Melamine modification of fuel cell electrodes

Strmcnik, Dusan; Farinazzo Bergamo Dias Martins, Pedro; Zorko, Milena; Lv, Haifeng; Stamenkovic, Vojislav

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Title: Melamine modification of fuel cell electrodes

Abstract

A method for forming a melamine-modified electrode that includes providing a metal based electrode and patterning a surface of the metal-based electrode by contacting the electrode with a melamine solution to form a patterned metal-based electrode. The patterned metal-based electrode includes metal sites blocked with melamine molecules and metal sites which are not blocked such that the metal-based electrode selectively adsorbs O2 instead of at least one of sulfate, phosphate, or sulphonate. A range of 20% to 40% of the metal sites are blocked with melamine molecules.

Inventors:: Strmcnik, Dusan; Farinazzo Bergamo Dias Martins, Pedro; Zorko, Milena; Lv, Haifeng; Stamenkovic, Vojislav

Issue Date:: 2023-01-10

Research Org.:: Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1987024

Patent Number(s):: 11552302

Application Number:: 17/481,042

Assignee:: UChicago Argonne, LLC (Chicago, IL)

DOE Contract Number:: AC02-06CH11357

Resource Type:: Patent

Resource Relation:: Patent File Date: 09/21/2021

Country of Publication:: United States

Language:: English

Citation Formats


                    Strmcnik, Dusan, Farinazzo Bergamo Dias Martins, Pedro, Zorko, Milena, Lv, Haifeng, and Stamenkovic, Vojislav. Melamine modification of fuel cell electrodes.  United States: N. p., 2023. 
        Web.

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                    Strmcnik, Dusan, Farinazzo Bergamo Dias Martins, Pedro, Zorko, Milena, Lv, Haifeng, & Stamenkovic, Vojislav. Melamine modification of fuel cell electrodes.  United States.

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                    Strmcnik, Dusan, Farinazzo Bergamo Dias Martins, Pedro, Zorko, Milena, Lv, Haifeng, and Stamenkovic, Vojislav. Tue .  
        "Melamine modification of fuel cell electrodes".  United States.  https://www.osti.gov/servlets/purl/1987024.

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@article{osti_1987024,

  title        = {Melamine modification of fuel cell electrodes},

  author       = {Strmcnik, Dusan and Farinazzo Bergamo Dias Martins, Pedro and Zorko, Milena and Lv, Haifeng and Stamenkovic, Vojislav},

  abstractNote = {A method for forming a melamine-modified electrode that includes providing a metal based electrode and patterning a surface of the metal-based electrode by contacting the electrode with a melamine solution to form a patterned metal-based electrode. The patterned metal-based electrode includes metal sites blocked with melamine molecules and metal sites which are not blocked such that the metal-based electrode selectively adsorbs O2 instead of at least one of sulfate, phosphate, or sulphonate. A range of 20% to 40% of the metal sites are blocked with melamine molecules.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2023},

  month        = {1}

}

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Similar Records

Title: Melamine modification of fuel cell electrodes

Abstract

Citation Formats

Oxygen Electrochemistry as a Cornerstone for Sustainable Energy Conversion journal, December 2013

Mesostructured thin films as electrocatalysts with tunable composition and surface morphology journal, November 2012

Recent Advances in Electrocatalysts for Oxygen Reduction Reaction journal, February 2016

Voltammetric and spectroscopic characterization of cyanide adlayers on Pt(h,k,l) in an acidic medium journal, January 1998

Isotopological Supramolecular Networks from Melamine and Fatty Acids journal, December 2008

Hydrogen-Bonded Structures of Trimesic and Melamine on Highly Oriented Pyrolytic Graphite journal, June 2014

Understanding Catalytic Activity Trends in the Oxygen Reduction Reaction journal, December 2017

Fuel Cell Electrodes patent-application, January 2013

Electrolyte-Dependent Oxygen Evolution Reactions in Alkaline Media: Electrical Double Layer and Interfacial Interactions journal, August 2019

Oxygen Reduction on Platinum Low-Index Single-Crystal Surfaces in Sulfuric Acid Solution: Rotating Ring-Pt(hkl) Disk Studies journal, March 1995

Structural Effects on the Oxygen Reduction Reaction on Pt Single-Crystal Electrodes Modified with Melamine journal, February 2020

Unique Activity of Platinum Adislands in the CO Electrooxidation Reaction journal, November 2008

Selective catalysts for the hydrogen oxidation and oxygen reduction reactions by patterning of platinum with calix[4]arene molecules journal, October 2010

Trends in activity for the water electrolyser reactions on 3d M(Ni,Co,Fe,Mn) hydr(oxy)oxide catalysts journal, May 2012

Self-Assembled Melamine Monolayer on Cu(111) journal, May 2013

Self-Assembly of Upright, Partially Dehydrogenated Melamine on Pd(111) journal, October 2013

Potential modulated reflectance spectroscopy of Pt(111) in acidic and alkaline media: cyanide adsorption journal, March 1999

