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Title: SINTERING METAL OXIDES

Abstract

A process is given for producing uranium dioxide material of great density by preparing a compacted mixture of uranium dioxide and from 1 to 3 wt.% of calcium hydride, heating the mixture to at least 675 deg C for decomposition of the hydride and then for sintering, preferably in a vacuum, at from 1550 to 2000 deg C. Calcium metal is formed, some uranium is reduced by the calcium to the metal and a product of high density is obtained.

Inventors:
Issue Date:
Research Org.:
Originating Research Org. not identified
OSTI Identifier:
4112241
Patent Number(s):
2952535
Assignee:
U.S. Atomic Energy Commission
Patent Classifications (CPCs):
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01G - COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01P - INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
NSA Number:
NSA-15-007697
Resource Type:
Patent
Resource Relation:
Other Information: Orig. Receipt Date: 31-DEC-61
Country of Publication:
United States
Language:
English
Subject:
METALS, CERAMICS, AND OTHER MATERIALS; CALCIUM; CALCIUM HYDRIDES; DECOMPOSITION; DENSITY; HEATING; HIGH TEMPERATURE; MIXING; PRODUCTION; REDUCTION; SINTERING; URANIUM; URANIUM DIOXIDE; VACUUM

Citation Formats

Roake, W E. SINTERING METAL OXIDES. United States: N. p., 1960. Web.
Roake, W E. SINTERING METAL OXIDES. United States.
Roake, W E. Tue . "SINTERING METAL OXIDES". United States.
@article{osti_4112241,
title = {SINTERING METAL OXIDES},
author = {Roake, W E},
abstractNote = {A process is given for producing uranium dioxide material of great density by preparing a compacted mixture of uranium dioxide and from 1 to 3 wt.% of calcium hydride, heating the mixture to at least 675 deg C for decomposition of the hydride and then for sintering, preferably in a vacuum, at from 1550 to 2000 deg C. Calcium metal is formed, some uranium is reduced by the calcium to the metal and a product of high density is obtained.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {1960},
month = {9}
}

Patent:
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