Ionically conductive powders and films, and methods of preparation

Kercher, Andrew K.; Westover, Andrew S.; Abdelmalak, Michael Naguib; Dudney, Nancy J.

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Title: Ionically conductive powders and films, and methods of preparation

Abstract

A solid ionically conductive composition (e.g., nanoparticles of less than 1 micron or a continuous film) comprising at least one element selected from alkali metal, alkaline earth metal, aluminum, zinc, copper, and silver in combination with at least two elements selected from oxygen, sulfur, silicon, phosphorus, nitrogen, boron, gallium, indium, tin, germanium, arsenic, antimony, bismuth, transition metals, and lanthanides. Also described is a battery comprising an anode, a cathode, and a solid electrolyte (corresponding to the above ionically conductive composition) in contact with or as part of the anode and/or cathode. Further described is a thermal (e.g., plasma-based) method of producing the ionically conductive composition. Further described is a method for using an additive manufacturing (AM) process to produce an object constructed of the ionically conductive composition by use of particles of the ionically conductive composition as a feed material in the AM process.

Inventors:: Kercher, Andrew K.; Westover, Andrew S.; Abdelmalak, Michael Naguib; Dudney, Nancy J.

Issue Date:: 2023-11-07

Research Org.:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 2293816

Patent Number(s):: 11807543

Application Number:: 16/944,293

Assignee:: UT-Battelle, LLC (Oak Ridge, TN)

DOE Contract Number:: AC05-00OR22725

Resource Type:: Patent

Resource Relation:: Patent File Date: 07/31/2020

Country of Publication:: United States

Language:: English

Citation Formats


                    Kercher, Andrew K., Westover, Andrew S., Abdelmalak, Michael Naguib, and Dudney, Nancy J. Ionically conductive powders and films, and methods of preparation.  United States: N. p., 2023. 
        Web.

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                    Kercher, Andrew K., Westover, Andrew S., Abdelmalak, Michael Naguib, & Dudney, Nancy J. Ionically conductive powders and films, and methods of preparation.  United States.

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                    Kercher, Andrew K., Westover, Andrew S., Abdelmalak, Michael Naguib, and Dudney, Nancy J. Tue .  
        "Ionically conductive powders and films, and methods of preparation".  United States.  https://www.osti.gov/servlets/purl/2293816.

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@article{osti_2293816,

  title        = {Ionically conductive powders and films, and methods of preparation},

  author       = {Kercher, Andrew K. and Westover, Andrew S. and Abdelmalak, Michael Naguib and Dudney, Nancy J.},

  abstractNote = {A solid ionically conductive composition (e.g., nanoparticles of less than 1 micron or a continuous film) comprising at least one element selected from alkali metal, alkaline earth metal, aluminum, zinc, copper, and silver in combination with at least two elements selected from oxygen, sulfur, silicon, phosphorus, nitrogen, boron, gallium, indium, tin, germanium, arsenic, antimony, bismuth, transition metals, and lanthanides. Also described is a battery comprising an anode, a cathode, and a solid electrolyte (corresponding to the above ionically conductive composition) in contact with or as part of the anode and/or cathode. Further described is a thermal (e.g., plasma-based) method of producing the ionically conductive composition. Further described is a method for using an additive manufacturing (AM) process to produce an object constructed of the ionically conductive composition by use of particles of the ionically conductive composition as a feed material in the AM process.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2023},

  month        = {11}

}

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Works referenced in this record:

Mixed alkali silicophosphate oxynitride glasses: Structure-property relations
journal, April 2017

Paraschiv, Georgiana Laura; Muñoz, Francisco; Tricot, Gregory
Journal of Non-Crystalline Solids, Vol. 462
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Thin film battery and method for making same
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Bates, John B.; Dudney, Nancy J.; Gruzalski, Greg R.
US Patent Document 5,338,625
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Preparation of phosphorus oxynitride glasses
journal, August 1986

Reidmeyer, Mary R.; Rajaram, Mohan; Day, Delbert E.
Journal of Non-Crystalline Solids, Vol. 85, Issue 1-2
https://doi.org/10.1016/0022-3093(86)90090-6

Ionic conductivities and structure of lithium phosphorus oxynitride glasses
journal, April 1995

Wang, B.; Kwak, B. S.; Sales, B. C.
Journal of Non-Crystalline Solids, Vol. 183, Issue 3
https://doi.org/10.1016/0022-3093(94)00665-2

Lithium sulfide compositions for battery electrolyte and battery electrode coatings
patent, December 2013

