Solvothermal synthesis of metal alkanoate and metal oxide nanoparticles
Abstract
A facile solvothermal method can be used to synthesize metal alkanoate nanoparticles using a metal nitrate precursor, alcohol/water, and alkanoic acid. The method can produce lanthanide (e.g., La, Ce, Pr, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, or Yb) and transition metal (e.g., Ag, Co, Cu, or Pb) alkanoate nanoparticles (<100 nm) with spherical morphology. These hybrid nanomaterials adopt a lamellar structure consisting of inorganic metal cation layers separated by an alkanoate anion bilayer and exhibit liquid crystalline phases during melting. The metal alkanoate nanoparticles can be calcined to produce metal oxide nanoparticles.
- Inventors:
- Issue Date:
- Research Org.:
- Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 2293662
- Patent Number(s):
- 11773046
- Application Number:
- 17/315,497
- Assignee:
- National Technology & Engineering Solutions of Sandia, LLC (Albuquerque, NM)
- DOE Contract Number:
- NA0003525
- Resource Type:
- Patent
- Resource Relation:
- Patent File Date: 05/10/2021
- Country of Publication:
- United States
- Language:
- English
Citation Formats
Treadwell, LaRico Juan, and Davis-Wheeler, Clare. Solvothermal synthesis of metal alkanoate and metal oxide nanoparticles. United States: N. p., 2023.
Web.
Treadwell, LaRico Juan, & Davis-Wheeler, Clare. Solvothermal synthesis of metal alkanoate and metal oxide nanoparticles. United States.
Treadwell, LaRico Juan, and Davis-Wheeler, Clare. Tue .
"Solvothermal synthesis of metal alkanoate and metal oxide nanoparticles". United States. https://www.osti.gov/servlets/purl/2293662.
@article{osti_2293662,
title = {Solvothermal synthesis of metal alkanoate and metal oxide nanoparticles},
author = {Treadwell, LaRico Juan and Davis-Wheeler, Clare},
abstractNote = {A facile solvothermal method can be used to synthesize metal alkanoate nanoparticles using a metal nitrate precursor, alcohol/water, and alkanoic acid. The method can produce lanthanide (e.g., La, Ce, Pr, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, or Yb) and transition metal (e.g., Ag, Co, Cu, or Pb) alkanoate nanoparticles (<100 nm) with spherical morphology. These hybrid nanomaterials adopt a lamellar structure consisting of inorganic metal cation layers separated by an alkanoate anion bilayer and exhibit liquid crystalline phases during melting. The metal alkanoate nanoparticles can be calcined to produce metal oxide nanoparticles.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue Oct 03 00:00:00 EDT 2023},
month = {Tue Oct 03 00:00:00 EDT 2023}
}
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