Stable ammonia absorbents

Cussler, Edward; McCormick, Alon; Malmali, Mohammadmahdi

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Title: Stable ammonia absorbents

Abstract

The present disclosure relates to systems and methods of making ammonia using stable ammonia absorbents. The system and method for producing ammonia, comprises a reactor comprising a catalyst that converts at least a portion of nitrogen feed gas and at least a portion of hydrogen feed gas to ammonia (NH3) forming a reaction mixture comprising the ammonia, unreacted nitrogen, and unreacted hydrogen. An absorber configured to selectively absorb ammonia from the reaction mixture at a temperature of about 180 deg. C. to 330 deg. C. and a pressure of about 1-20 bar, the absorber comprising a solid absorbent. Preferably the solid absorbent is at least one metal halide and a solid support. The unabsorbed ammonium, the unreacted nitrogen, and unreacted hydrogen gas are recycled to the reactor.

Inventors:: Cussler, Edward; McCormick, Alon; Malmali, Mohammadmahdi

Issue Date:: 2023-01-10

Research Org.:: Univ. of Minnesota, Minneapolis, MN (United States)

Sponsoring Org.:: USDOE Advanced Research Projects Agency - Energy (ARPA-E)

OSTI Identifier:: 1987008

Patent Number(s):: 11548789

Application Number:: 16/759,950

Assignee:: Regents of the University of Minnesota (Minneapolis, MN)

DOE Contract Number:: AR0000804

Resource Type:: Patent

Resource Relation:: Patent File Date: 11/02/2018

Country of Publication:: United States

Language:: English

Citation Formats


                    Cussler, Edward, McCormick, Alon, and Malmali, Mohammadmahdi. Stable ammonia absorbents.  United States: N. p., 2023. 
        Web.

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                    Cussler, Edward, McCormick, Alon, & Malmali, Mohammadmahdi. Stable ammonia absorbents.  United States.

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                    Cussler, Edward, McCormick, Alon, and Malmali, Mohammadmahdi. Tue .  
        "Stable ammonia absorbents".  United States.  https://www.osti.gov/servlets/purl/1987008.

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@article{osti_1987008,

  title        = {Stable ammonia absorbents},

  author       = {Cussler, Edward and McCormick, Alon and Malmali, Mohammadmahdi},

  abstractNote = {The present disclosure relates to systems and methods of making ammonia using stable ammonia absorbents. The system and method for producing ammonia, comprises a reactor comprising a catalyst that converts at least a portion of nitrogen feed gas and at least a portion of hydrogen feed gas to ammonia (NH3) forming a reaction mixture comprising the ammonia, unreacted nitrogen, and unreacted hydrogen. An absorber configured to selectively absorb ammonia from the reaction mixture at a temperature of about 180 deg. C. to 330 deg. C. and a pressure of about 1-20 bar, the absorber comprising a solid absorbent. Preferably the solid absorbent is at least one metal halide and a solid support. The unabsorbed ammonium, the unreacted nitrogen, and unreacted hydrogen gas are recycled to the reactor.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2023},

  month        = {1}

}

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Works referenced in this record:

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Similar Records

Title: Stable ammonia absorbents

Abstract

Citation Formats

Thermogravimetric examination of the dehydration process of calcium bromide hydrate under quasi isothermal and quasi isobaric conditions journal, June 1979

The Monoammoniate of Lithium Borohydride, Li(NH 3 )BH 4 : An Effective Ammonia Storage Compound journal, June 2009

Ammonia sorption on composites 'CaCl2 in inorganic host matrix': isosteric chart and its performance journal, July 2006

Thermodynamics on Ammonia Absorption of Metal Halides and Borohydrides journal, July 2014

Converting Wind Energy to Ammonia at Lower Pressure journal, November 2017

Production of Ammonia from Air and Water patent-application, October 2011

Better Absorbents for Ammonia Separation journal, March 2018

Kinetic Expression with Diffusion Correction for Ammonia Synthesis on Industrial Catalyst journal, November 1968