Cyclic Voltammetry, FTIRS, and DEMS Study of the Electrooxidation of Carbon Monoxide, Formic Acid, and Methanol on Cyanide-Modified Pt(111) Electrodes journal, June 2009

Lattice-strain control of the activity in dealloyed core–shell fuel cell catalysts journal, April 2010

pH and potential dependence of the electrical double layer at well-defined electrode surfaces: Cs + and Ca 2+ ions at Pt(111) (2√3 X. 2√.3)R30°-CN, Pt(111) (√13 X√.13)R14°-CN, and Pt(111) (2 X 2)-SCN journal, September 1985

Alloys of platinum and early transition metals as oxygen reduction electrocatalysts journal, September 2009

Spectroelectrochemical study on CN− adsorbed at Pt(111) in sulphuric and perchloric media journal, November 1998

Kinetic Analysis of Oxygen Reduction on Pt(111) in Acid Solutions: Intrinsic Kinetic Parameters and Anion Adsorption Effects journal, April 2004

Improved Rate for the Oxygen Reduction Reaction in a Sulfuric Acid Electrolyte using a Pt(111) Surface Modified with Melamine journal, January 2021

Catalyst and Process for Producing the Same, Catalytic Electrode and Process for Producing the Same, Membrane/Electrode Union, and Electrochemical Device patent-application, November 2006

Two-Dimensional Self-Assembled Structures of Melamine and Melem at the Aqueous Solution−Au(111) Interface † journal, February 2011

Surface coordination chemistry of well-defined platinum electrodes: surface polyprotic acidity of platinum(111)(2 .sqroot. 3 .times. 2 .sqroot. 3)R30.degree.-hydrogen isocyanide journal, May 1985

Advanced Platinum Alloy Electrocatalysts for the Oxygen Reduction Reaction journal, April 2012

Direct Observation of Complexation of Alkali Cations on Cyanide-Modified Pt(111) by Scanning Tunneling Microscopy journal, January 1996

Energy and fuels from electrochemical interfaces journal, December 2016

Structural effects of adsorbed CN adlayers on the co-adsorption of OH− at the Pt(111) surface in sulfuric acid medium journal, July 1999

In-situ spectroscopy of cyanide vibrations on Pt(111) and Pt(110) electrode surfaces: potential dependencies and the influence of surface disorder journal, July 1995

Distinction between Intermediates Produced in Main and Side Electrodic Reactions journal, December 1966

Ordered Growth of Upright Melamine Species on Ni{111}: A Study with Scanning Tunnelling Microscopy and Reflection Absorption Infrared Spectroscopy journal, March 2012

Characterization of an electrode adlayer by in-situ infrared spectroscopy: cyanide on Pt(111) journal, July 1995

Facile Approach to Enhance Oxygen Reduction Activity by Modification of Platinum Nanoparticles by Melamine-Formaldehyde Polymer journal, January 2019

Cation Effects on Infrared Reflection Absorption Spectra of Cyanide Adsorbed on Pt(111) Electrode in Electrolyte Solutions journal, August 1997

Enhanced electrocatalysis of the oxygen reduction reaction based on patterning of platinum surfaces with cyanide journal, August 2010

The role of non-covalent interactions in electrocatalytic fuel-cell reactions on platinum journal, August 2009

Enhancing Hydrogen Evolution Activity in Water Splitting by Tailoring Li+-Ni(OH)2-Pt Interfaces journal, December 2011

Catalyst for oxygen reduction reaction in fuel cells patent, June 2016

At Least Three Contiguous Atoms Are Necessary for CO Formation during Methanol Electrooxidation on Platinum journal, October 2006

Design of electrocatalysts for oxygen- and hydrogen-involving energy conversion reactions journal, January 2015

Cyanide adsorbed as a monolayer at the low-index surface planes of platinum metal electrodes: an in situ study by infrared spectroscopy journal, September 1993

Melamine Structures on the Au(111) Surface journal, July 2008

Surface science studies of model fuel cell electrocatalysts journal, April 2002

Ordered ionic layers formed on platinum(111) from aqueous solutions journal, January 1985

Oxygen Electrochemistry as a Cornerstone for Sustainable Energy Conversion
journal, December 2013

Mesostructured thin films as electrocatalysts with tunable composition and surface morphology
journal, November 2012

Recent Advances in Electrocatalysts for Oxygen Reduction Reaction
journal, February 2016

Voltammetric and spectroscopic characterization of cyanide adlayers on Pt(h,k,l) in an acidic medium
journal, January 1998

Isotopological Supramolecular Networks from Melamine and Fatty Acids
journal, December 2008

Hydrogen-Bonded Structures of Trimesic and Melamine on Highly Oriented Pyrolytic Graphite
journal, June 2014

Understanding Catalytic Activity Trends in the Oxygen Reduction Reaction
journal, December 2017

Fuel Cell Electrodes
patent-application, January 2013

Electrolyte-Dependent Oxygen Evolution Reactions in Alkaline Media: Electrical Double Layer and Interfacial Interactions
journal, August 2019

Oxygen Reduction on Platinum Low-Index Single-Crystal Surfaces in Sulfuric Acid Solution: Rotating Ring-Pt(hkl) Disk Studies
journal, March 1995

