Methods for electropolishing and coating aluminum on air and/or moisture sensitive substrates

Freiderich, John W.; Boyd, Tasha L.

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Title: Methods for electropolishing and coating aluminum on air and/or moisture sensitive substrates

Abstract

Methods for electropolishing and coating aluminum on a surface of an air and/or moisture sensitive substrate, including: in a vessel, submerging the substrate in a first molten salt bath and applying an anodizing current to the substrate at a first temperature to electropolish the surface of the substrate; wherein the first molten salt bath includes one of a first organic salt bath and first inorganic salt bath; wherein, when used, the first organic salt bath includes one of (a) aluminum halide and ionic liquid, (b) a combination of an aluminum halide and halogenatedmethylphenylsulfone (C₆(H_5-y,X_y)SO₂CX₃, where y is a number from 0-5), (c) a combination of an aluminum halide, an ionic liquid, and halogenatedmethylphenylsulfone (C₆(H_5-y,X_y)SO₂CX₃), and (d) AlF₃-organofluoride-hydrofluoric acid adduct; wherein, when used, the first inorganic salt bath includes aluminum halide and alkali metal halide; and wherein the anodizing current is 10-30 mA/cm².

Inventors:: Freiderich, John W.; Boyd, Tasha L.

Issue Date:: 2022-10-04

Research Org.:: Oak Ridge Y-12 Plant (Y-12), Oak Ridge, TN (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1986648

Patent Number(s):: 11459658

Application Number:: 17/379,395

Assignee:: Consolidated Nuclear Security, LLC (Oak Ridge, TN)

DOE Contract Number:: NA0001942

Resource Type:: Patent

Resource Relation:: Patent File Date: 07/19/2021

Country of Publication:: United States

Language:: English

Citation Formats


                    Freiderich, John W., and Boyd, Tasha L. Methods for electropolishing and coating aluminum on air and/or moisture sensitive substrates.  United States: N. p., 2022. 
        Web.

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                    Freiderich, John W., & Boyd, Tasha L. Methods for electropolishing and coating aluminum on air and/or moisture sensitive substrates.  United States.

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                    Freiderich, John W., and Boyd, Tasha L. Tue .  
        "Methods for electropolishing and coating aluminum on air and/or moisture sensitive substrates".  United States.  https://www.osti.gov/servlets/purl/1986648.

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@article{osti_1986648,

  title        = {Methods for electropolishing and coating aluminum on air and/or moisture sensitive substrates},

  author       = {Freiderich, John W. and Boyd, Tasha L.},

  abstractNote = {Methods for electropolishing and coating aluminum on a surface of an air and/or moisture sensitive substrate, including: in a vessel, submerging the substrate in a first molten salt bath and applying an anodizing current to the substrate at a first temperature to electropolish the surface of the substrate; wherein the first molten salt bath includes one of a first organic salt bath and first inorganic salt bath; wherein, when used, the first organic salt bath includes one of (a) aluminum halide and ionic liquid, (b) a combination of an aluminum halide and halogenatedmethylphenylsulfone (C6(H5-y,Xy)SO2CX3, where y is a number from 0-5), (c) a combination of an aluminum halide, an ionic liquid, and halogenatedmethylphenylsulfone (C6(H5-y,Xy)SO2CX3), and (d) AlF3-organofluoride-hydrofluoric acid adduct; wherein, when used, the first inorganic salt bath includes aluminum halide and alkali metal halide; and wherein the anodizing current is 10-30 mA/cm2.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2022},

  month        = {10}

}

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Similar Records

Title: Methods for electropolishing and coating aluminum on air and/or moisture sensitive substrates

Abstract

Citation Formats

Electrodeposition of aluminum from molten AlCl3–NaCl–KCl mixture journal, August 2006

Method for molten salt electroplating of steel patent, October 1990

Hot dip plating method and apparatus patent, November 2000

Aluminum electroplating apparatus patent, August 1992

Coating Method Using Ionic Liquid patent-application, July 2012

Electrodeposition of Aluminum patent, August 1948

Aluminum electroplating solution patent, April 1983

Aluminum or aluminum alloy molten salt electroplating bath having good throwing power, electroplating method using the bath, and pretreatment method of the bath patent, March 2018

Electrodeposition of Aluminum patent, August 1948

Electrodeposition of Al, Mn, and Al–Mn Alloy on aluminum electrodes from molten salt (AlCl3–NaCl–KCl) journal, January 2009

Methods and materials for electroplating aluminum in ionic liquids patent, February 2018

Aluminum electroplating method patent, August 1991

Some Problems Concerning Aluminium Electro-plating in Molten Salts. journal, January 1980

Electrolyte for the electrodeposition of aluminum patent, November 1983

Aluminum Plating Solution, Method for Manufacturing Aluminum Film, and Porous Aluminum Object patent-application, May 2017