Composites “binary salts in porous matrix” for adsorption heat transformation journal, February 2013

Metal-organic frameworks with high capacity and selectivity for harmful gases journal, August 2008

Indirect, Reversible High-Density Hydrogen Storage in Compact Metal Ammine Salts journal, July 2008

Rate equation and mechanism of ammonia synthesis at industrial conditions journal, February 1964

Dissociation pressures and enthalpies of reaction in MgCl2 · nH2O and CaCl2 · nNH3 journal, June 1981

Ammonia sorbent development for on-board H2 purification journal, March 2015

Functionalization of carbon silica composites with active metal sites for NH 3 and SO 2 adsorption journal, February 2016

Performance of a Small-Scale Haber Process journal, March 2016

Modeling of fixed bed adsorption of phenols on granular activated carbon journal, June 2008

Low energy ammonia synthesis process patent, April 1979

Continuous lumping of nonlinear chemical kinetics journal, August 1989

Ammonia synthesis method patent, April 1989

Novel ammonia sorbents “porous matrix modified by active salt” for adsorptive heat transformation journal, May 2010

Thermal Conductivity of Gaseous Ammonia in the Temperature Range 358-925 k. journal, January 1981

Activation on Ammonia Absorbing Reaction for Magnesium Chloride journal, November 2015

Dominance of Surface Barriers in Molecular Transport through Silicalite-1 journal, November 2013

Ammonia Removal Using Activated Carbons: Effect of the Surface Chemistry in Dry and Moist Conditions journal, December 2011

Ammonia as a green fuel and hydrogen source for vehicular applications journal, May 2009

Process for Making Ammonia patent-application, May 2015

Ammonia for hydrogen storage: challenges and opportunities journal, January 2008

Ammonia Synthesis at Low Pressure journal, August 2017

A high-density ammonia storage/delivery system based on Mg(NH3)6Cl2 for SCR – DeNO x in vehicles journal, April 2006

Detonator of the population explosion journal, July 1999

Exceptional ammonia uptake by a covalent organic framework journal, February 2010

Generation of Nanopores during Desorption of NH 3 from Mg(NH 3 ) 6 Cl 2 journal, January 2006

Application of the Temkin kinetic equation to ammonia synthesis in large-scale reactors journal, January 1952

Solid-gas chemical heat pumps: Field of application and performance of the internal heat of reaction recovery process journal, May 1993

Column absorption for reproducible cyclic separation in small scale ammonia synthesis journal, February 2017

Ammonia absorption at haber process conditions journal, March 2012

Solid ammonia as energy carrier: Current status and future prospects journal, October 2009

Ammonia Absorption on Alkaline Earth Halides as Ammonia Separation and Storage Procedure journal, January 2004

Process for Making Ammonia patent-application, June 2017

How a century of ammonia synthesis changed the world journal, September 2008

Ammonia adsorption by MgCl2, CaCl2 and BaCl2 confined to porous alumina: the fixed bed adsorber journal, May 2005

Kinetics of water adsorption on silica Fuji Davison RD journal, November 2006

Ammonia Synthesis at Reduced Pressure via Reactive Separation journal, August 2016

The kinetics of water adsorption on porous alumina journal, September 1970

Evaluation of MOFs for air purification and air quality control applications: Ammonia removal from air journal, March 2015

Ammonia-storage in lithium intercalated fullerides journal, January 2015

Metal ammine complexes for hydrogen storage journal, January 2005

Thermogravimetric examination of the dehydration process of calcium bromide hydrate under quasi isothermal and quasi isobaric conditions
journal, June 1979

The Monoammoniate of Lithium Borohydride, Li(NH ₃ )BH ₄ : An Effective Ammonia Storage Compound
journal, June 2009

Ammonia sorption on composites 'CaCl2 in inorganic host matrix': isosteric chart and its performance
journal, July 2006

