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Title: Metal boride aerogels

Abstract

A metal boride aerogel includes a three-dimensional aerogel structure comprising metal boride particles having an average diameter of less than one micron. A method is disclosed for forming a metal boride aerogel including dispersing boron nanoparticles in a solution of a metal salt, forming a boron-loaded metal oxide precursor gel using the dispersed boron nanoparticles in the solution of the metal salt, drying the boron-loaded metal oxide precursor gel to form a boron-loaded metal oxide precursor aerogel, and heating the boron-loaded metal oxide precursor aerogel to form a metal boride aerogel. The metal boride aerogel is essentially free of metal oxide.

Inventors:
; ;
Issue Date:
Research Org.:
Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1998251
Patent Number(s):
11617998
Application Number:
16/810,672
Assignee:
Lawrence Livermore National Security, LLC (Livermore, CA)
DOE Contract Number:  
AC52-07NA27344
Resource Type:
Patent
Resource Relation:
Patent File Date: 03/05/2020
Country of Publication:
United States
Language:
English

Citation Formats

Worsley, Marcus A., Baumann, Theodore F., and Kuntz, Joshua. Metal boride aerogels. United States: N. p., 2023. Web.
Worsley, Marcus A., Baumann, Theodore F., & Kuntz, Joshua. Metal boride aerogels. United States.
Worsley, Marcus A., Baumann, Theodore F., and Kuntz, Joshua. Tue . "Metal boride aerogels". United States. https://www.osti.gov/servlets/purl/1998251.
@article{osti_1998251,
title = {Metal boride aerogels},
author = {Worsley, Marcus A. and Baumann, Theodore F. and Kuntz, Joshua},
abstractNote = {A metal boride aerogel includes a three-dimensional aerogel structure comprising metal boride particles having an average diameter of less than one micron. A method is disclosed for forming a metal boride aerogel including dispersing boron nanoparticles in a solution of a metal salt, forming a boron-loaded metal oxide precursor gel using the dispersed boron nanoparticles in the solution of the metal salt, drying the boron-loaded metal oxide precursor gel to form a boron-loaded metal oxide precursor aerogel, and heating the boron-loaded metal oxide precursor aerogel to form a metal boride aerogel. The metal boride aerogel is essentially free of metal oxide.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2023},
month = {4}
}

Works referenced in this record:

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Ultra-Lightweight Energy Storage Material
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patent-application, January 2009


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patent-application, January 2015


TiB 2 Powders Synthesis by Borothermal Reduction in TiO 2 Under Vacuum
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