Structural Effects on the Oxygen Reduction Reaction on Pt Single-Crystal Electrodes Modified with Melamine
journal, February 2020

Unique Activity of Platinum Adislands in the CO Electrooxidation Reaction
journal, November 2008

Selective catalysts for the hydrogen oxidation and oxygen reduction reactions by patterning of platinum with calix[4]arene molecules
journal, October 2010

Trends in activity for the water electrolyser reactions on 3d M(Ni,Co,Fe,Mn) hydr(oxy)oxide catalysts
journal, May 2012

Self-Assembled Melamine Monolayer on Cu(111)
journal, May 2013

Self-Assembly of Upright, Partially Dehydrogenated Melamine on Pd(111)
journal, October 2013

Potential modulated reflectance spectroscopy of Pt(111) in acidic and alkaline media: cyanide adsorption
journal, March 1999

Cyclic Voltammetry, FTIRS, and DEMS Study of the Electrooxidation of Carbon Monoxide, Formic Acid, and Methanol on Cyanide-Modified Pt(111) Electrodes
journal, June 2009

Lattice-strain control of the activity in dealloyed core–shell fuel cell catalysts
journal, April 2010

pH and potential dependence of the electrical double layer at well-defined electrode surfaces: Cs ⁺ and Ca ²⁺ ions at Pt(111) (2√3 X. 2√.3)R30°-CN, Pt(111) (√13 X√.13)R14°-CN, and Pt(111) (2 X 2)-SCN
journal, September 1985

Alloys of platinum and early transition metals as oxygen reduction electrocatalysts
journal, September 2009

Spectroelectrochemical study on CN⁻ adsorbed at Pt(111) in sulphuric and perchloric media
journal, November 1998

Kinetic Analysis of Oxygen Reduction on Pt(111) in Acid Solutions: Intrinsic Kinetic Parameters and Anion Adsorption Effects
journal, April 2004

Improved Rate for the Oxygen Reduction Reaction in a Sulfuric Acid Electrolyte using a Pt(111) Surface Modified with Melamine
journal, January 2021

Catalyst and Process for Producing the Same, Catalytic Electrode and Process for Producing the Same, Membrane/Electrode Union, and Electrochemical Device
patent-application, November 2006

Two-Dimensional Self-Assembled Structures of Melamine and Melem at the Aqueous Solution−Au(111) Interface ^†
journal, February 2011

Surface coordination chemistry of well-defined platinum electrodes: surface polyprotic acidity of platinum(111)(2 .sqroot. 3 .times. 2 .sqroot. 3)R30.degree.-hydrogen isocyanide
journal, May 1985

Advanced Platinum Alloy Electrocatalysts for the Oxygen Reduction Reaction
journal, April 2012

Direct Observation of Complexation of Alkali Cations on Cyanide-Modified Pt(111) by Scanning Tunneling Microscopy
journal, January 1996

Energy and fuels from electrochemical interfaces
journal, December 2016

Structural effects of adsorbed CN adlayers on the co-adsorption of OH⁻ at the Pt(111) surface in sulfuric acid medium
journal, July 1999

In-situ spectroscopy of cyanide vibrations on Pt(111) and Pt(110) electrode surfaces: potential dependencies and the influence of surface disorder
journal, July 1995

Distinction between Intermediates Produced in Main and Side Electrodic Reactions
journal, December 1966

Ordered Growth of Upright Melamine Species on Ni{111}: A Study with Scanning Tunnelling Microscopy and Reflection Absorption Infrared Spectroscopy
journal, March 2012

Characterization of an electrode adlayer by in-situ infrared spectroscopy: cyanide on Pt(111)
journal, July 1995

Facile Approach to Enhance Oxygen Reduction Activity by Modification of Platinum Nanoparticles by Melamine-Formaldehyde Polymer
journal, January 2019

Cation Effects on Infrared Reflection Absorption Spectra of Cyanide Adsorbed on Pt(111) Electrode in Electrolyte Solutions
journal, August 1997

Enhanced electrocatalysis of the oxygen reduction reaction based on patterning of platinum surfaces with cyanide
journal, August 2010

The role of non-covalent interactions in electrocatalytic fuel-cell reactions on platinum
journal, August 2009

Enhancing Hydrogen Evolution Activity in Water Splitting by Tailoring Li+-Ni(OH)2-Pt Interfaces
journal, December 2011

Catalyst for oxygen reduction reaction in fuel cells
patent, June 2016

At Least Three Contiguous Atoms Are Necessary for CO Formation during Methanol Electrooxidation on Platinum
journal, October 2006

Design of electrocatalysts for oxygen- and hydrogen-involving energy conversion reactions
journal, January 2015

Cyanide adsorbed as a monolayer at the low-index surface planes of platinum metal electrodes: an in situ study by infrared spectroscopy
journal, September 1993

Melamine Structures on the Au(111) Surface
journal, July 2008

Surface science studies of model fuel cell electrocatalysts
journal, April 2002

Ordered ionic layers formed on platinum(111) from aqueous solutions
journal, January 1985