Equipment for use in molten metal plating bath patent, May 2000

Electrodeposition of elemental zirconium patent-application, May 2012

Aluminum plating cell patent, May 1981

Aluminium electroplating formulations patent, July 2007

Apparatus for the electrodeposition of metal patent, February 1986

Electrodeposition of alloys and compounds from high-temperature molten salts journal, January 2017

Methods for producing a high temperature oxidation resistant MCrAlX coating on superalloy substrates patent, September 2017

Fabric care composition patent-application, February 2004

Method for cleaning aluminum articles patent, June 1981

Co-deposition of Al–Cr–Ni alloys using constant potential and potential pulse techniques in AlCl3–NaCl–KCl molten salt journal, February 2007

Overview over studies of electrodeposition of Al or Al alloys from low temperature chloroaluminate molten salts journal, October 2016

Electrodepositing aluminum coating on uranium from aluminum chloride-1-ethyl-3-methylimidazolium chloride ionic liquid journal, January 2017

Aluminum electroplating solution patent-application, July 2013

Fused Salt Method for Coating Uranium with a Metal patent, February 1959

Aspects of Molybdenum Chemistry in the Basic NaCl / AlCl3 Melt at 175°C journal, October 1977

Electrodeposition of Aluminum patent, August 1948

Method of plating light weight metal to enhance lateral corrosion resistance patent, June 1979

Plating bath for electrodeposition of aluminum and plating process making use of the bath patent, February 1990

Leveling Additives for Electrodeposition patent-application, March 2016

Plating bath for electrodeposition of aluminum and process for the same patent, May 1988

Apparatus and Method for Ionic Liquid Electroplating patent-application, April 2015

Preparation of Metal Substrate Surfaces for Electroplating in Ionic Liquids patent-application, November 2015

Electrodeposition of aluminum from molten AlCl3–NaCl–KCl mixture
journal, August 2006

Method for molten salt electroplating of steel
patent, October 1990

Hot dip plating method and apparatus
patent, November 2000

Aluminum electroplating apparatus
patent, August 1992

Coating Method Using Ionic Liquid
patent-application, July 2012

Electrodeposition of Aluminum
patent, August 1948

Aluminum electroplating solution
patent, April 1983

Aluminum or aluminum alloy molten salt electroplating bath having good throwing power, electroplating method using the bath, and pretreatment method of the bath
patent, March 2018

Electrodeposition of Aluminum
patent, August 1948

Electrodeposition of Al, Mn, and Al–Mn Alloy on aluminum electrodes from molten salt (AlCl3–NaCl–KCl)
journal, January 2009

Methods and materials for electroplating aluminum in ionic liquids
patent, February 2018

Aluminum electroplating method
patent, August 1991

Some Problems Concerning Aluminium Electro-plating in Molten Salts.
journal, January 1980

Electrolyte for the electrodeposition of aluminum
patent, November 1983

Aluminum Plating Solution, Method for Manufacturing Aluminum Film, and Porous Aluminum Object
patent-application, May 2017

Equipment for use in molten metal plating bath
patent, May 2000

Electrodeposition of elemental zirconium
patent-application, May 2012

Aluminum plating cell
patent, May 1981

Aluminium electroplating formulations
patent, July 2007

Apparatus for the electrodeposition of metal
patent, February 1986

Electrodeposition of alloys and compounds from high-temperature molten salts
journal, January 2017

Methods for producing a high temperature oxidation resistant MCrAlX coating on superalloy substrates
patent, September 2017

Fabric care composition
patent-application, February 2004

Method for cleaning aluminum articles
patent, June 1981

Co-deposition of Al–Cr–Ni alloys using constant potential and potential pulse techniques in AlCl3–NaCl–KCl molten salt
journal, February 2007

Overview over studies of electrodeposition of Al or Al alloys from low temperature chloroaluminate molten salts
journal, October 2016

Electrodepositing aluminum coating on uranium from aluminum chloride-1-ethyl-3-methylimidazolium chloride ionic liquid
journal, January 2017

Aluminum electroplating solution
patent-application, July 2013

Fused Salt Method for Coating Uranium with a Metal
patent, February 1959

Aspects of Molybdenum Chemistry in the Basic NaCl / AlCl3 Melt at 175°C
journal, October 1977

Electrodeposition of Aluminum
patent, August 1948

Method of plating light weight metal to enhance lateral corrosion resistance
patent, June 1979

Plating bath for electrodeposition of aluminum and plating process making use of the bath
patent, February 1990

Leveling Additives for Electrodeposition
patent-application, March 2016

Plating bath for electrodeposition of aluminum and process for the same
patent, May 1988

Apparatus and Method for Ionic Liquid Electroplating
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Preparation of Metal Substrate Surfaces for Electroplating in Ionic Liquids
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