United States.
@article{osti_4212401,
title = {NON-AQUEOUS DISSOLUTION OF MASSIVE PLUTONIUM},
author = {Reavis, J G and Leary, J A and Walsh, K A},
abstractNote = {A method is presented for obtaining non-aqueous solutions or plutonium from massive forms of the metal. In the present invention massive plutonium is added to a salt melt consisting of 10 to 40 weight per cent of sodium chloride and the balance zinc chloride. The plutonium reacts at about 800 deg C with the zinc chloride to form a salt bath of plutonium trichloride, sodium chloride, and metallic zinc. The zinc is separated from the salt melt by forcing the molten mixture through a Pyrex filter.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {1959},
month = {5}
}

Patent:
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