Liang, Chengdu; Liu, Zengcai; Fu, Wunjun
US Patent Document 8,597,838
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Impact of nitridation of metaphosphate glasses on liquid fragility
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Paraschiv, Georgiana Laura; Muñoz, Francisco; Jensen, Lars R.
Journal of Non-Crystalline Solids, Vol. 441
https://doi.org/10.1016/j.jnoncrysol.2016.03.009

An interpretation for the increase of ionic conductivity by nitrogen incorporation in LiPON oxynitride glasses
journal, February 2013

Mascaraque, Nerea; Fierro, José Luis G.; Durán, Alicia
Solid State Ionics, Vol. 233
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Plasma Synthesis of Spherical Crystalline and Amorphous Electrolyte Nanopowders for Solid-State Batteries
journal, February 2020

Westover, Andrew S.; Kercher, Andrew K.; Kornbluth, Mordechai
ACS Applied Materials & Interfaces, Vol. 12, Issue 10
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Solid electrolyte and all solid state battery containing same
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Ugaji, Masaya; Mino, Shinji; Shibano, Yasuyuki
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Lithium sulfide compositions for battery electrolyte and battery electrode coatings
patent, October 2014

Liang, Chengdu; Liu, Zengcai; Fu, Wujun
US Patent Document 8,871,391
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Nano-Engineered Coatings for Anode Active Materials, Cathode Active Materials, and Solid-State Electrolytes and Methods of Making Batteries Containing Nano-Engineered Coatings
patent-application, December 2016

Albano, Fabio; Dahlberg, Kevin; Anderson, Erik
US Patent Application 15/170374; 20160351973
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High conducting oxide—sulfide composite lithium superionic conductor
patent, January 2017

Liang, Chengdu; Rangasamy, Ezhiylmurugan; Dudney, Nancy J.
US Patent Document 9,548,512
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High energy density secondary lithium batteries
patent, March 2019

Nanda, Jagjit; Dudney, Nancy J.; Narula, Chaitanya K.
US Patent Document 10,224,565
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Vitreous Solid Electrolyte Sheets of Li Ion Conducting Sulfur-based Glass and Associated Structures, Cells and Methods
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Visco, Steven J.; NImon, Yevgeniy S.; De Jonghe, Lutgard C.
US Patent Application 14/954812; 20160190640
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Kawaji, Jun; Yamaki, Takahiro
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Similar Records

Title: Ionically conductive powders and films, and methods of preparation

Abstract

Citation Formats

Mixed alkali silicophosphate oxynitride glasses: Structure-property relations journal, April 2017

Thin film battery and method for making same patent, August 1994

Preparation of phosphorus oxynitride glasses journal, August 1986

Ionic conductivities and structure of lithium phosphorus oxynitride glasses journal, April 1995

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Plasma Synthesis of Spherical Crystalline and Amorphous Electrolyte Nanopowders for Solid-State Batteries journal, February 2020

Solid electrolyte and all solid state battery containing same patent, April 2009

Lithium sulfide compositions for battery electrolyte and battery electrode coatings patent, October 2014

Nano-Engineered Coatings for Anode Active Materials, Cathode Active Materials, and Solid-State Electrolytes and Methods of Making Batteries Containing Nano-Engineered Coatings patent-application, December 2016

High conducting oxide—sulfide composite lithium superionic conductor patent, January 2017

High energy density secondary lithium batteries patent, March 2019

Vitreous Solid Electrolyte Sheets of Li Ion Conducting Sulfur-based Glass and Associated Structures, Cells and Methods patent-application, June 2016

Solid electrolyte and all-solid state lithium ion secondary battery patent, December 2017

Mixed alkali silicophosphate oxynitride glasses: Structure-property relations
journal, April 2017

Thin film battery and method for making same
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Preparation of phosphorus oxynitride glasses
journal, August 1986

Ionic conductivities and structure of lithium phosphorus oxynitride glasses
journal, April 1995

Lithium sulfide compositions for battery electrolyte and battery electrode coatings
patent, December 2013

Impact of nitridation of metaphosphate glasses on liquid fragility
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An interpretation for the increase of ionic conductivity by nitrogen incorporation in LiPON oxynitride glasses
journal, February 2013

Plasma Synthesis of Spherical Crystalline and Amorphous Electrolyte Nanopowders for Solid-State Batteries
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Solid electrolyte and all solid state battery containing same
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Lithium sulfide compositions for battery electrolyte and battery electrode coatings
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Nano-Engineered Coatings for Anode Active Materials, Cathode Active Materials, and Solid-State Electrolytes and Methods of Making Batteries Containing Nano-Engineered Coatings
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High conducting oxide—sulfide composite lithium superionic conductor
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Vitreous Solid Electrolyte Sheets of Li Ion Conducting Sulfur-based Glass and Associated Structures, Cells and Methods
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