Thermodynamics on Ammonia Absorption of Metal Halides and Borohydrides
journal, July 2014

Converting Wind Energy to Ammonia at Lower Pressure
journal, November 2017

Production of Ammonia from Air and Water
patent-application, October 2011

Better Absorbents for Ammonia Separation
journal, March 2018

Kinetic Expression with Diffusion Correction for Ammonia Synthesis on Industrial Catalyst
journal, November 1968

Composites “binary salts in porous matrix” for adsorption heat transformation
journal, February 2013

Metal-organic frameworks with high capacity and selectivity for harmful gases
journal, August 2008

Indirect, Reversible High-Density Hydrogen Storage in Compact Metal Ammine Salts
journal, July 2008

Rate equation and mechanism of ammonia synthesis at industrial conditions
journal, February 1964

Dissociation pressures and enthalpies of reaction in MgCl2 · nH2O and CaCl2 · nNH3
journal, June 1981

Ammonia sorbent development for on-board H2 purification
journal, March 2015

Functionalization of carbon silica composites with active metal sites for NH 3 and SO 2 adsorption
journal, February 2016

Performance of a Small-Scale Haber Process
journal, March 2016

Modeling of fixed bed adsorption of phenols on granular activated carbon
journal, June 2008

Low energy ammonia synthesis process
patent, April 1979

Continuous lumping of nonlinear chemical kinetics
journal, August 1989

Ammonia synthesis method
patent, April 1989

Novel ammonia sorbents “porous matrix modified by active salt” for adsorptive heat transformation
journal, May 2010

Thermal Conductivity of Gaseous Ammonia in the Temperature Range 358-925 k.
journal, January 1981

Activation on Ammonia Absorbing Reaction for Magnesium Chloride
journal, November 2015

Dominance of Surface Barriers in Molecular Transport through Silicalite-1
journal, November 2013

Ammonia Removal Using Activated Carbons: Effect of the Surface Chemistry in Dry and Moist Conditions
journal, December 2011

Ammonia as a green fuel and hydrogen source for vehicular applications
journal, May 2009

Process for Making Ammonia
patent-application, May 2015

Ammonia for hydrogen storage: challenges and opportunities
journal, January 2008

Ammonia Synthesis at Low Pressure
journal, August 2017

A high-density ammonia storage/delivery system based on Mg(NH3)6Cl2 for $SCR$ – ${DeNO}_{x}$ in vehicles
journal, April 2006

Detonator of the population explosion
journal, July 1999

Exceptional ammonia uptake by a covalent organic framework
journal, February 2010

Generation of Nanopores during Desorption of NH ₃ from Mg(NH ₃ ) ₆ Cl ₂
journal, January 2006

Application of the Temkin kinetic equation to ammonia synthesis in large-scale reactors
journal, January 1952

Solid-gas chemical heat pumps: Field of application and performance of the internal heat of reaction recovery process
journal, May 1993

Column absorption for reproducible cyclic separation in small scale ammonia synthesis
journal, February 2017

Ammonia absorption at haber process conditions
journal, March 2012

Solid ammonia as energy carrier: Current status and future prospects
journal, October 2009

Ammonia Absorption on Alkaline Earth Halides as Ammonia Separation and Storage Procedure
journal, January 2004

Process for Making Ammonia
patent-application, June 2017

How a century of ammonia synthesis changed the world
journal, September 2008

Ammonia adsorption by MgCl2, CaCl2 and BaCl2 confined to porous alumina: the fixed bed adsorber
journal, May 2005

Kinetics of water adsorption on silica Fuji Davison RD
journal, November 2006

Ammonia Synthesis at Reduced Pressure via Reactive Separation
journal, August 2016

The kinetics of water adsorption on porous alumina
journal, September 1970

Evaluation of MOFs for air purification and air quality control applications: Ammonia removal from air
journal, March 2015

Ammonia-storage in lithium intercalated fullerides
journal, January 2015

Metal ammine complexes for hydrogen storage
journal, January 2005