METHOD OF PRODUCING NIOBIUM METAL
Abstract
A process is given for preparing ductile niobium metal by the reduction of niobium pentoxide with carbon. The invention resides in the addition, to the reaction mass, of from 0.05 to 0.4 atom of titanium (in the form of metallic titanium, titanium carbide, and/or titanium oxide) per one mole of niobium pentoxide. The mixture is heated under subatmospheric pressure to above 1300 deg C but below the melting point of niobium, and the carbon- and oxygen-free niobium sponge obtained is cooled under reduced pressure.
- Inventors:
- Issue Date:
- Research Org.:
- Originating Research Org. not identified
- OSTI Identifier:
- 4169498
- Patent Number(s):
- 2937939
- Assignee:
- U.S. Atomic Energy Commission DTIE; NSA-14-021923
- NSA Number:
- NSA-14-021923
- Resource Type:
- Patent
- Resource Relation:
- Other Information: Orig. Receipt Date: 31-DEC-60
- Country of Publication:
- United States
- Language:
- English
- Subject:
- METALS, CERAMICS, AND OTHER MATERIALS; ADDITIVES; CARBON; COOLING; DUCTILITY; HEATING; HIGH TEMPERATURE; NIOBIUM; NIOBIUM OXIDES; PREPARATION; PRESSURE; REDUCTION; TITANIUM; TITANIUM CARBIDES; TITANIUM OXIDES
Citation Formats
Wilhelm, H.A., and Stevens, E.R. METHOD OF PRODUCING NIOBIUM METAL. United States: N. p., 1960.
Web.
Wilhelm, H.A., & Stevens, E.R. METHOD OF PRODUCING NIOBIUM METAL. United States.
Wilhelm, H.A., and Stevens, E.R. Tue .
"METHOD OF PRODUCING NIOBIUM METAL". United States.
@article{osti_4169498,
title = {METHOD OF PRODUCING NIOBIUM METAL},
author = {Wilhelm, H.A. and Stevens, E.R.},
abstractNote = {A process is given for preparing ductile niobium metal by the reduction of niobium pentoxide with carbon. The invention resides in the addition, to the reaction mass, of from 0.05 to 0.4 atom of titanium (in the form of metallic titanium, titanium carbide, and/or titanium oxide) per one mole of niobium pentoxide. The mixture is heated under subatmospheric pressure to above 1300 deg C but below the melting point of niobium, and the carbon- and oxygen-free niobium sponge obtained is cooled under reduced pressure.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {1960},
month = {5}
}
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